CN105779118A - Peanut oil decoloring method - Google Patents

Peanut oil decoloring method Download PDF

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Publication number
CN105779118A
CN105779118A CN201610203409.2A CN201610203409A CN105779118A CN 105779118 A CN105779118 A CN 105779118A CN 201610203409 A CN201610203409 A CN 201610203409A CN 105779118 A CN105779118 A CN 105779118A
Authority
CN
China
Prior art keywords
arachidis hypogaeae
oleum arachidis
hypogaeae semen
activated carbon
decolouring
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610203409.2A
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Chinese (zh)
Inventor
刘必衍
曾惜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CHONGQING BEYOND OCEAN CARBON MANUFACTURE Co Ltd
Original Assignee
CHONGQING BEYOND OCEAN CARBON MANUFACTURE Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CHONGQING BEYOND OCEAN CARBON MANUFACTURE Co Ltd filed Critical CHONGQING BEYOND OCEAN CARBON MANUFACTURE Co Ltd
Priority to CN201610203409.2A priority Critical patent/CN105779118A/en
Publication of CN105779118A publication Critical patent/CN105779118A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/001Refining fats or fatty oils by a combination of two or more of the means hereafter
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A23D9/04Working-up
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/008Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/10Refining fats or fatty oils by adsorption

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention provides a peanut oil decoloring method. The method comprises the following steps: filtering out impurities, namely, pouring the peanut oil in a filter device to obtain the peanut oil without particle impurity; (2) primarily decoloring: adding the peanut oil in a decoloring tower, adding a decoloring agent, uniformly mixing, and ultrasonically stirring to decolor; (3) secondarily decoloring: adding the mixed decoloring agent, and uniformly mixing; and (4) adding the decolored peanut oil in an impeller type filtering machine to filter. Through the adoption of the method provided by the invention, the problem that the existing peanut oil decoloring process treatment effect is bad is improved.

Description

A kind of Oleum Arachidis hypogaeae semen discoloration method
Technical field
The invention belongs to technical field of solar, be specifically related to a kind of Oleum Arachidis hypogaeae semen discoloration method.
Background technology
Plasticiser also known as plasticizer, is the common environmental hormone compounds of a class, has in recent years become one of global pollutant the most general.For avoiding it to endanger, " priority pollutants list " is all listed in by China, the U.S., Japan and European Union etc., and its addition in food contact material is defined.Have now been found that what exist in Vegetable oil lipoprotein has dimethyl phthalate (DMP), diethyl phthalate (DEP), dibutyl phthalate (DBP), diisobutyl phthalate (DIBP), butyl benzyl phthalate (BBP) and phthalic acid two (2-ethyl) own ester (DEHP) etc..Root is according to research reports, adopt the solid absorbent can PAEs in partial removal drinking water or sewage, such as adopting activated carbon-attapulgite composite filtering material to be removed by the DBP of 94% in drinking water, DMP, DEP and DEHP in water are also had certain elimination effect by solid absorbent.But, the adsorbing and removing research of the PAEs for existing in edible vegetable oil but has no report.
Summary of the invention
It is an object of the invention to provide a kind of Oleum Arachidis hypogaeae semen discoloration method, present invention improves the problem that existing Oleum Arachidis hypogaeae semen decoloration process treatment effect is poor.
A kind of Oleum Arachidis hypogaeae semen discoloration method, its step is as follows:
(1) contaminant filter: pour Oleum Arachidis hypogaeae semen into defecator, obtains the Oleum Arachidis hypogaeae semen without granule foreign;
(2) first time decolouring: joined by Oleum Arachidis hypogaeae semen in bleaching tower, adds decolorising agent, adopts the mode of ultrasonic agitation to decolour after mix homogeneously;
(3) second time decolouring: add mixing decolorising agent, mix homogeneously;
(4) Oleum Arachidis hypogaeae semen after decolouring is joined filtration in leaf filter.
Defecator in described step (1) adopts metal mesh filter to filter with foaming body and combines, and the aperture of described wire netting is 1mm, and the porosity of described foaming body is not more than 20ppi.
Decolouring alr mode in described step (2) refers to and arranges agitating device bottom bleaching tower, and upper end, bleaching tower center arranges Vltrasonic device.
Decolorising agent in described step (2) adopts the one in active hargil, attapulgite, JNC01 activated carbon, H-1 activated carbon, H-2 activated carbon, YS-900 activated carbon, JTF-F activated carbon, 55F-A activated carbon, 55JN-C activated carbon, Norit8014-2 activated carbon, and the addition of described decolorising agent is the 2-3% of oil weight.
In described step (2), bleaching temperature is 55-75 DEG C, and bleaching time is 15-35min, and decolouring pressure is 0.08-0.1MPa.
Mixing decolorising agent in described step (3) adopts active hargil and attapulgite to mix, described active hargil 20-40%, attapulgite 60-80%.
In described step (3), bleaching temperature is 50-60 DEG C, and bleaching time is 10-20min, and decolouring pressure is 0.08-0.1MPa.
Compared with prior art, the method have the advantages that
Oleum Arachidis hypogaeae semen decoloration process provided by the invention has good treatment effect, can effectively reduce pigmentation, improve the product color of Oleum Arachidis hypogaeae semen, and the harmful substance contained in Oleum Arachidis hypogaeae semen also is able to by good absorption so that the Oleum Arachidis hypogaeae semen after decolouring meets the requirement of high-grade product.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further:
Embodiment 1
A kind of Oleum Arachidis hypogaeae semen discoloration method, its step is as follows:
(1) contaminant filter: pour Oleum Arachidis hypogaeae semen into defecator, obtains the Oleum Arachidis hypogaeae semen without granule foreign;
(2) first time decolouring: joined by Oleum Arachidis hypogaeae semen in bleaching tower, adds decolorising agent, adopts the mode of ultrasonic agitation to decolour after mix homogeneously;
(3) second time decolouring: add mixing decolorising agent, mix homogeneously;
(4) Oleum Arachidis hypogaeae semen after decolouring is joined filtration in leaf filter.
Defecator in described step (1) adopts metal mesh filter to filter with foaming body and combines, and the aperture of described wire netting is 1mm, the porosity 10ppi of described foaming body.
Decolouring alr mode in described step (2) refers to and arranges agitating device bottom bleaching tower, and upper end, bleaching tower center arranges Vltrasonic device.
Decolorising agent in described step (2) adopts 55JN-C activated carbon, and the addition of described decolorising agent is the 2% of oil weight.
In described step (2), bleaching temperature is 55 DEG C, and bleaching time is 15min, and decolouring pressure is 0.08MPa.
Mixing decolorising agent in described step (3) adopts active hargil and attapulgite to mix, described active hargil 20%, attapulgite 80%.
In described step (3), bleaching temperature is 50 DEG C, and bleaching time is 10min, and decolouring pressure is 0.08MPa.
Embodiment 2
A kind of Oleum Arachidis hypogaeae semen discoloration method, its step is as follows:
(1) contaminant filter: pour Oleum Arachidis hypogaeae semen into defecator, obtains the Oleum Arachidis hypogaeae semen without granule foreign;
(2) first time decolouring: joined by Oleum Arachidis hypogaeae semen in bleaching tower, adds decolorising agent, adopts the mode of ultrasonic agitation to decolour after mix homogeneously;
(3) second time decolouring: add mixing decolorising agent, mix homogeneously;
(4) Oleum Arachidis hypogaeae semen after decolouring is joined filtration in leaf filter.
Defecator in described step (1) adopts metal mesh filter to filter with foaming body and combines, and the aperture of described wire netting is 1mm, the porosity 20ppi of described foaming body.
Decolouring alr mode in described step (2) refers to and arranges agitating device bottom bleaching tower, and upper end, bleaching tower center arranges Vltrasonic device.
Decolorising agent in described step (2) adopts active hargil, and the addition of described decolorising agent is the 2-3% of oil weight.
In described step (2), bleaching temperature is 75 DEG C, and bleaching time is 35min, and decolouring pressure is 0.1MPa.
Mixing decolorising agent in described step (3) adopts active hargil and attapulgite to mix, described active hargil 40%, attapulgite 60%.
In described step (3), bleaching temperature is 60 DEG C, and bleaching time is 20min, and decolouring pressure is 0.1MPa.
Embodiment 3
A kind of Oleum Arachidis hypogaeae semen discoloration method, its step is as follows:
(1) contaminant filter: pour Oleum Arachidis hypogaeae semen into defecator, obtains the Oleum Arachidis hypogaeae semen without granule foreign;
(2) first time decolouring: joined by Oleum Arachidis hypogaeae semen in bleaching tower, adds decolorising agent, adopts the mode of ultrasonic agitation to decolour after mix homogeneously;
(3) second time decolouring: add mixing decolorising agent, mix homogeneously;
(4) Oleum Arachidis hypogaeae semen after decolouring is joined filtration in leaf filter.
Defecator in described step (1) adopts metal mesh filter to filter with foaming body and combines, and the aperture of described wire netting is 1mm, the porosity 15ppi of described foaming body.
Decolouring alr mode in described step (2) refers to and arranges agitating device bottom bleaching tower, and upper end, bleaching tower center arranges Vltrasonic device.
Decolorising agent in described step (2) adopts H-1 activated carbon, and the addition of described decolorising agent is the 2-3% of oil weight.
In described step (2), bleaching temperature is 65 DEG C, and bleaching time is 25min, and decolouring pressure is 0.09MPa.
Mixing decolorising agent in described step (3) adopts active hargil and attapulgite to mix, described active hargil 30%, attapulgite 70%.
In described step (3), bleaching temperature is 55 DEG C, and bleaching time is 15min, and decolouring pressure is 0.09MPa.
The foregoing is only one embodiment of the invention, be not limiting as the present invention, all employings are equal to the technical scheme that the mode of replacement or equivalent transformation obtains, and all fall within protection scope of the present invention.

Claims (7)

1. an Oleum Arachidis hypogaeae semen discoloration method, its step is as follows:
(1) contaminant filter: pour Oleum Arachidis hypogaeae semen into defecator, obtains the Oleum Arachidis hypogaeae semen without granule foreign;
(2) first time decolouring: joined by Oleum Arachidis hypogaeae semen in bleaching tower, adds decolorising agent, adopts the mode of ultrasonic agitation to decolour after mix homogeneously;
(3) second time decolouring: add mixing decolorising agent, mix homogeneously;
(4) Oleum Arachidis hypogaeae semen after decolouring is joined filtration in leaf filter.
2. a kind of Oleum Arachidis hypogaeae semen discoloration method according to claims 1, it is characterized in that, defecator in described step (1) adopts metal mesh filter to filter with foaming body and combines, and the aperture of described wire netting is 1mm, and the porosity of described foaming body is not more than 20ppi.
3. a kind of Oleum Arachidis hypogaeae semen discoloration method according to claims 1, it is characterised in that the decolouring alr mode in described step (2) refers to and arranges agitating device bottom bleaching tower, and upper end, bleaching tower center arranges Vltrasonic device.
4. a kind of Oleum Arachidis hypogaeae semen discoloration method according to claims 1, it is characterized in that, decolorising agent in described step (2) adopts the one in active hargil, attapulgite, JNC01 activated carbon, H-1 activated carbon, H-2 activated carbon, YS-900 activated carbon, JTF-F activated carbon, 55F-A activated carbon, 55JN-C activated carbon, Norit8014-2 activated carbon, and the addition of described decolorising agent is the 2-3% of oil weight.
5. a kind of Oleum Arachidis hypogaeae semen discoloration method according to claims 1, it is characterised in that in described step (2), bleaching temperature is 55-75 DEG C, and bleaching time is 15-35min, and decolouring pressure is 0.08-0.1MPa.
6. a kind of Oleum Arachidis hypogaeae semen discoloration method according to claims 1, it is characterised in that the mixing decolorising agent in described step (3) adopts active hargil and attapulgite to mix, described active hargil 20-40%, attapulgite 60-80%.
7. a kind of Oleum Arachidis hypogaeae semen discoloration method according to claims 1, it is characterised in that in described step (3), bleaching temperature is 50-60 DEG C, and bleaching time is 10-20min, and decolouring pressure is 0.08-0.1MPa.
CN201610203409.2A 2016-04-01 2016-04-01 Peanut oil decoloring method Pending CN105779118A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113025424A (en) * 2021-03-18 2021-06-25 吉林省百利生物科技有限公司 Method for removing plasticizer from grease
CN113186032A (en) * 2021-05-31 2021-07-30 江南大学 Method for decoloring peony seed oil

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105038982A (en) * 2015-08-28 2015-11-11 成都市新津迎先粮油有限公司 Rapeseed oil decolouring process
CN105154221A (en) * 2015-07-31 2015-12-16 崇州市白头甘泉工业油脂厂 Efficient grease decoloring method

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105154221A (en) * 2015-07-31 2015-12-16 崇州市白头甘泉工业油脂厂 Efficient grease decoloring method
CN105038982A (en) * 2015-08-28 2015-11-11 成都市新津迎先粮油有限公司 Rapeseed oil decolouring process

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
张明明等: "油脂用邻苯二甲酸酯类塑化剂的吸附脱除研究", 《粮油食品科技》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113025424A (en) * 2021-03-18 2021-06-25 吉林省百利生物科技有限公司 Method for removing plasticizer from grease
CN113025424B (en) * 2021-03-18 2021-12-28 吉林省百利生物科技有限公司 Method for removing plasticizer from grease
CN113186032A (en) * 2021-05-31 2021-07-30 江南大学 Method for decoloring peony seed oil

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Applicant after: Chongqing Fei Yang environmental Polytron Technologies Inc

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Applicant before: Chongqing Beyond Ocean Carbon Manufacture Co., Ltd.

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Applicant after: Chongqing Fei Yang environmental Polytron Technologies Inc

Address before: Summer Baqing 400000 River Street Chongqing city Banan District Jiangjin District

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