CN105749847A - Reaction device - Google Patents
Reaction device Download PDFInfo
- Publication number
- CN105749847A CN105749847A CN201610262256.9A CN201610262256A CN105749847A CN 105749847 A CN105749847 A CN 105749847A CN 201610262256 A CN201610262256 A CN 201610262256A CN 105749847 A CN105749847 A CN 105749847A
- Authority
- CN
- China
- Prior art keywords
- reaction
- guide plate
- motor
- reaction vessel
- chuck
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00004—Scale aspects
- B01J2219/00009—Pilot-scale plants
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00132—Controlling the temperature using electric heating or cooling elements
- B01J2219/00135—Electric resistance heaters
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention provides a reaction device.The reaction device comprises a supporting foot, a reaction vessel is installed on the supporting foot, the upper portion of the reaction vessel is covered with a guide plate, a motor is fixed above the guide plate, the lower portion of the motor is connected with a stirrer, and the stirrer extends into the reaction vessel through a guide plate; a jacket is arranged on the outer side of the reaction vessel in a surrounding mode, and electrical heating tubes are installed on the lower portion of the jacket.According to the novel reaction device, for pilot-scale reactions of which the chemical reaction matter quantity is smaller than 10 kg, stable external conditions can be guaranteed, human errors are avoided, the testing speed is increased, and expanded production is promoted.
Description
Technical field
The present invention relates to a kind of reaction unit.
Background technology
Chemicals is when preparation, early stage is typically via the reaction test of lab scale, pilot scale, ability volume production after stable testing is qualified, lab scale and pilot process all complete at laboratory, the reactant quality related to during lab scale is generally less than 1000 grams, the reactant quality that pilot scale relates to is between 1 kilogram to 10 kilogram, in view of the reactant quality of pilot scale is bigger, general reaction vessel is utilized to be difficult to complete at laboratory, blowing, feeding, stirring are all wasted time and energy, and response error very easily occurs, cause that result deviates, be unfavorable for the expanding production in later stage.
Summary of the invention
For solving above-mentioned technical problem, the invention provides a kind of new reaction unit, for the pilot scale reaction less than 10 kilograms of the chemical reactant quality, it is possible to ensure the stablizing of external condition, it is to avoid personal error, accelerate test speed, be beneficial to expanding production.
A kind of reaction unit, including a leg, leg is installed a reaction pot, is stamped a guide plate above reaction pot, and a guide plate motor fixed above, this motor is connected below an agitator, and this agitator is stretched in described reaction pot by guide plate；This reaction pot wraps around a chuck, and chuck is installed below electrothermal tube.
Preferably, being additionally provided with oil-out and discharging opening below described chuck, a side end face is provided with charging aperture and gas outlet.
The present invention proposes a kind of reaction unit, is stirred by driven by motor agitator, and electrothermal tube directly heats, and simplifies practical operation flow process, makes reaction more abundant, and external reaction condition is easier to control, it is to avoid personal error, accelerates test speed, is beneficial to expanding production.
Accompanying drawing explanation
In order to be illustrated more clearly that the embodiment of the present invention or technical scheme of the prior art, the accompanying drawing used required in embodiment or description of the prior art will be briefly described below.
Fig. 1 is the structural representation of a kind of reaction unit disclosed in the embodiment of the present invention.
1, leg 2, reaction pot 3, guide plate 4, motor 5, agitator 6, chuck
7, electrothermal tube 8, oil-out 9, discharging opening 10, charging aperture 11, gas outlet.
Detailed description of the invention
Below in conjunction with accompanying drawing, the technical scheme in the embodiment of the present invention is clearly and completely described.
As it is shown in figure 1, a kind of reaction unit, including a leg 1, leg 1 is installed a reaction pot 2, above reaction pot 2, is stamped a guide plate 3, guide plate 3 motor 4 fixed above, this motor 4 is connected below an agitator 5, and this agitator 5 is stretched in described reaction pot 2 by guide plate 3；This reaction pot 2 wraps around a chuck 6, and chuck 6 is installed below electrothermal tube 7.
Being additionally provided with oil-out 8 and discharging opening 9 below described chuck 6, a side end face is provided with charging aperture 10 and gas outlet 11.
During practical operation, reaction pot 2 is put in reactant mixing, motor 4 is utilized to be stirred, reduce manpower, the electrothermal tube 7 below chuck 6 is utilized to directly heat, power and response time according to electrothermal tube 7 control reaction temperature, during practical operation, thermometer assigned by guide plate 3, temperature can be controlled in real time, by arranging discharging opening 9, charging aperture 10, gas outlet 11 and oil-out 8, can meet and have gas to produce, the multiple chemical reactions such as powder product or liquid product, simplify practical operation flow process, make reaction more abundant, external reaction condition is easier to control, avoid personal error, accelerate test speed, it is beneficial to expanding production.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all amendments made within the spirit of the present invention and converting on an equal basis, all should drop within protection scope of the present invention.
Claims (2)
1. kind of reaction unit, including a leg, leg is installed a reaction pot, it is characterised in that be stamped a guide plate above reaction pot, and a guide plate motor fixed above, this motor is connected below an agitator, and this agitator is stretched in described reaction pot by guide plate；This reaction pot wraps around a chuck, and chuck is installed below electrothermal tube.
2. a kind of reaction unit according to claim 1, it is characterised in that being additionally provided with oil-out and discharging opening below described chuck, a side end face is provided with charging aperture and gas outlet.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610262256.9A CN105749847A (en) | 2016-04-25 | 2016-04-25 | Reaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610262256.9A CN105749847A (en) | 2016-04-25 | 2016-04-25 | Reaction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105749847A true CN105749847A (en) | 2016-07-13 |
Family
ID=56325819
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610262256.9A Pending CN105749847A (en) | 2016-04-25 | 2016-04-25 | Reaction device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105749847A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106040135A (en) * | 2016-05-31 | 2016-10-26 | 镇江中化聚氨酯工业设备有限公司 | Reaction device |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003236303A (en) * | 2002-02-13 | 2003-08-26 | Konica Corp | Concentrating crystallization apparatus |
| CN204447986U (en) * | 2014-12-08 | 2015-07-08 | 贾瑞瑾 | A kind of reaction unit |
| CN205032165U (en) * | 2015-08-20 | 2016-02-17 | 王碧霞 | Corrosion -resistant reaction unit |
-
2016
- 2016-04-25 CN CN201610262256.9A patent/CN105749847A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003236303A (en) * | 2002-02-13 | 2003-08-26 | Konica Corp | Concentrating crystallization apparatus |
| CN204447986U (en) * | 2014-12-08 | 2015-07-08 | 贾瑞瑾 | A kind of reaction unit |
| CN205032165U (en) * | 2015-08-20 | 2016-02-17 | 王碧霞 | Corrosion -resistant reaction unit |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106040135A (en) * | 2016-05-31 | 2016-10-26 | 镇江中化聚氨酯工业设备有限公司 | Reaction device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160713 |