CN105771821B - A kind of gas liquid reaction parallel test tank - Google Patents
A kind of gas liquid reaction parallel test tank Download PDFInfo
- Publication number
- CN105771821B CN105771821B CN201610174385.2A CN201610174385A CN105771821B CN 105771821 B CN105771821 B CN 105771821B CN 201610174385 A CN201610174385 A CN 201610174385A CN 105771821 B CN105771821 B CN 105771821B
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- Prior art keywords
- tank body
- parallel test
- shim
- liquid reaction
- lampshade
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1856—Stationary reactors having moving elements inside placed in parallel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)
- Devices For Use In Laboratory Experiments (AREA)
Abstract
The invention discloses a kind of gas liquid reaction parallel test tanks, by tank body, cover, shim and lower bucket composition, the space of the bottom surface of tank body upward 2/3rds is divided longitudinally into several identical compartments by shim, the quantity of compartment is more than 2, concave surface is set among compartment bottom surface, gas port is set on cover, air gauge and sample tap, shim intersection sets cylindrical shape lampshade, lampshade is arranged on shim intersection hypomere, lampshade is in tank body bottom opening, lamp is inserted into lampshade, lower bucket upper bottom surface is heating dish, magnetic stirring apparatus is set in lower bucket, the agitating paddle axis of magnetic stirring apparatus is connected by supporting rod with lamp.Superjacent air space connects in tank body, and reaction is conducive to the progress of parallel test in identical gaseous environment.
Description
Technical field
The present invention relates to a kind of gas liquid reaction parallel test tanks.
Background technology
At present, realize that there are many device category of vapor-liquid two phases reaction, however carry out the equipment of parallel test parameter investigation very
It is few, how disposably multiple response parameters to be investigated, while avoid other parameter influence be chemical experiment now always
The target of pursuit.The equipment of chemical reaction small-scale experiment use, the material all very littles used, the variation of some response parameter small range
It will carry out great influence to reaction zone, thus the requirement of parallel laboratory test device is more urgent.
The content of the invention
In order to overcome the above-mentioned deficiencies of the prior art, the object of the present invention is to provide a kind of gas liquid reaction parallel test tank,
Superjacent air space connects in tank body, in identical gaseous environment, is conducive to the progress of parallel test.
To achieve these goals, the present invention adopts the following technical scheme that：
A kind of gas liquid reaction parallel test tank is made of tank body, cover, shim and lower bucket, and the cover can seal
It is placed on the tank body, the tank body bottom surface is plane bottom, and the shim is by the bottom surface of the tank body upward 2/3rds
Space is divided longitudinally into several identical compartments, and the quantity of the compartment is more than two, concave surface is set among the compartment bottom surface, described
Gas port, air gauge and sample tap are set on cover, and the gas port sets switch, and each compartment, which is correspondingly arranged described in one, to be taken
Sample mouth, the shim intersection set cylindrical shape lampshade, and the lampshade is arranged on shim intersection hypomere, the lamp
The tank body bottom opening is covered on, lamp is inserted into the lampshade, sets the lower bucket under the tank body, on the lower bucket
Bottom surface is heating dish, sets magnetic stirring apparatus in the lower bucket, the agitating paddle axis of the magnetic stirring apparatus by supporting rod with
The lamp connection.
It is preferred that：The longitudinal section of the tank body is symmetrical figure, the longitudinal section by upper bottom, bottom and the upper bottom of connection and
The arc of bottom is formed.
It is preferred that：The arc convex surface is outside.
It is preferred that：The concave surface size is identical.
It is preferred that：Iron plate interlayer is set under the concave surface.
It is preferred that：The quantity of the compartment is four or six.
It is preferred that：The tank body and the shim are made of transparent material.
Beneficial effects of the present invention：
1. compartment superjacent air space connects, compartment is made to be in identical environment, gas is after cover entrance full of in entire tank
Environment makes the condition that compartment obtains gas identical, such as：Gas source, system pressure etc. are identical, realize that multiple gas liquid reactions are parallel
It carries out, also achieves the investigation of gas liquid reaction parameter.
2. tank body, shim are transparent material（Glass etc.）It is made, realizes the Real Time Observation of reacting phenomenon.
3. the quantity of compartment is two or more, that is, the quantity for the reaction being carried out at the same time is more than two, multiple reactions
Progress more embody the ability of the device parallel test.The quantity of compartment is preferably arranged to two or three or four or six.
4. the size of compartment is identical, further avoid because of the difference for the response parameter that compartment different band is come, intensifier into
The ability of row parallel laboratory test.
5. cover sets gas port, gas and vacuumized convenient for being conveyed into tank body, gas port set switch realize vacuumize and
The switching of inflatable body.
6. the reaction among compartment bottom surface concave surface being set to be conducive to be stirred is put into magneton stirring.Concave surface size is identical,
Beneficial to progress parallel reaction.Iron plate interlayer is set among bottom surface under concave surface, the setting of iron plate interlayer can make magneton be put into every
Between after inhale on concave surface, prevent different compartment magnetons from assembling, make easy to operate.In addition, leaving certain space around iron plate, place
Iron plate heating expansion damage tank body.
7. lampshade is arranged on shim intersection, intersection hypomere is preferably provided at, lamp is set in lampshade, is conducive to react
The observation of phenomenon, while suitable for the parallel progress of light reaction Type Test.
8. the longitudinal section of tank body is symmetrical figure, longitudinal section is by upper bottom, bottom and the arc structure of the upper bottom of connection and bottom
Into.Convex surface is outside, can amplification test phenomenon, coordinate the use of lamp in lampshade that reacting phenomenon can be made more obvious.
9. lampshade is in bottom opening, for wiring or the configuration of the power supply of lamp.
10. sample tap is designed for sampling, convenient for the real-time tracking of reaction, sample tap can also be used for adding for reaction.
11. barometric presence is more conducive to and comprehensive record is carried out to parallel test.
12. fan-shaped cross section or covering of the fan for compartment, different from conventional reaction vessel, in the case where magneton stirs,
Liquid vortex flows in compartment, due to not round and smooth in compartment, make should smooth eddying motion liquid it is hindered, liquid exists
It is unfolded at compartment within angle, shows the larger contact area with overhead gas, the performance of reacting phenomenon is more obvious herein.
13. tank body and electricity consumption can be separated as the lower bucket of the energy, tank body is carried out the operation such as scrubbing more convenient.
14. magnetic stirring apparatus is used for providing magnetic agitation, heating dish is used for heating to tank body.
15. agitating paddle axis is connected by supporting rod with lamp, lamp is made to be rotated simultaneously with agitating paddle, the rotation of lamp can felt
More vivid judgement mixing speed on official.
16. compact battery may be employed in the power supply of lamp, can also be connected to by wiring on the circuit of lower bucket, the company of wiring
Mode is connect to be rotatablely connected at agitating paddle axis.
17. sample tap, gas port and air gauge are arranged on cover, sample tap, gas port and air gauge lower end are not revealed from cover
Go out, reduce the distribution that gas in tank body is influenced due to exposing.
18. sealing of tank cover is placed on tank body, positioner between cover and tank body is set, enables the sample tap on cover
Compartment is accurately aimed at, facilitates sampling.
19. tank body and cover are by the card and card slot of mutual cooperation come the opposite position of tank body and cover when determining that lid closes
It puts, sample tap is made accurately to be directed at compartment.
Description of the drawings
Fig. 1 is schematic structural view of the invention.
Wherein, 1. tank body, 2. covers, 3. shims, 4. compartments, 5. gas ports, 6. air gauges, 7. lampshades, 8. lamps, 9. supports
Bar, 10. sample taps, 11. times buckets, 12. agitating paddles.
Specific embodiment
The invention will be further described below in conjunction with the accompanying drawings.
As shown in Figure 1, a kind of gas liquid reaction parallel test tank, is made of, institute tank body 1, cover 2, shim 3 and lower bucket 11
It states cover 2 and can seal and be placed on the tank body 1,1 bottom surface of tank body is plane bottom, and the shim 3 is by the tank body 1
The space of bottom surface upward 2/3rds is divided longitudinally into several identical compartments 4, and the quantity of the compartment 4 is more than two, the compartment 4
Concave surface among bottom surface is set, gas port 5, air gauge 6 and sample tap 10 are set on the cover 2, the gas port 5 sets switch, often
A compartment 4 is correspondingly arranged a sample tap 10, and 3 intersection of shim sets cylindrical shape lampshade 7, the lampshade
7 are arranged on the 3 intersection hypomere of shim, and the lampshade 7 is inserted into the lamp in 1 bottom opening of tank body, lamp 8
In cover 7, described 1 time setting lower bucket 11 of tank body, lower 11 upper bottom surface of bucket is heating dish, and magnetic force is set in the lower bucket 11
Blender, 12 axis of agitating paddle of the magnetic stirring apparatus are connected by supporting rod 9 with the lamp 8.
It is preferred that：The longitudinal section of the tank body 1 is symmetrical figure, and the longitudinal section is by upper bottom, bottom and the upper bottom of connection
It is formed with the arc of bottom.
It is preferred that：The arc convex surface is outside.
It is preferred that：The concave surface size is identical.
It is preferred that：Iron plate interlayer is set under the concave surface.
It is preferred that：The quantity of the compartment 4 is four or six.
It is preferred that：The tank body 1 and the shim are made of transparent material.
Above-mentioned, although the foregoing specific embodiments of the present invention is described with reference to the accompanying drawings, not protects model to the present invention
The limitation enclosed, those skilled in the art should understand that, based on the technical solutions of the present invention, those skilled in the art are not
Need to make the creative labor the various modifications or changes that can be made still within protection scope of the present invention.
Claims (7)
1. a kind of gas liquid reaction parallel test tank, by tank body（1）, cover（2）, shim（3）With lower bucket（11）Composition, the tank
Lid（2）It can seal and be placed on the tank body（1）On, the tank body（1）Bottom surface be plane bottom, the shim（3）By the tank
Body（1）The space of bottom surface upward 2/3rds be divided longitudinally into several identical compartments（4）, the compartment（4）Quantity be more than
Two, the compartment（4）Concave surface, the cover are set among bottom surface（2）Upper setting gas port（5）, air gauge（6）And sample tap
（10）, the gas port（5）Switch, each compartment are set（4）It is correspondingly arranged a sample tap（10）, the shim
（3）Intersection sets cylindrical shape lampshade（7）, the lampshade（7）It is arranged on the shim（3）Intersection hypomere, the lampshade
（7）In the tank body（1）Bottom opening, lamp（8）It is inserted into the lampshade（7）It is interior, the tank body（1）Under lower setting is described
Bucket（11）, the lower bucket（11）Upper bottom surface is heating dish, the lower bucket（11）Interior setting magnetic stirring apparatus, the magnetic stirring apparatus
Agitating paddle（12）Axis passes through supporting rod（9）With the lamp（8）Connection.
2. a kind of gas liquid reaction parallel test device as described in claim 1, it is characterized in that, the tank body（1）Longitudinal section
For symmetrical figure, the longitudinal section is made of upper bottom, bottom and the arc of the upper bottom of connection and bottom.
3. a kind of gas liquid reaction parallel test device as claimed in claim 2, it is characterized in that, the arc convex surface is outside.
4. a kind of gas liquid reaction parallel test device as described in claim 1, it is characterized in that, the concave surface size is identical.
5. a kind of gas liquid reaction parallel test device as described in claim 1, it is characterized in that, under the concave surface iron plate is set to press from both sides
Layer.
6. a kind of gas liquid reaction parallel test device as described in claim 1, it is characterized in that, the compartment（4）Quantity be
Four or six.
7. a kind of gas liquid reaction parallel test device as described in claim 1, it is characterized in that, the tank body（1）With described point
Partition is made of transparent material.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610174385.2A CN105771821B (en) | 2016-03-24 | 2016-03-24 | A kind of gas liquid reaction parallel test tank |
| CN201711298485.7A CN107744784B (en) | 2016-03-24 | 2016-03-24 | Gas-liquid reaction parallel test tank |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610174385.2A CN105771821B (en) | 2016-03-24 | 2016-03-24 | A kind of gas liquid reaction parallel test tank |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711298485.7A Division CN107744784B (en) | 2016-03-24 | 2016-03-24 | Gas-liquid reaction parallel test tank |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105771821A CN105771821A (en) | 2016-07-20 |
| CN105771821B true CN105771821B (en) | 2018-05-29 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610174385.2A Active CN105771821B (en) | 2016-03-24 | 2016-03-24 | A kind of gas liquid reaction parallel test tank |
| CN201711298485.7A Active CN107744784B (en) | 2016-03-24 | 2016-03-24 | Gas-liquid reaction parallel test tank |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711298485.7A Active CN107744784B (en) | 2016-03-24 | 2016-03-24 | Gas-liquid reaction parallel test tank |
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| CN (2) | CN105771821B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110237795A (en) * | 2019-05-15 | 2019-09-17 | 铜仁学院 | A kind of photocatalytic reaction device |
| CN110193512B (en) * | 2019-05-21 | 2024-06-18 | 中电建路桥集团有限公司 | Device and method for repairing petroleum organic matter contaminated soil by two-dimensional alternating current electric field reinforced microorganisms |
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|---|---|---|---|---|
| CN1303731A (en) * | 1999-12-15 | 2001-07-18 | 环球油品公司 | Combined catalysis reactor |
| CN104190344A (en) * | 2014-07-25 | 2014-12-10 | 北京泊菲莱科技有限公司 | Light irradiation multi-sample parallel reaction device |
| CN204193930U (en) * | 2014-10-22 | 2015-03-11 | 华中师范大学 | High pressure apparatus for photoreaction |
| CN204193929U (en) * | 2014-10-22 | 2015-03-11 | 华中师范大学 | Normal pressure visible light catalytic parallel reaction instrument |
| CN204656542U (en) * | 2015-05-31 | 2015-09-23 | 任凌云 | A kind of temperature control stirring parallel reaction device |
| CN105032328A (en) * | 2015-08-24 | 2015-11-11 | 郑州大学 | Chemical parallel reaction device |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US6783737B2 (en) * | 2002-01-25 | 2004-08-31 | Bristol-Myers Squibb Company | High pressure chemistry reactor |
| CN1378082A (en) * | 2002-05-09 | 2002-11-06 | 云南烟草科学研究院工业研究所 | Method and device for detecting harmess of passive smoking |
| KR100789235B1 (en) * | 2005-11-08 | 2008-01-02 | 주식회사 엘지화학 | Parallel type polymerization reactor |
| CN102578049B (en) * | 2012-02-29 | 2013-11-20 | 成都鼎明光电科技有限公司 | Insect phototaxis testing device |
| CN103454236B (en) * | 2013-09-30 | 2015-09-23 | 重庆大学 | A kind of accurately residual spectral method of detection of agriculture |
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2016
- 2016-03-24 CN CN201610174385.2A patent/CN105771821B/en active Active
- 2016-03-24 CN CN201711298485.7A patent/CN107744784B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1303731A (en) * | 1999-12-15 | 2001-07-18 | 环球油品公司 | Combined catalysis reactor |
| CN104190344A (en) * | 2014-07-25 | 2014-12-10 | 北京泊菲莱科技有限公司 | Light irradiation multi-sample parallel reaction device |
| CN204193930U (en) * | 2014-10-22 | 2015-03-11 | 华中师范大学 | High pressure apparatus for photoreaction |
| CN204193929U (en) * | 2014-10-22 | 2015-03-11 | 华中师范大学 | Normal pressure visible light catalytic parallel reaction instrument |
| CN204656542U (en) * | 2015-05-31 | 2015-09-23 | 任凌云 | A kind of temperature control stirring parallel reaction device |
| CN105032328A (en) * | 2015-08-24 | 2015-11-11 | 郑州大学 | Chemical parallel reaction device |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107744784B (en) | 2019-12-06 |
| CN105771821A (en) | 2016-07-20 |
| CN107744784A (en) | 2018-03-02 |
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| TA01 | Transfer of patent application right |
Effective date of registration: 20180425 Address after: 362000 294 Mei Zhong village, pengpeng Town, Yongchun County, Quanzhou, Fujian Applicant after: Lv Qiongjia Address before: 262610 238 Yuezhuang village, Xin Zhai Town, Linqu County, Weifang, Shandong Applicant before: Zhang Hongmei |
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Effective date of registration: 20190708 Address after: 333300 Tashan Industrial Zone, Leping Industrial Park, Jingdezhen City, Jiangxi Province Patentee after: Jiangxi Huaxing Chemical Co., Ltd. Address before: 362000 294 Mei Zhong village, pengpeng Town, Yongchun County, Quanzhou, Fujian Patentee before: Lv Qiongjia |
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