CN105802740B - A kind of candle pigment and its production technology - Google Patents
A kind of candle pigment and its production technology Download PDFInfo
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- CN105802740B CN105802740B CN201610161382.5A CN201610161382A CN105802740B CN 105802740 B CN105802740 B CN 105802740B CN 201610161382 A CN201610161382 A CN 201610161382A CN 105802740 B CN105802740 B CN 105802740B
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- pigment
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- candle
- thermoplastic elastomer
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
- C11C5/002—Ingredients
- C11C5/004—Ingredients dyes, pigments; products giving a coloured flame
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
- C11C5/008—Candles characterised by their form; Composite candles, e.g. candles containing zones of different composition, inclusions, or the like
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- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Composite Materials (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provides a kind of candle pigment that dispersion staining power is strong, color saturation is high, including the following components calculated by weight：65 85 parts of wax, 1 10 parts of pigment, 15 parts of thermoplastic elastomer (TPE), 15 parts of plasticiser；A kind of production technology of candle pigment:A. 15 parts of 1 10 parts of pigment and thermoplastic elastomer (TPE) are well mixed and form mixture；B. 15 parts of plasticiser is added in the mixture, puts into extruder after being well mixed, semi-finished product are extruded at 120 DEG C 150 DEG C；C. extruder is put into after being well mixed 65 85 parts of semi-finished product and wax, wax stone is extruded at 90 DEG C 130 DEG C；The candle pigment of present invention dispersion staining ability in paraffin is strong, for candle simple production process, and candle finished product color saturation is high；Pigment first mixes with thermoplastic elastomer (TPE) and produces particle aggregation when pigment can be avoided directly to be mixed with wax；Wax stone is by repeatedly grinding, reheating extrusion, and finished color uniform colorless is poor.
Description
Technical field
The present invention relates to candle pigment art, more particularly, to be a kind of candle pigment and its production technology.
Background technology
Colored candle is typically mixed into casting after candle pigment by paraffin and formed.Because traditional candle pigment can not be effective
Be dispersed in paraffin, tinting strength, tinting power is not enough, to be incubated and mix the long period during production, and finished product color saturation not enough,
Color is not bright-coloured, pigment concentration content is not high, the easy fire-retardant candle if excessive candle pigment is added.
The content of the invention
It is an object of the invention to overcome above-mentioned deficiency, there is provided a kind of candle that dispersion staining power is strong, color saturation is high
Pigment and its production technology.
To achieve the above object, technical solution of the invention is：A kind of candle pigment, including calculate by weight with
Lower component：65-85 parts of wax, 1-10 parts of pigment, thermoplastic elastomer (TPE)（TPE）1-5 parts.
It is preferred that, the wax includes one kind or several in macromolecule synthesising wax, low molecule synthetic wax, non-synthetic one-component wax
Kind；The pigment is included in soluble dyes, non-solubility pigment, inorganic pigment, organic pigment, natural pigment, synthetic dyestuff
One or more.
It is preferred that, the wax include PE polyethylene, PP polypropylene, HDPE high density polyethylene (HDPE)s, LDPE low density polyethylene (LDPE)s,
The resistance to punching of LLDPE LLDPEs, PVC polyvinyl chloride, GPPS General Purpose Polystyrenres, EPS polystyrene foams, HIPS
Hitting property polystyrene, AS, SAN styrene-acrylonitrile copolymer, ABS acrylonitrile-butadiene-styrene copolymerized compound,
Co-polymer, PET polyethylene terephthalates, the PBT of PMMA polymethacrylates, EVA ethene-vinyl acetate gather
The poly- carbonic acid resin of terephthaldehyde's acid butyl ester, PA polyamide, PC, POM polyoxymethylene resins, PPO polyphenylene oxide, PPS polyphenylene sulfides,
One kind in PU polyurethane, PS polystyrene polymerics or low molecule synthetic wax, non-synthetic one-component wax, native paraffin
Or it is several.
It is preferred that, the thermoplastic elastomer (TPE) includes olefin hydrocarbons thermoplasticity elastic body, diene analog thermoplastic elastomer, chloroethene
Ethylenic thermoplastic elastomer, styrene analog thermoplastic elastomer, polyurethane-type thermoplastic elastomer, etc. other thermoplastic elastomer (TPE)s
One or more in TPE derivative copolymers.
It is preferred that, the pigment includes pigment yellow（PY), pigment is orange（PO), paratonere（PR), pigment violet（PV）, pigment
It is blue（PB), naphthol green（PG), pigment brown（PBr), pigment black（PBk), Pigment white（Other extraordinary fluorescent materials synthesis face such as PW),
The one or more of material and other mixing secondary color synthetic dyestuffs.
It is preferred that, in addition to 1-5 parts of plasticiser；It is pungent that the plasticiser includes ditridecyl phthalate, phthalic acid two
Ester, di-n-octyl phthalate, BBP(Butyl Benzyl Phthalate, di-sec-octyl phthalate, dicyclohexyl phthalate,
Dibutyl phthalate, diisobutyl phthalate, repefral, diethyl phthalate, adjacent benzene two
Formic acid dinonyl, diisooctyl phthalate, etc. one or more in other phthalate plasticizer or plasticiser.
A kind of production technology of candle pigment, comprises the following steps:
A. 1-5 parts of 1-10 parts of pigment and thermoplastic elastomer (TPE) are well mixed and form mixture；
B. extruder is put into the mixture, and semi-finished product are extruded at 120 DEG C -150 DEG C；
C. extruder is put into after being well mixed 65-85 parts of semi-finished product and wax, wax stone is extruded at 90 DEG C -130 DEG C；
D. wax stone is put into grinder and grinds to form chip or irregular thread.
A kind of production technology of candle pigment, comprises the following steps:
A. 1-5 parts of 1-10 parts of pigment and thermoplastic elastomer (TPE) are well mixed and form mixture；
B. 1-5 parts of plasticiser is added in the mixture, extruder is put into after being well mixed, and is extruded at 120 DEG C -150 DEG C
Form semi-finished product；
C. extruder is put into after being well mixed 65-85 parts of semi-finished product and wax, wax stone is extruded at 90 DEG C -130 DEG C；
D. wax stone is put into grinder and grinds to form chip or irregular thread.
It is preferred that, step a also includes at least standing mixture into 12 hours；Also include step:
E. step d wax stone chip is put into extruder, second of wax stone is extruded at 90 DEG C -130 DEG C；By second
Secondary wax stone input grinder grinds to form chip, and second of wax stone chip is put into extruder, is extruded at 90 DEG C -130 DEG C
Third time wax stone；Third time wax stone input grinder is ground to form into chip or irregular thread.
It is preferred that, step a also includes at least standing mixture into 12 hours；Also include step：
E. wax stone chip is put into extruder, wax stone is extruded at 90 DEG C -130 DEG C, wax stone input grinder is ground
Wear into chip or irregular thread；
F. repeat step e at least 1 time or until wax stone chip color is uniform.
By using above-mentioned technical scheme, the beneficial effects of the invention are as follows：The candle pigment of the present invention divides in paraffin
Dissipate colorability it is strong, for candle simple production process, candle finished product color saturation is high；Pigment is first mixed with thermoplastic elastomer (TPE)
Conjunction produces particle aggregation when pigment can be avoided directly to be mixed with wax；Wax stone is by repeatedly grinding, reheating extrusion, and finished color is equal
Even no color differnece.
Embodiment
Specific examples below further illustrates the present invention.
Embodiment 1：
A kind of candle pigment of the present invention, including the following components calculated by weight：65 parts of wax, 10 parts of pigment, thermoplastic elastomehc
5 parts of body of property, 5 parts of plasticiser；The wax is Tissuemat E, and the pigment is the pigment Yellow 14 in pigment yellow（CAS 5468-75-
7）, the plasticiser is dioctyl phthalate, and the thermoplastic elastomer (TPE) is diene analog thermoplastic elastomer.
A kind of production technology of candle pigment, comprises the following steps:
A. 5 parts of 10 parts of pigment and thermoplastic elastomer (TPE) are well mixed and form mixture by weight, mixture is stood 12
Individual hour；
B. add 5 parts of plasticiser in the mixture, it is well mixed after put into extruder, be extruded at 120 DEG C half into
Product；If pigment is not scattered good with the plasticiser direct hybrid pigment particle later stage；
C. extruder is put into after being well mixed 65 parts of semi-finished product and wax, wax stone is extruded at 90 DEG C；
D. wax stone is put into grinder and grinds to form chip or irregular thread；
E. wax stone chip is put into extruder, wax stone is extruded at 90 DEG C, wax stone input grinder ground to form broken
Bits are irregular thread；
F. the wax stone chip for repeating e2 formation of step is candle pigment.
Pigment first mixed with thermoplastic elastomer (TPE) and stand after 12 hours formed pigment molecule bleeding power it is stronger, finished product
Color is evenly.
Embodiment 2：
A kind of candle pigment of the present invention, including the following components calculated by weight：85 parts of wax, 1 part of pigment, thermoplastic elastic
1 part of body, 1 part of plasticiser；The wax is Tissuemat E, and the pigment is naphthol green, and the plasticiser is the ring of phthalic acid two
Own ester, the thermoplastic elastomer (TPE) is polyvinyl chloride-base thermoplastic elastomer.
A kind of production technology of candle pigment, comprises the following steps:
A. 1 part of 1 part of pigment and thermoplastic elastomer (TPE) are well mixed and form mixture by weight, mixture is stood 24
Individual hour；
B. add 1 part of plasticiser in the mixture, it is well mixed after put into extruder, be extruded at 150 DEG C half into
Product；
C. extruder is put into after being well mixed 85 parts of semi-finished product and wax, wax stone is extruded at 130 DEG C；
D. wax stone is put into grinder and grinds to form chip or irregular thread；
E. wax stone chip is put into extruder, wax stone is extruded at 130 DEG C, wax stone input grinder ground to form broken
Bits are irregular thread；
F. the wax stone chip for repeating e1 formation of step is candle pigment.
Embodiment 3：
A kind of candle pigment, including the following components calculated by weight：70 parts of wax, 5 parts of pigment, thermoplastic elastomer (TPE) 3；Institute
Wax is stated for PMMA polymethacrylates waxes, the pigment is paratonere 57:1（CAS 5281-4-9）, the plasticiser is neighbour
Rutgers, the thermoplastic elastomer (TPE) is styrene analog thermoplastic elastomer.
A kind of production technology of above-mentioned candle pigment, comprises the following steps:
A. 3 parts of 5 parts of pigment and thermoplastic elastomer (TPE) are well mixed and form mixture by weight, pigment is commercially available pigment
Powder, thermoplastic elastomer (TPE) is commercially available thermoplastic elastic particle；
B. mixture is put into extruder, semi-finished product is extruded at 130 DEG C；
C. extruder is put into after being well mixed 70 parts of semi-finished product and wax, wax stone is extruded at 100 DEG C；
D. wax stone is put into grinder and grinds to form chip or irregular thread.
Embodiment 4：
A kind of candle pigment, including the following components calculated by weight：80 parts of wax, 6 parts of pigment, 4 parts of thermoplastic elastomer (TPE)；
The wax is polyamide wax, and the pigment is the pigment blue 15 in alizarol saphirol（CAS 147-14-8）, the thermoplastic elastomer (TPE)
For polyurethane-type thermoplastic elastomer.
A kind of production technology of candle pigment, comprises the following steps:
A. it is well mixed by weight by 4 parts of 6 parts of pigment and thermoplastic elastomer (TPE) and forms mixture, standing mixt 18 is small
When；
B. extruder will be put into mixture, semi-finished product is extruded at 140 DEG C；
C. extruder is put into after being well mixed 80 parts of semi-finished product and wax, wax stone is extruded at 120 DEG C；
D. wax stone is put into grinder and grinds to form chip or irregular thread；
E. step d wax stone chip is put into extruder, second of wax stone is extruded at 90 DEG C -130 DEG C；By second
Secondary wax stone input grinder grinds to form chip, and second of wax stone chip is put into extruder, is extruded at 90 DEG C -130 DEG C
Third time wax stone；Third time wax stone input grinder is ground to form into chip or irregular thread.
Embodiment 5：
A kind of candle pigment, including the following components calculated by weight：65-85 parts of wax, 1-10 parts of pigment, thermoplastic elastic
1-5 parts of body；The wax includes the one or more in macromolecule synthesising wax, low molecule synthetic wax, non-synthetic one-component wax；It is described
Pigment include soluble dyes, non-solubility pigment, inorganic pigment, organic pigment, natural pigment, one kind in synthetic dyestuff or
It is several；The wax includes polyethylene, polypropylene, high density polyethylene (HDPE), low density polyethylene (LDPE), LLDPE, polychlorostyrene
Ethene, General Purpose Polystyrenre, polystyrene foam, impact resistant polystyrene, styrene-acrylonitrile copolymer, acrylonitrile
- the co-polymer, poly terephthalic acid of butadiene-styrene copolymerized compound, polymethacrylates, ethene-vinyl acetate
It is glycol ester, PA polybutyleneterephthalate, polyamide, poly- carbonic acid resin, polyoxymethylene resin, polyphenylene oxide, polyphenylene sulfide, poly-
One or more in urethanes, polystyrene polymeric or low molecule synthetic wax, non-synthetic one-component wax；The heat
Thermoplastic elastic includes olefin hydrocarbons thermoplasticity elastic body, diene analog thermoplastic elastomer, polyvinyl chloride-base thermoplastic elastomer, benzene second
Ethylenic thermoplastic elastomer, polyurethane-type thermoplastic elastomer；The pigment includes pigment yellow, orange pigment, paratonere, pigment
In purple, alizarol saphirol, naphthol green, pigment brown, pigment black, Pigment white, extraordinary fluorescent material synthetic dyestuff, mixing secondary color synthetic dyestuff
One or more；Also include 1-5 parts of plasticiser；The plasticiser include ditridecyl phthalate, dioctyl phthalate,
Di-n-octyl phthalate, BBP(Butyl Benzyl Phthalate, di-sec-octyl phthalate, dicyclohexyl phthalate, neighbour
Dibatyl phithalate, diisobutyl phthalate, repefral, diethyl phthalate, O-phthalic
One or more in sour dinonyl, diisooctyl phthalate.
A kind of production technology of candle pigment, comprises the following steps:
A. 1-5 parts of 1-10 parts of pigment and thermoplastic elastomer (TPE) are well mixed and form mixture, standing mixt at least 12
Individual hour；
B. 1-5 parts of plasticiser is added in the mixture, extruder is put into after being well mixed, and is extruded at 120 DEG C -150 DEG C
Form semi-finished product；
C. extruder is put into after being well mixed 65-85 parts of semi-finished product and wax, wax stone is extruded at 90 DEG C -130 DEG C；
D. wax stone is put into grinder and grinds to form chip or irregular thread；
E. wax stone chip is put into extruder, wax stone is extruded at 90 DEG C -130 DEG C, wax stone input grinder is ground
Wear into chip or irregular thread；
F. repeat step e at least 1 time or until wax stone chip color is uniform.
It is above-described, only presently preferred embodiments of the present invention, it is impossible to limit the scope of this practicality implementation, it is every according to
Equivalent change and decoration that scope of the present invention patent is made, should all still fall within the range of the present invention covers.
Claims (8)
1. a kind of production technology of candle pigment, candle pigment includes the following components calculated by weight：65-85 parts of wax, pigment
1-10 parts, 1-5 parts of thermoplastic elastomer (TPE)；Production technology comprises the following steps:
A. 1-5 parts of 1-10 parts of pigment and thermoplastic elastomer (TPE) are well mixed and form mixture；
B. extruder is put into the mixture, and semi-finished product are extruded at 120 DEG C -150 DEG C；
C. extruder is put into after being well mixed 65-85 parts of semi-finished product and wax, wax stone is extruded at 90 DEG C -130 DEG C；
D. wax stone is put into grinder and grinds to form chip.
2. a kind of production technology of candle pigment according to claim 1, it is characterised in that：The wax is closed including macromolecule
One or more into wax, low molecule synthetic wax, non-synthetic one-component wax；The pigment includes soluble dyes, non-solvable
One or more in property pigment, inorganic pigment, organic pigment, natural pigment, synthetic dyestuff.
3. a kind of production technology of candle pigment according to claim 1, it is characterised in that：The wax include polyethylene,
It is polypropylene, high density polyethylene (HDPE), low density polyethylene (LDPE), LLDPE, polyvinyl chloride, General Purpose Polystyrenre, poly-
Styrenic foams, impact resistant polystyrene, styrene-acrylonitrile copolymer, acrylonitrile-butadiene-styrene copolymerisation
Co-polymer, polyethylene terephthalate, the poly terephthalic acid of thing, polymethacrylates, ethene-vinyl acetate
Butyl ester, polyamide, poly- carbonic acid resin, polyoxymethylene resin, polyphenylene oxide, polyphenylene sulfide, polyurethane, polystyrene
One or more in macromolecule or low molecule synthetic wax, non-synthetic one-component wax.
4. a kind of production technology of candle pigment according to claim 1, it is characterised in that：The thermoplastic elastomer (TPE) bag
Olefin-containing analog thermoplastic elastomer, diene analog thermoplastic elastomer, polyvinyl chloride-base thermoplastic elastomer, styrene analog thermoplastic bullet
One or more in property body, polyurethane-type thermoplastic elastomer.
5. a kind of production technology of candle pigment according to claim 1, it is characterised in that：The pigment includes pigment
Huang, orange pigment, paratonere, pigment violet, alizarol saphirol, naphthol green, pigment brown, pigment black, Pigment white, extraordinary fluorescent material synthesis
One or more in pigment, mixing secondary color synthetic dyestuff.
6. a kind of production technology of candle pigment according to claim 1-5 any one, it is characterised in that：Step b's
1-5 parts of plasticiser is added in mixture, extruder is put into after being well mixed；The plasticiser includes ditridecyl phthalate, neighbour
Dioctyl phthalate, di-n-octyl phthalate, BBP(Butyl Benzyl Phthalate, di-sec-octyl phthalate, adjacent benzene two
Formic acid dicyclohexyl maleate, dibutyl phthalate, diisobutyl phthalate, repefral, phthalic acid
One or more in diethylester, diisononyl phthalate, diisooctyl phthalate.
7. a kind of production technology of candle pigment according to claim 1-5 any one, it is characterised in that：Step a is also
Including mixture at least to be stood to 12 hours；Also include step:
E. step d wax stone chip is put into extruder, second of wax stone is extruded at 90 DEG C -130 DEG C；By second of wax
Block input grinder grinds to form chip, and second of wax stone chip is put into extruder, the 3rd is extruded at 90 DEG C -130 DEG C
Secondary wax stone；Third time wax stone input grinder is ground to form into chip.
8. a kind of production technology of candle pigment according to claim 6, it is characterised in that：Step a also includes will mixing
Thing at least stands 12 hours；Also include step：
E. wax stone chip is put into extruder, wax stone is extruded at 90 DEG C -130 DEG C, wax stone input grinder is ground to form
Chip；
F. repeat step e at least 1 time or until wax stone chip color is uniform.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610161382.5A CN105802740B (en) | 2016-03-22 | 2016-03-22 | A kind of candle pigment and its production technology |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610161382.5A CN105802740B (en) | 2016-03-22 | 2016-03-22 | A kind of candle pigment and its production technology |
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| Publication Number | Publication Date |
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| CN105802740A CN105802740A (en) | 2016-07-27 |
| CN105802740B true CN105802740B (en) | 2017-08-08 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106317564B (en) * | 2016-08-23 | 2019-01-11 | 福建索邦化工有限公司 | Candle pigment and its production technology |
| US11186794B1 (en) * | 2019-03-04 | 2021-11-30 | United States Of America As Represented By The Administrator Of Nasa | Hybrid fuel grain and method for making same |
| CN111961534A (en) * | 2020-08-04 | 2020-11-20 | 福建索邦化工有限公司 | Special fluorescent pigment for candle and production process thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1384178A (en) * | 2001-04-30 | 2002-12-11 | 上海捷发国际贸易有限公司 | Transparent candle and its formula and production process |
| CN1441041A (en) * | 2002-02-27 | 2003-09-10 | 比欧化学有限公司 | Transparent inflammable capable being stored stably |
| US7220288B2 (en) * | 2002-08-13 | 2007-05-22 | Belmay, Inc. | Protection of fragrance in a wax candle using an antioxidant |
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