CN105778737A - Coating material for stainless steel vacuum bottles and preparation method of coating material for stainless steel vacuum bottles - Google Patents
Coating material for stainless steel vacuum bottles and preparation method of coating material for stainless steel vacuum bottles Download PDFInfo
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- CN105778737A CN105778737A CN201610157851.6A CN201610157851A CN105778737A CN 105778737 A CN105778737 A CN 105778737A CN 201610157851 A CN201610157851 A CN 201610157851A CN 105778737 A CN105778737 A CN 105778737A
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- China
- Prior art keywords
- coating material
- acid
- rustless steel
- thermos flask
- parts
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
- C09D167/08—Polyesters modified with higher fatty oils or their acids, or with natural resins or resin acids
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
Abstract
The invention discloses a coating material for stainless steel vacuum bottles and a preparation method of the coating material for the stainless steel vacuum bottles. The coating material is prepared from, by weight, 40-60 parts of short oil alkyd resin, 1-2 parts of vinyltriamine, 2.5-3.5 parts of plasticizer, 15-25 parts of butyl rubber, 5-15 parts of amino siloxane, 1-1.5 parts of silver nanoparticles, 0.5-2 parts of a coupling agent and 10-30 parts of a solvent. The coating material for the stainless steel vacuum bottles is high in adhesion and excellent in mechanical property and anti-impact performance and has a favorable antibacterial function due to containing of an antibacterial agent.
Description
Technical field:
The present invention relates to a kind of coating material technical field, be specifically related to a kind of rustless steel insulation
Bottle coating material.
Background technology:
Alkyd resin class material occupies the biggest proportion in coatings art, and it has the cost of raw material
The advantages such as low, adhesive force is stronger.Alkyd resin oil content very big on the impact of performance, oil
Spending the least, its vitrification point can be the highest, and the speed of release solvent can be the fastest, and color and
The retentivity of luminosity is the best.But finding in Shi Jian, the alkyd resin of short oil is in the process of use
In easily occur coating scratch phenomenon, this is owing to the volatilization of solvent makes coating uneven drying slowly
One, thus be easily generated coating heterogeneity and easily scratch.
In daily life, rustless steel thermos flask due to its not cracky the most gradually substitute conventional vacuum
Bottle.One layer of protective coating is added outside rustless steel thermos flask, can also corrosion resistant while
Increase aesthetics, expanded service life.Owing to thermos flask in use can often connect with water
Touching, general coating material can bubble after long-term use, and the phenomenon such as come off.Therefore carry
Adhesive force and the resistance to water of high thermos flask coating material are particularly important.
Chinese patent 201010270610.5 discloses a kind of water-borne baking paint and preparation side thereof
Method.By using hydroxyl modified aqueous acrylic acid resin and methyl-etherified amino resins, make this painting
Without without benzene type organic in material, from without health is caused serious harm.But still
Unresolved use coating material poor water resistance in thermos flask, the problem easily scratched.
When utilizing thermos flask to contain food, have food debris and be retained in outside, if the most clear
Washing and be easy to breed bacteria, healthy to people impacts.So in coating material
Adding antibiotic substance is a kind of extraordinary improved means.
Summary of the invention:
It is an object of the invention to provide a kind of coating material for rustless steel thermos flask, its attachment
Power is strong, and life-time service does not haves foaming, and the phenomenon such as come off.Coating material uses oil content shorter
Alkyd resin, thus improve the color of coating material and the holding performance of luminosity, solvent uses
Easy volatile solvent, can all volatilize after overbaking, can improve the homogeneity of coating, also will not
Human body is damaged.With the addition of antibacterial simultaneously, make the more safety and sanitation of this coating material.
It is a further object to provide the preparation method of this coating material.
The rustless steel thermos flask coating material of the present invention, by weight, this coating material by
Following components forms:
Short oil-ity alcohol acid resin 40-60 part vinyl triamine 1-2 part
Plasticizer 2.5-3.5 part butyl rubber 15-25 part
Amino silicone 5-15 part nano silver particles 1-1.5 part
Coupling agent 0.5-2 part solvent 10-30 part
Wherein said short oil-ity alcohol acid resin is that vegetable oil acid, binary acid and polyhydric alcohol are by esterification
Effect polycondensation forms.
Preferred as technique scheme, described oil content is 35%-36%
Preferred as technique scheme, described vegetable oil acid be eleostearic acid, linoleic acid,
One or more mixture in behenic acid, castor oil acid.
Preferred as technique scheme, described binary acid be maleic anhydride, adipic acid,
One or more mixture in decanedioic acid
Preferred as technique scheme, described polyhydric alcohol is diethylene glycol, trihydroxy methyl third
Alkane, trimethylolethane, one or more mixture in tetramethylolmethane
Preferred as technique scheme, described plasticizer is glycerol, Polyethylene Glycol, the third two
One or more mixture in alcohol
Preferred as technique scheme, described coupling agent be isobutyl triethoxy silane,
One or more mixture in silane coupler DL560, silane coupler DL171.
Preferred as technique scheme, described solvent is butyl acetate, n-butyl alcohol, isobutyl
One or more mixture in alcohol
Preferred as technique scheme, a kind of coating material, in terms of weight is divided, including with
Lower component:
Short oil-ity alcohol acid resin 55 parts, vinyl triamine 1.5 parts,
Plasticizer 3.5 parts, butyl rubber 20 parts,
Amino oxosilane 6.5 parts, nano silver particles 1.2 parts,
Coupling agent 1.3 parts, solvent 11,
Wherein said short oil-ity alcohol acid resin is that vegetable oil acid, binary acid and polyhydric alcohol are by esterification
Effect polycondensation forms, and polycondensation method can use state of the art to implement.(program does not goes out
The most in detail in the claims, should delete, as needed to retain, one can be increased in detail in the claims
Bar dependent claims)
The preparation method of a kind of rustless steel thermos flask coating material of the present invention includes following step
Rapid:
(1) short oil-ity alcohol acid resin is joined in partial solvent, stir under the conditions of 60 DEG C
After 30min, grinder grinds 30min, obtains mixed liquor A,
(2) by vinyl triamine, plasticizer adds in partial solvent, and amino oxosilane adds
In solvent, under the conditions of 90 DEG C, stir 60min, obtain mixed liquid B,
(3) by nano silver particles, butyl rubber and coupling agent add in mixed liquor A, at a high speed
After disperseing 30min on dispersion machine, obtain mixed liquor C,
(4) mixed liquid B is mixed with mixed liquor C, and under the conditions of 60 after stirring 60min,
Evacuation removes bubble removing, by obtained mixture with the air spraying of 0.5-0.6MPa in molding
Mould, solidifies 40min, obtains rustless steel thermos flask coating material at 150 DEG C.
The method have the advantages that
This coating material does not contains benzene, will not damage human body.Solvent for use is volatile
Solvent, in spraying process, can quickly volatilize through high-temperature heating, can improve coating distribution
Homogeneity.Vinyl triamine is the firming agent of excellent performance, has good film performance,
The surface gloss of coating material can be improved.The interpolation of amino oxosilane can effectively strengthen
Coating material and the adhesion of base material, make coating material difficult drop-off.Nano silver particles is well recognized as
Strong bactericidal agent, a small amount of interpolation can play excellence bactericidal effect, make this coating material
There is antibiotic property, also make rustless steel thermos flask safer, health.
Detailed description of the invention:
In order to be better understood from the present invention, below by embodiment, the present invention is further described,
Embodiment is served only for explaining the present invention, and the present invention will not constitute any restriction.
Embodiment 1:
Short oil-ity alcohol acid resin 45 parts, vinyl triamine 1.5 parts,
Plasticizer 2.7 parts, butyl rubber 16 parts,
Amino oxosilane 2.5 parts, nano silver particles 1.3 parts,
Coupling agent 1.0 parts, solvent 27,
Wherein said short oil-ity alcohol acid resin is that vegetable oil acid, binary acid and polyhydric alcohol are by esterification
Effect polycondensation forms, and polycondensation method can use state of the art to implement.
Preferably described as technique scheme
The preparation method of above-mentioned rustless steel thermos flask coating material comprises the following steps:
(1) short oil-ity alcohol acid resin is joined in partial solvent, stir under the conditions of 60 DEG C
After 30min, grinder grinds 30min, obtains mixed liquor A,
(2) by vinyl triamine, plasticizer adds in partial solvent, and amino oxosilane adds
In solvent, under the conditions of 90 DEG C, stir 60min, obtain mixed liquid B,
(3) by nano silver particles, butyl rubber and coupling agent add in mixed liquor A, at height
After disperseing 30min on speed dispersion machine, obtain mixed liquor C,
(4) mixed liquid B is mixed with mixed liquor C, and under the conditions of 60 DEG C, stir 60min
After, evacuation removes bubble removing, by obtained mixture with the air spraying of 0.5-0.6MPa in
Mould, solidifies 40min, obtains rustless steel thermos flask coating material at 150 DEG C.
Embodiment 2
Short oil-ity alcohol acid resin 55 parts, vinyl triamine 1.5 parts,
Plasticizer 3.5 parts, butyl rubber 20 parts,
Amino oxosilane 6.5 parts, nano silver particles 1.2 parts,
Coupling agent 1.3 parts, solvent 11,
Wherein said short oil-ity alcohol acid resin is that vegetable oil acid, binary acid and polyhydric alcohol are by esterification
Effect polycondensation forms, and polycondensation method can use state of the art to implement.
Preferably described as technique scheme
The preparation method of above-mentioned rustless steel thermos flask coating material comprises the following steps:
(1) short oil-ity alcohol acid resin is joined in partial solvent, stir under the conditions of 60 DEG C
After 30min, grinder grinds 30min, obtains mixed liquor A,
(2) by vinyl triamine, plasticizer adds in partial solvent, and amino oxosilane adds
In solvent, under the conditions of 90 DEG C, stir 60min, obtain mixed liquid B,
(3) by nano silver particles, butyl rubber and coupling agent add in mixed liquor A, at height
After disperseing 30min on speed dispersion machine, obtain mixed liquor C,
(4) mixed liquid B is mixed with mixed liquor C, and under the conditions of 60, stir 60min
After, evacuation removes bubble removing, by obtained mixture with the air spraying of 0.5-0.6MPa in
Mould, solidifies 40min, obtains rustless steel thermos flask coating material at 150 DEG C.
Embodiment 3
Short oil-ity alcohol acid resin 50 parts, vinyl triamine 1.8 parts,
Plasticizer 2.3 parts, butyl rubber 20 parts,
Amino oxosilane 7 parts, nano silver particles 1.5 parts,
Coupling agent 1.4 parts, solvent 16,
Wherein said short oil-ity alcohol acid resin is that vegetable oil acid, binary acid and polyhydric alcohol are by esterification
Effect polycondensation forms, and polycondensation method can use state of the art to implement.
Preferably described as technique scheme
The preparation method of above-mentioned rustless steel thermos flask coating material comprises the following steps:
(1) short oil-ity alcohol acid resin is joined in partial solvent, stir under the conditions of 60 DEG C
After 30min, grinder grinds 30min, obtains mixed liquor A,
(2) by vinyl triamine, plasticizer adds in partial solvent, and amino oxosilane adds
In solvent, under the conditions of 90 DEG C, stir 60min, obtain mixed liquid B,
(3) by nano silver particles, butyl rubber and coupling agent add in mixed liquor A, at height
After disperseing 30min on speed dispersion machine, obtain mixed liquor C,
(4) mixed liquid B is mixed with mixed liquor C, and under the conditions of 60, stir 60min
After, evacuation removes bubble removing, by obtained mixture with the air spraying of 0.5-0.6MPa in
Mould, solidifies 40min, obtains rustless steel thermos flask coating material at 150 DEG C.
Embodiment 4
Short oil-ity alcohol acid resin 57 parts, vinyl triamine 1.3 parts,
Plasticizer 3.2 parts, butyl rubber 18 parts,
Amino oxosilane 5 parts, nano silver particles 1 part,
Coupling agent 15 parts, solvent 13,
Wherein said short oil-ity alcohol acid resin is that vegetable oil acid, binary acid and polyhydric alcohol are by esterification
Effect polycondensation forms, and polycondensation method can use state of the art to implement.
Preferably described as technique scheme
The preparation method of above-mentioned rustless steel thermos flask coating material comprises the following steps:
(1) short oil-ity alcohol acid resin is joined in partial solvent, stir under the conditions of 60 DEG C
After 30min, grinder grinds 30min, obtains mixed liquor A,
(2) by vinyl triamine, plasticizer adds in partial solvent, and amino oxosilane adds
In solvent, under the conditions of 90 DEG C, stir 60min, obtain mixed liquid B,
(3) by nano silver particles, butyl rubber and coupling agent add in mixed liquor A, at height
After disperseing 30min on speed dispersion machine, obtain mixed liquor C,
(4) mixed liquid B is mixed with mixed liquor C, and under the conditions of 60, stir 60min
After, evacuation removes bubble removing, by obtained mixture with the air spraying of 0.5-0.6MPa in
Mould, solidifies 40min, obtains rustless steel thermos flask coating material at 150 DEG C.
Above-described embodiment has all carried out performance test, and wherein comparative example is that common stainless steel thermos flask is used
Coating material, test result is as shown in Table 1 and Table 2.
Table 1
Table 2
From the point of view of Tables 1 and 2, the glof club head coating material that the present invention provides adheres to
Power is strong, and mechanical property is good, excellent shock resistance.
Claims (9)
1. a rustless steel thermos flask coating material, it is characterised in that by weight,
This coating material is composed of the following components:
Short oil-ity alcohol acid resin 40-60 part, vinyl triamine 1-2 part,
Plasticizer 2.5-3.5 part, butyl rubber 15-25 part,
Amino silicone 5-15 part, nano silver particles 1-1.5 part,
Coupling agent 0.5-2 part, solvent 10-30 part,
Wherein said short oil-ity alcohol acid resin is that vegetable oil acid, binary acid and polyhydric alcohol are by esterification
Effect polycondensation forms.
Rustless steel thermos flask coating material the most according to claim 1, its feature exists
In: the oil content of described short oil-ity alcohol acid resin is 35%-36%.
Rustless steel thermos flask coating material the most according to claim 1, its feature exists
In: described vegetable oil acid is in eleostearic acid, linoleic acid, behenic acid, castor oil acid
Plant or multiple mixture.
Rustless steel thermos flask coating material the most according to claim 1, its feature exists
In: described binary acid is that one or more in maleic anhydride, adipic acid, decanedioic acid are mixed
Compound.
Rustless steel thermos flask coating material the most according to claim 1, its feature exists
In: described polyhydric alcohol is diethylene glycol, trimethylolpropane, trimethylolethane, Ji Wusi
One or more mixture in alcohol.
Rustless steel thermos flask coating material the most according to claim 1, its feature exists
In: described plasticizer is glycerol, Polyethylene Glycol, one or more mixture in propylene glycol.
Rustless steel thermos flask coating material the most according to claim 1, its feature exists
In: described coupling agent is isobutyl triethoxy silane, silane coupler DL560, silane idol
One or more mixture in connection agent DL171.
Rustless steel thermos flask coating material the most according to claim 1, its feature exists
In: described solvent is butyl acetate, n-butyl alcohol, one or more mixture in isobutanol.
9. the preparation method of a rustless steel thermos flask coating material, it is characterised in that by with
Lower step forms:
(1) short oil-ity alcohol acid resin is joined in partial solvent, stir under the conditions of 60 DEG C
After 30min, grinder grinds 30min, obtains mixed liquor A；
(2) by vinyl triamine, plasticizer adds in partial solvent, and amino oxosilane adds
In solvent, under the conditions of 90 DEG C, stir 60min, obtain mixed liquid B；
(3) by nano silver particles, butyl rubber and coupling agent add in mixed liquor A, at height
After disperseing 30min on speed dispersion machine, obtain mixed liquor C；
(4) mixed liquid B is mixed with mixed liquor C, and under the conditions of 60 DEG C, stir 60min
After, evacuation removes bubble removing, by obtained mixture with the air spraying of 0.5-0.6MPa in
Mould, solidifies 40min, obtains rustless steel thermos flask coating material at 150 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610157851.6A CN105778737A (en) | 2016-03-18 | 2016-03-18 | Coating material for stainless steel vacuum bottles and preparation method of coating material for stainless steel vacuum bottles |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610157851.6A CN105778737A (en) | 2016-03-18 | 2016-03-18 | Coating material for stainless steel vacuum bottles and preparation method of coating material for stainless steel vacuum bottles |
Publications (1)
| Publication Number | Publication Date |
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| CN105778737A true CN105778737A (en) | 2016-07-20 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610157851.6A Pending CN105778737A (en) | 2016-03-18 | 2016-03-18 | Coating material for stainless steel vacuum bottles and preparation method of coating material for stainless steel vacuum bottles |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101967316A (en) * | 2010-09-08 | 2011-02-09 | 中国乐凯胶片集团公司 | Nontoxic antifouling paint for oceanographic ship and facilities and method for preparing paint |
| CN102690590A (en) * | 2012-06-14 | 2012-09-26 | 海安县国力化工有限公司 | Chlorinated rubber rust coating |
| CN103232796A (en) * | 2013-05-13 | 2013-08-07 | 扬州大学 | Quick-drying anticorrosive dipping prime paint with low viscosity as well as preparation and application method thereof |
| CN104250476A (en) * | 2014-09-19 | 2014-12-31 | 苏州云舒新材料科技有限公司 | Marine long-lasting antifouling paint and preparation method thereof |
| CN105238161A (en) * | 2015-09-22 | 2016-01-13 | 安徽皖东化工有限公司 | Nanometer negative ion powder-modified nontoxic low-surface-energy marine coating and manufacturing method thereof |
-
2016
- 2016-03-18 CN CN201610157851.6A patent/CN105778737A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101967316A (en) * | 2010-09-08 | 2011-02-09 | 中国乐凯胶片集团公司 | Nontoxic antifouling paint for oceanographic ship and facilities and method for preparing paint |
| CN102690590A (en) * | 2012-06-14 | 2012-09-26 | 海安县国力化工有限公司 | Chlorinated rubber rust coating |
| CN103232796A (en) * | 2013-05-13 | 2013-08-07 | 扬州大学 | Quick-drying anticorrosive dipping prime paint with low viscosity as well as preparation and application method thereof |
| CN104250476A (en) * | 2014-09-19 | 2014-12-31 | 苏州云舒新材料科技有限公司 | Marine long-lasting antifouling paint and preparation method thereof |
| CN105238161A (en) * | 2015-09-22 | 2016-01-13 | 安徽皖东化工有限公司 | Nanometer negative ion powder-modified nontoxic low-surface-energy marine coating and manufacturing method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 刘德峥: "《精细化工生产工艺 第二版》", 30 September 2008, 化学工业出版社 * |
| 谌伟庆 等: "纳米材料对醇酸树脂涂料的改性", 《江苏化工》 * |
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Application publication date: 20160720 |