A kind of Oleum Arachidis hypogaeae semen discoloration method
Technical field
The invention belongs to technical field of solar, be specifically related to a kind of Oleum Arachidis hypogaeae semen discoloration method.
Background technology
Plasticiser also known as plasticizer, is the common environmental hormone compounds of a class, has in recent years become one of global pollutant the most general.For avoiding it to endanger, " priority pollutants list " is all listed in by China, the U.S., Japan and European Union etc., and its addition in food contact material is defined.Have now been found that what exist in Vegetable oil lipoprotein has dimethyl phthalate (DMP), diethyl phthalate (DEP), dibutyl phthalate (DBP), diisobutyl phthalate (DIBP), butyl benzyl phthalate (BBP) and phthalic acid two (2-ethyl) own ester (DEHP) etc..Root is according to research reports, adopt the solid absorbent can PAEs in partial removal drinking water or sewage, such as adopting activated carbon-attapulgite composite filtering material to be removed by the DBP of 94% in drinking water, DMP, DEP and DEHP in water are also had certain elimination effect by solid absorbent.But, the adsorbing and removing research of the PAEs for existing in edible vegetable oil but has no report.
Summary of the invention
It is an object of the invention to provide a kind of Oleum Arachidis hypogaeae semen discoloration method, present invention improves the problem that existing Oleum Arachidis hypogaeae semen decoloration process treatment effect is poor.
A kind of Oleum Arachidis hypogaeae semen discoloration method, its step is as follows:
(1) contaminant filter: pour Oleum Arachidis hypogaeae semen into defecator, obtains the Oleum Arachidis hypogaeae semen without granule foreign;
(2) first time decolouring: joined by Oleum Arachidis hypogaeae semen in bleaching tower, adds decolorising agent, adopts the mode of ultrasonic agitation to decolour after mix homogeneously;
(3) second time decolouring: add mixing decolorising agent, mix homogeneously;
(4) Oleum Arachidis hypogaeae semen after decolouring is joined filtration in leaf filter.
Defecator in described step (1) adopts metal mesh filter to filter with foaming body and combines, and the aperture of described wire netting is 1mm, and the porosity of described foaming body is not more than 20ppi.
Decolouring alr mode in described step (2) refers to and arranges agitating device bottom bleaching tower, and upper end, bleaching tower center arranges Vltrasonic device.
Decolorising agent in described step (2) adopts the one in active hargil, attapulgite, JNC01 activated carbon, H-1 activated carbon, H-2 activated carbon, YS-900 activated carbon, JTF-F activated carbon, 55F-A activated carbon, 55JN-C activated carbon, Norit8014-2 activated carbon, and the addition of described decolorising agent is the 2-3% of oil weight.
In described step (2), bleaching temperature is 55-75 DEG C, and bleaching time is 15-35min, and decolouring pressure is 0.08-0.1MPa.
Mixing decolorising agent in described step (3) adopts active hargil and attapulgite to mix, described active hargil 20-40%, attapulgite 60-80%.
In described step (3), bleaching temperature is 50-60 DEG C, and bleaching time is 10-20min, and decolouring pressure is 0.08-0.1MPa.
Compared with prior art, the method have the advantages that
Oleum Arachidis hypogaeae semen decoloration process provided by the invention has good treatment effect, can effectively reduce pigmentation, improve the product color of Oleum Arachidis hypogaeae semen, and the harmful substance contained in Oleum Arachidis hypogaeae semen also is able to by good absorption so that the Oleum Arachidis hypogaeae semen after decolouring meets the requirement of high-grade product.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further:
Embodiment 1
A kind of Oleum Arachidis hypogaeae semen discoloration method, its step is as follows:
(1) contaminant filter: pour Oleum Arachidis hypogaeae semen into defecator, obtains the Oleum Arachidis hypogaeae semen without granule foreign;
(2) first time decolouring: joined by Oleum Arachidis hypogaeae semen in bleaching tower, adds decolorising agent, adopts the mode of ultrasonic agitation to decolour after mix homogeneously;
(3) second time decolouring: add mixing decolorising agent, mix homogeneously;
(4) Oleum Arachidis hypogaeae semen after decolouring is joined filtration in leaf filter.
Defecator in described step (1) adopts metal mesh filter to filter with foaming body and combines, and the aperture of described wire netting is 1mm, the porosity 10ppi of described foaming body.
Decolouring alr mode in described step (2) refers to and arranges agitating device bottom bleaching tower, and upper end, bleaching tower center arranges Vltrasonic device.
Decolorising agent in described step (2) adopts 55JN-C activated carbon, and the addition of described decolorising agent is the 2% of oil weight.
In described step (2), bleaching temperature is 55 DEG C, and bleaching time is 15min, and decolouring pressure is 0.08MPa.
Mixing decolorising agent in described step (3) adopts active hargil and attapulgite to mix, described active hargil 20%, attapulgite 80%.
In described step (3), bleaching temperature is 50 DEG C, and bleaching time is 10min, and decolouring pressure is 0.08MPa.
Embodiment 2
A kind of Oleum Arachidis hypogaeae semen discoloration method, its step is as follows:
(1) contaminant filter: pour Oleum Arachidis hypogaeae semen into defecator, obtains the Oleum Arachidis hypogaeae semen without granule foreign;
(2) first time decolouring: joined by Oleum Arachidis hypogaeae semen in bleaching tower, adds decolorising agent, adopts the mode of ultrasonic agitation to decolour after mix homogeneously;
(3) second time decolouring: add mixing decolorising agent, mix homogeneously;
(4) Oleum Arachidis hypogaeae semen after decolouring is joined filtration in leaf filter.
Defecator in described step (1) adopts metal mesh filter to filter with foaming body and combines, and the aperture of described wire netting is 1mm, the porosity 20ppi of described foaming body.
Decolouring alr mode in described step (2) refers to and arranges agitating device bottom bleaching tower, and upper end, bleaching tower center arranges Vltrasonic device.
Decolorising agent in described step (2) adopts active hargil, and the addition of described decolorising agent is the 2-3% of oil weight.
In described step (2), bleaching temperature is 75 DEG C, and bleaching time is 35min, and decolouring pressure is 0.1MPa.
Mixing decolorising agent in described step (3) adopts active hargil and attapulgite to mix, described active hargil 40%, attapulgite 60%.
In described step (3), bleaching temperature is 60 DEG C, and bleaching time is 20min, and decolouring pressure is 0.1MPa.
Embodiment 3
A kind of Oleum Arachidis hypogaeae semen discoloration method, its step is as follows:
(1) contaminant filter: pour Oleum Arachidis hypogaeae semen into defecator, obtains the Oleum Arachidis hypogaeae semen without granule foreign;
(2) first time decolouring: joined by Oleum Arachidis hypogaeae semen in bleaching tower, adds decolorising agent, adopts the mode of ultrasonic agitation to decolour after mix homogeneously;
(3) second time decolouring: add mixing decolorising agent, mix homogeneously;
(4) Oleum Arachidis hypogaeae semen after decolouring is joined filtration in leaf filter.
Defecator in described step (1) adopts metal mesh filter to filter with foaming body and combines, and the aperture of described wire netting is 1mm, the porosity 15ppi of described foaming body.
Decolouring alr mode in described step (2) refers to and arranges agitating device bottom bleaching tower, and upper end, bleaching tower center arranges Vltrasonic device.
Decolorising agent in described step (2) adopts H-1 activated carbon, and the addition of described decolorising agent is the 2-3% of oil weight.
In described step (2), bleaching temperature is 65 DEG C, and bleaching time is 25min, and decolouring pressure is 0.09MPa.
Mixing decolorising agent in described step (3) adopts active hargil and attapulgite to mix, described active hargil 30%, attapulgite 70%.
In described step (3), bleaching temperature is 55 DEG C, and bleaching time is 15min, and decolouring pressure is 0.09MPa.
The foregoing is only one embodiment of the invention, be not limiting as the present invention, all employings are equal to the technical scheme that the mode of replacement or equivalent transformation obtains, and all fall within protection scope of the present invention.