CN105801204A - Method for co-producing liquid seaweed fertilizer by utilizing seaweed extract - Google Patents
Method for co-producing liquid seaweed fertilizer by utilizing seaweed extract Download PDFInfo
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- CN105801204A CN105801204A CN201610105959.0A CN201610105959A CN105801204A CN 105801204 A CN105801204 A CN 105801204A CN 201610105959 A CN201610105959 A CN 201610105959A CN 105801204 A CN105801204 A CN 105801204A
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- Prior art keywords
- seaweed
- polyoxyethylene
- extracted liquor
- fatty alcohol
- polyoxyethylene ether
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F11/00—Other organic fertilisers
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
Abstract
The invention relates to a method for co-producing a liquid seaweed fertilizer by utilizing a seaweed extract. The method comprises the following steps: washing fresh or dried seaweeds, adding the fresh or dried seaweeds to a reaction kettle containing a mixture of a certain mass of water and organic solvents according to a certain mass ratio, stirring the materials at a high speed for pulping (the dried seaweeds need to be soaked to swell and then are pulped), adding a certain mass of wetting and penetrating agents after pulping, soaking and extracting, recovering part of the organic solvents through low temperature and low pressure distillation after soaking at a certain temperature for a period of time, finally obtaining seaweed residues and the seaweed extract through filter pressing, mixing the seaweed extract with macroelement fertilizers and stirring the materials until the macroelement fertilizers are completely dissolved, thus obtaining the product. The method has the beneficial technical effects that combining the fertilizers with active ingredients of the seaweeds, the product has obvious effects on improvement of the stress resistance and disease resistance of crops; and besides, being fully water-soluble, the product can meet the requirements of modern agriculture.
Description
Technical field
The present invention relates to a kind of production method utilizing seaweed extracted liquor coproduction liquid seaweed manure.
Background technology
It is still strong acid, highly basic high temperature and high pressure extraction that the Sargassum liquid main flow extracting method of alga fertilizer is prepared by China, and this extracting mode not only breaks up the effective ingredient in Sargassum, and produces low with safety in utilization.The method utilizing microorganism enzymolysis and extraction also achieves some progress, but owing to enzymolysis time is long, causes that extraction efficiency is too low, it is impossible to meet the market demand.Currently also have method strong acid, highly basic high temperature and high pressure extraction combined with enzymolysis, although saved extraction time, but in strong acid, highly basic high temperature and high pressure extraction process still can to a certain extent to Sargassum in effective ingredient damage.
Summary of the invention
The technical problem to be solved is to provide a kind of production method utilizing seaweed extracted liquor coproduction liquid seaweed manure.It is short that seaweed extracted liquor in the method production process has extracting cycle, the advantage that efficiency is high, and extract in process and will not effective ingredient in Sargassum be damaged.
In order to solve above-mentioned technical problem, the present invention by the following technical solutions:
A kind of production method utilizing seaweed extracted liquor coproduction liquid seaweed manure, it is characterised in that carry out according to following steps:
1), fresh Sargassum is cleaned standby, or dry seaweed be dipped to fresh Sargassum moisture consistent state and clean standby, the alternate products that this step obtains is called A product;
2), water, organic solvent and product A are added separately in reactor, pull an oar in the lump;
3), beaten and added wetting and penetrating agent after slurry, soaked 12~72 hours at 20~45 DEG C;
4), low-temp low-pressure Distillation recovery part organic solvent: vapo(u)rizing temperature is 45~65 DEG C, and distillation pressure is-0.5~-1.2Mpa;
5), filter pressing obtain Sargassum slag and filtrate, described filtrate is seaweed extracted liquor;
6), being mixed with macroelement fertilizer by described seaweed extracted liquor, stirring and dissolving obtains liquid seaweed manure completely;
Wherein the mass ratio of A product, water, organic solvent and wetting and penetrating agent is 5~30:10~85:10~85:0.01~0.1;The mass ratio of seaweed extracted liquor and a great number of elements is 50~99:1~50.
Described organic solvent is the two or more of a kind of or arbitrary proportion in ethanol, ether, methanol and ethyl acetate.
Described wetting and penetrating agent is dodecylbenzene sodium sulfonate, sodium lauryl sulphate, alkylphenol polyoxyethylene, sorbitan fatty acid ester-20, sorbitan fatty acid ester-30, sorbitan fatty acid ester-80, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, polyoxyethylene 20 sorbitan monolaurate-60, polyoxyethylene 20 sorbitan monolaurate-80, fatty alcohol-polyoxyethylene ether-3, fatty alcohol-polyoxyethylene ether-4, fatty alcohol-polyoxyethylene ether-5, fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-15, fatty alcohol-polyoxyethylene ether-20, a kind of or arbitrary proportion in fatty alcohol-polyoxyethylene ether-23 and dimethyl-silicon wet goods two or more.
Described macroelement fertilizer is the two or more of a kind of or arbitrary proportion in carbamide, ammonium sulfate, PHOSPHORIC ACID TECH.GRADE potassium dihydrogen, PHOSPHORIC ACID TECH.GRADE ammonium dihydrogen, potassium sulfate, potassium chloride and potassium nitrate.
Described Sargassum refers to: a kind of or arbitrary proportion in Thallus Laminariae (Thallus Eckloniae), Thallus Porphyrae, Thallus Laminariae (Thallus Eckloniae), opotism and Entermorpha two or more.
In step 5), pressure filter selects filter cloth aperture to be 800~4500 orders.
The present invention has following Advantageous Effects:
1, in the present invention, Sargassum liquid adopts low temperature, Low Voltage Pure physics to extract, it is ensured that Sargassum effective ingredient is not destroyed.
2, seaweeds appearance has the protecting film of one layer of thickness; prevent external substance from invading; so simple water or organic solvent extract at normal temperatures and pressures can be very slow; the present invention adds wetting and penetrating agent can make the contact area of water and organic solvent and Sargassum increase; rapid solution breaks through described protecting film at normal temperatures and pressures; thus reaching the purpose of rapid extraction, therefore it is more convenient for the application of heavy industrialization.
3, the present invention adopts the extracting method that water and organic solvent combine, and reduces cost than simple organic solvent extraction.
4, the present invention adopts the extracting method that water and organic solvent combine, and adds the compatibility of product, meets the requirement of modern agriculture (water droplet filling).Because such as simple organic solvent extraction, it is possible to extract can not be dissolved completely in water, and product compatibility is poor, it is impossible to meets agricultural modernization (water droplet filling) requirement.
5, fertilizer effective ingredient in Sargassum is combined by the present invention, can significantly improve that crop is degeneration-resistant, disease resistance.
6, the present invention is entirely water-soluble meets modern agriculture demand.
Detailed description of the invention
The present invention is further illustrated below in conjunction with instantiation.
Embodiment 1
Fresh Entermorpha after cleaning is joined in the reactor filling water and ethanol and pulls an oar, the sorbitan fatty acid ester-20 as wetting and penetrating agent and alkylphenol polyoxyethylene is added after making beating, fresh Entermorpha, water, ethanol, alkylphenol polyoxyethylene and sorbitan fatty acid ester-20 are 20:15:64.96:0.02:0.02 according to mass ratio, soak 72 hours at 20 DEG C, in negative pressure 0.5Mpa, Distillation recovery part organic solvent under temperature 45 C, pressure filter adopts 1000 order filter clothes to carry out filter pressing, gained filtrate mixes according to mass ratio 90:10 with carbamide, it is product of the present invention after stirring and dissolving is entirely complete.
Embodiment 2
nullBy clean after dry Thallus Laminariae (Thallus Eckloniae) and dry Entermorpha be made into dry seaweed in proportion,It is dipped to and Fresh Laminaria Japonica moisture consistent state,Join and fill water、In the reactor of ethanol and ether,Pull an oar in the lump,The alkylphenol polyoxyethylene as wetting and penetrating agent and polyoxyethylene 20 sorbitan monolaurate-60 is added after making beating,The dry Thallus Laminariae (Thallus Eckloniae) soaked、Dry Entermorpha、Water、Ethanol、Ether、Mass ratio between alkylphenol polyoxyethylene and polyoxyethylene 20 sorbitan monolaurate-60 is 4:2:25:60.97:8:0.01:0.02,Soak 60 hours at 25 DEG C,In negative pressure 0.7Mpa,Distillation recovery part organic solvent under temperature 50 C,Pressure filter adopts 1200 order filter clothes to carry out filter pressing,Gained filtrate、Carbamide and PHOSPHORIC ACID TECH.GRADE ammonium dihydrogen mix according to mass ratio 84:10:6,It is product of the present invention after stirring and dissolving is entirely complete.
Embodiment 3
nullFresh Laminaria Japonica after cleaning is joined and fills water、Ethanol、The reactor of ethyl acetate and ether is pulled an oar,The dodecylbenzene sodium sulfonate as wetting and penetrating agent is added after making beating、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-60 and dimethicone,Fresh Laminaria Japonica、Water、Ethanol、Ethyl acetate、Ether、Dodecylbenzene sodium sulfonate、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28.96:0.01:0.01:0.01:0.01,Soak 46 hours at 30 DEG C,In negative pressure 1.0Mpa,Distillation recovery part organic solvent at temperature 55 DEG C,Pressure filter adopts 1400 order filter clothes to carry out filter pressing,Gained filtrate、Carbamide and PHOSPHORIC ACID TECH.GRADE potassium dihydrogen mix according to mass ratio 78:15:7,It is product of the present invention after stirring and dissolving is entirely complete.
Embodiment 4
nullBy clean after dry Thallus Laminariae (Thallus Eckloniae)、Dry opotism and dry Entermorpha are made into dry seaweed in proportion,It is dipped to and Fresh Laminaria Japonica moisture consistent state,Join in the reactor filling water and ethanol and pull an oar,The sodium lauryl sulphate as wetting and penetrating agent and sorbitan fatty acid ester-60 is added after making beating,Dry Thallus Laminariae (Thallus Eckloniae) after immersion、Dry opotism、Dry Entermorpha、Water、Ether、Ethyl acetate、Sodium lauryl sulphate and sorbitan fatty acid ester-60 are according to mass ratio 3:3:1:25:25:42.96:0.02:0.02,Soak 24 hours at 35 DEG C,In negative pressure 1.2Mpa,Distillation recovery part organic solvent under temperature 50 C,Pressure filter adopts 2000 order filter clothes to carry out filter pressing,Gained filtrate、Potassium nitrate、PHOSPHORIC ACID TECH.GRADE ammonium dihydrogen and ammonium sulfate mix according to mass ratio 80:10:5:5,It is product of the present invention after stirring and dissolving is entirely complete.
Further illustrate below in conjunction with experimental data and the method have the benefit that
For the sample that Different Extraction Method on market is collected, carrying out the detection of Sargassum polysaccharides after oven drying at low temperature, testing result is table 1 such as.
Table 1
Highly basic extraction method | Highly basic adds enzymatic isolation method | Acidic hydrolysis | The inventive method | |
Sargassum polysaccharides (%) | 30.2 | 36.7 | 42.1 | 44.6 |
Adopt Sargassum polysaccharides content in this method extract the highest as can be seen from Table 1, Sargassum effective ingredient is destroyed minimum.
For common liq Water soluble fertilizer (except being not added with seaweed extracted liquor, other preparation condition and embodiment 1 are identical), the liquid Water soluble fertilizer (except being not added with seaweed extracted liquor, other preparation condition is identical with embodiment 1) of adding certain producer's Sargassum liquid as follows with fertilizer efficiency experimental data under embodiment 1 equal conditions:
1 materials and methods
1.1 experimental field overviews
Testing and carry out at Fushan District, Yantai City self-operation experiment booth, soil is brunisolic soil.Soil nutrient situation is: organic 80.36g/kg, alkali-hydrolyzable nitrogen 76.5mg/kg, available phosphorus 82.3mg/kg, available potassium 78.8mg/kg, pH5.99.
1.2 experiment materials to be tested
Common liq Water soluble fertilizer (except being not added with seaweed extracted liquor, other preparation condition is identical with embodiment 1), the liquid Water soluble fertilizer (except being not added with seaweed extracted liquor, other preparation condition is identical with embodiment 1) adding certain producer's Sargassum liquid and each 4.5kg of embodiment 1;1 mu of intensive shadow on lung booth of same management.
1.3 experimental designs
Experiment is divided into 9 communities, and 3 communities are one group of totally 3 groups of experiment, repeats for 3 times, cross arrangement, divides 3 drip irrigations according to plant growth situation, 0.5kg tri-kinds is tested fertilizer and is dissolved separately in 500kg water, and drip irrigation is one group of experiment in 3 communities respectively, repeats 3 times;Plot area 66m2,, surrounding sets protection row, north-south, line-spacing 22cm, spacing in the rows 16cm, every community 1875 strain.
1.4 experiments are implemented
Each processing except experiment fertilizer difference, all consistent intensive shadow on lung of other agronomy control measures is plant October in 2015 15 kinds, and first time November 8 in 2015 processes, November 15 in 2015, second time processed, November 25 in 2015, third time processed, and within 2015, December 10 is gathered in the crops, and added up yield.
2 results and analysis
The impact on intensive shadow on lung character of 2.1 different disposal
Owing to intensive shadow on lung trophophase is short, fertilizer requirement is not as big, and trophophase does not with the naked eye observe 3 kinds of significant differences tested.Temperature reduced suddenly and snowed field November 24 in 2015, owing to not preventing in advance, intensive shadow on lung occurrence of large-area cold injury, though November 25 supplements fertilizer in time and rescues, within 1st, cold injury quantity is added up in December after rescuing a week, 3 communities totally 1501 strains of drip irrigation common liq Water soluble fertilizer will be obvious that cold injury, drip irrigation is added 3 communities totally 1212 strains of the liquid Water soluble fertilizer of certain producer's Sargassum liquid and be will be obvious that cold injury, 3 communities totally 982 strains of drip irrigation embodiment 1 will be obvious that cold injury, the resistance improving crop is had obvious effect by alga fertilizer as can be seen from the data, product effect of the present invention is especially prominent.
The impact on intensive shadow on lung yield of 2.2 different disposal
Table 2
As can be seen from Table 2, the intensive shadow on lung yield of drip irrigation product of the present invention significantly improves.
3 discuss
Test the product just for the different manufacturers Different Extraction Method can bought on market, and it has been Sargassum polysaccharides detection and contrast experiment, being not necessarily of being commercially available is best, and notebook data can only illustrate most like products that product of the present invention is better than on market to have bought;Containing abundant active substance in Sargassum, how being maximally utilized by these active substances is the R&D direction in our future.
Claims (6)
1. the production method utilizing seaweed extracted liquor coproduction liquid seaweed manure, it is characterised in that carry out according to following steps:
1), fresh Sargassum is cleaned standby, or dry seaweed be dipped to fresh Sargassum moisture consistent state and clean standby, the alternate products that this step obtains is called A product;
2), water, organic solvent and product A are added separately in reactor, pull an oar in the lump;
3), beaten and added wetting and penetrating agent after slurry, soaked 12~72 hours at 20~45 DEG C;
4), low-temp low-pressure Distillation recovery part organic solvent: vapo(u)rizing temperature is 45~65 DEG C, and distillation pressure is-0.5~-1.2Mpa;
5), filter pressing obtain Sargassum slag and filtrate, described filtrate is seaweed extracted liquor;
6), being mixed with macroelement fertilizer by described seaweed extracted liquor, stirring and dissolving obtains liquid seaweed manure completely;
Wherein the mass ratio of A product, water, organic solvent and wetting and penetrating agent is 5~30:10~85:10~85:0.01~0.1;The mass ratio of seaweed extracted liquor and a great number of elements is 50~99:1~50.
2. a kind of production method utilizing seaweed extracted liquor coproduction liquid seaweed manure as claimed in claim 1, it is characterised in that: described organic solvent is the two or more of a kind of or arbitrary proportion in ethanol, ether, methanol and ethyl acetate.
null3. a kind of production method utilizing seaweed extracted liquor coproduction liquid seaweed manure as claimed in claim 1,It is characterized in that: described wetting and penetrating agent is dodecylbenzene sodium sulfonate、Sodium lauryl sulphate、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-20、Sorbitan fatty acid ester-30、Sorbitan fatty acid ester-80、Polyoxyethylene 20 sorbitan monolaurate-20、Polyoxyethylene 20 sorbitan monolaurate-40、Polyoxyethylene 20 sorbitan monolaurate-60、Polyoxyethylene 20 sorbitan monolaurate-80、Fatty alcohol-polyoxyethylene ether-3、Fatty alcohol-polyoxyethylene ether-4、Fatty alcohol-polyoxyethylene ether-5、Fatty alcohol-polyoxyethylene ether-7、Fatty alcohol-polyoxyethylene ether-9、Fatty alcohol-polyoxyethylene ether-15、Fatty alcohol-polyoxyethylene ether-20、A kind of or arbitrary proportion in fatty alcohol-polyoxyethylene ether-23 and dimethyl-silicon wet goods two or more.
4. a kind of production method utilizing seaweed extracted liquor coproduction liquid seaweed manure as claimed in claim 1, it is characterised in that: described macroelement fertilizer is the two or more of a kind of or arbitrary proportion in carbamide, ammonium sulfate, PHOSPHORIC ACID TECH.GRADE potassium dihydrogen, PHOSPHORIC ACID TECH.GRADE ammonium dihydrogen, potassium sulfate, potassium chloride and potassium nitrate.
5. a kind of production method utilizing seaweed extracted liquor coproduction liquid seaweed manure as claimed in claim 1, it is characterised in that: described Sargassum refers to: a kind of or arbitrary proportion in Thallus Laminariae (Thallus Eckloniae), Thallus Porphyrae, Thallus Laminariae (Thallus Eckloniae), opotism and Entermorpha two or more.
6. a kind of production method utilizing seaweed extracted liquor coproduction liquid seaweed manure as claimed in claim 1, it is characterised in that: in step 5), pressure filter selects filter cloth aperture to be 800~4500 orders.
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Cited By (2)
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CN106854112A (en) * | 2016-12-24 | 2017-06-16 | 贵州大学 | A kind of production method of the liquid seaweed manure for being exclusively used in rhizoma Gastrodiae |
CN114605194A (en) * | 2022-03-29 | 2022-06-10 | 河北德沃多肥料有限公司 | Novel plant nutrient solution |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106854112A (en) * | 2016-12-24 | 2017-06-16 | 贵州大学 | A kind of production method of the liquid seaweed manure for being exclusively used in rhizoma Gastrodiae |
CN114605194A (en) * | 2022-03-29 | 2022-06-10 | 河北德沃多肥料有限公司 | Novel plant nutrient solution |
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