CN105732083A - Wet-process firing method of ceramsite by using cow dung - Google Patents

Wet-process firing method of ceramsite by using cow dung Download PDF

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Publication number
CN105732083A
CN105732083A CN201610014497.1A CN201610014497A CN105732083A CN 105732083 A CN105732083 A CN 105732083A CN 201610014497 A CN201610014497 A CN 201610014497A CN 105732083 A CN105732083 A CN 105732083A
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China
Prior art keywords
cattle manure
bentonite
ceramsite
temperature
compressing
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CN201610014497.1A
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CN105732083B (en
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韩新宇
史建武
吴玉珍
刘树银
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Kunming University of Science and Technology
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Kunming University of Science and Technology
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/009Porous or hollow ceramic granular materials, e.g. microballoons

Abstract

The invention relates to a wet-processing firing method of ceramsite by using cow dung and belongs to the technical field of ceramsite production. The method comprises steps of raw material mixing, granulating, pretreatment, high temperature burning, and cooling. The produced ceramsite has the advantages of small density, many pores, uniform morphology and components, high strength, and wear resistant property, can prevent corrosion, freezing, and knocking, has a good insulation performance, can insulate heat and sound, is dampproof, and is suitable for the construction industry.

Description

A kind of by the method for cattle manure dry method baking ceramsite
Technical field
A kind of method that the present invention relates to cattle manure dry method baking ceramsite, belongs to haydite manufacture technology field.
Background technology
Haydite density is little, portion's hole is many, form and composition uniform, intensity is high, wear-resistant, and there is good corrosion resistance, freeze-proof, shock resistance and insulating (insulation, heat insulation, sound insulation, moisture resistance), so being widely used in building materials, agricultural, industry, gardening, fire-resistant heat insulating material, environmental project and other field.At present, the method producing haydite is a lot, and Zhu Xiang etc. uses mud, cattle manure wet method to burn out Superlight ceramsites, but the moisture content of stock own is high, has a large amount of steam to occur, make product ftracture in dry run, and intensity is relatively low, and water absorption rate is higher, and technique is more complicated;The flyash such as Du Xin, clay and mud dry method burn out high-strength ceramic granule, but relatively costly, and current clay has become as China and needs resources to be protected.Therefore, the method for existing production haydite is not ideal enough.
Summary of the invention
A kind of method that the invention provides cattle manure dry method baking ceramsite; solve and make because a large amount of steam occurs in dry run that haydite density is big, water absorption rate is higher, comprcssive strength is relatively low; and preparation method is complicated, relatively costly, by technical problems such as the clay resources of state guarantee.And raw material is garbage, it may be achieved refuse reclamation, replaces clay with bentonite simultaneously, saved resource.
A kind of method that the technical scheme is that cattle manure dry method baking ceramsite, specifically comprising the following steps that of the described method with cattle manure dry method baking ceramsite
Step1, batch mixing;Adding adjuvant cattle manure in major ingredient bentonite, form material, this material includes bentonite, cattle manure, and bentonite, cattle manure are the ratio stirring mixing of 4:1 by weight;The used discarded cattle manure that cattle manure is vaccary, dries cattle manure at 100~110 DEG C, then pulverizes with pulverizer, then filters out, with sieve, the cattle manure that size is 80~120 orders;
Step2, pelletize;The material powder compressing machine that mixes is compressing, and briquetting pressure is 6.5~8.0Mpa, and the dwell time is 20~35s, and being pressed into diameter is 30mm, and height is the cylinder of 10mm;
Step3, pretreatment;Compressing material is placed in crucible, then moves in Muffle furnace, be at 300~400 DEG C, dry expanded 10~30min in temperature;
Step4, high-temperature roasting;Make Muffle furnace be warming up to 1180~1220 DEG C, the material constant temperature after expanded for drying is burnt swollen 10~20min;
Step5, cooling;The material of high-temperature roasting is naturally cooled to room temperature, obtains haydite finished product.
The invention has the beneficial effects as follows:
The haydite density that the present invention burns out is little, portion's hole is many, form and composition uniform, intensity is high, wear-resistant, and there is good corrosion resistance, freeze-proof, shock resistance and insulating (insulation, heat insulation, sound insulation, moisture resistance), density, water absorption rate, comprcssive strength meet national standard.Preparation method is simple, and cost is low, it is easy to accomplish continuous prodution, constant product quality, free from environmental pollution, corrosion-free, and raw material is garbage, it may be achieved refuse reclamation, replaces clay with bentonite simultaneously, has saved resource.
Detailed description of the invention
Embodiment 1: a kind of with the method for cattle manure dry method baking ceramsite, specifically comprising the following steps that of the described method with cattle manure dry method baking ceramsite
Step1, batch mixing;Adding adjuvant cattle manure in major ingredient bentonite, form material, this material includes bentonite, cattle manure, and bentonite, cattle manure are the ratio stirring mixing of 4:1 by weight, i.e. optional bentonite 80 parts, cattle manure 20 parts, stirring mixing;The used discarded cattle manure that cattle manure is vaccary, dries cattle manure at 100 DEG C, then pulverizes with pulverizer, then filters out, with sieve, the cattle manure that size is 80 orders;
Step2, pelletize;The material powder compressing machine that mixes is compressing, and briquetting pressure is 6.5Mpa, and the dwell time is 35s, and being pressed into diameter is 30mm, and height is the cylinder of 10mm;
Step3, pretreatment;Compressing material is placed in crucible, then moves in Muffle furnace, be at 400 DEG C, dry expanded 20min in temperature;
Step4, high-temperature roasting;Make Muffle furnace be warming up to 1180 DEG C, the material constant temperature after expanded for drying is burnt swollen 20min;
Step5, cooling;The material of high-temperature roasting is naturally cooled to room temperature, obtains haydite finished product.
Performance indications such as table 1 after testing:
Table 1
It can be seen that the haydite density burnt out with this understanding is less from the performance of table 1, internal void is many, and water absorption rate is relatively low, and comprcssive strength is higher, and form and composition uniform.Owing to preheating time is moderate, material is warmed and reaches best viscosity, plays foaming effect.
Embodiment 2: a kind of with the method for cattle manure dry method baking ceramsite, specifically comprising the following steps that of the described method with cattle manure dry method baking ceramsite
Step1, batch mixing;Adding adjuvant cattle manure in major ingredient bentonite, form material, this material includes bentonite, cattle manure, and bentonite, cattle manure are the ratio stirring mixing of 4:1 by weight, i.e. optional bentonite 80 parts, cattle manure 20 parts, stirring mixing;The used discarded cattle manure that cattle manure is vaccary, dries cattle manure at 110 DEG C, then pulverizes with pulverizer, then filters out, with sieve, the cattle manure that size is 100 orders;
Step2, pelletize;The material powder compressing machine that mixes is compressing, and briquetting pressure is 7.5Mpa, and the dwell time is 20s, and being pressed into diameter is 30mm, and height is the cylinder of 10mm;
Step3, pretreatment;Compressing material is placed in crucible, then moves in Muffle furnace, be at 350 DEG C, dry expanded 10min in temperature;
Step4, high-temperature roasting;Make Muffle furnace be warming up to 1200 DEG C, the material constant temperature after expanded for drying is burnt swollen 15min;
Step5, cooling;The material of high-temperature roasting is naturally cooled to room temperature, obtains haydite finished product.
Performance indications such as table 2 after testing:
Table 2
It can be seen that the haydite density burnt out with this understanding is less from the performance of table 2, internal void is many, and water absorption rate is relatively low, and comprcssive strength is higher, and form and composition uniform.Owing to sintering temperature is suitable for, the gas of internal generation q.s makes its dilatancy, and body fused solution phasor is very big, and the effect of liquid phase surface tension is moderate, and solid particle is close to each other due to liquid phase surface tension, and liquid phase is filled in gas and makes body densification.
Embodiment 3: a kind of with the method for cattle manure dry method baking ceramsite, specifically comprising the following steps that of the described method with cattle manure dry method baking ceramsite
Step1, batch mixing;Adding adjuvant cattle manure in major ingredient bentonite, form material, this material includes bentonite, cattle manure, and bentonite, cattle manure are the ratio stirring mixing of 4:1 by weight, i.e. optional bentonite 80 parts, cattle manure 20 parts, stirring mixing;The used discarded cattle manure that cattle manure is vaccary, dries cattle manure at 110 DEG C, then pulverizes with pulverizer, then filters out, with sieve, the cattle manure that size is 120 orders;
Step2, pelletize;The material powder compressing machine that mixes is compressing, and briquetting pressure is 8.0Mpa, and the dwell time is 30s, and being pressed into diameter is 30mm, and height is the cylinder of 10mm;
Step3, pretreatment;Compressing material is placed in crucible, then moves in Muffle furnace, be at 300 DEG C, dry expanded 30min in temperature;
Step4, high-temperature roasting;Make Muffle furnace be warming up to 1220 DEG C, the material constant temperature after expanded for drying is burnt swollen 10min;
Step5, cooling;The material of high-temperature roasting is naturally cooled to room temperature, obtains haydite finished product.
Performance indications such as table 3 after testing:
Table 3
It can be seen that the haydite density burnt out with this understanding is less from the performance of table 3, internal void is many, and water absorption rate is relatively low, and comprcssive strength is higher, and form and composition uniform.Firing of haydite is not had too much influence by preheating temperature.
Embodiment 4: a kind of with the method for cattle manure dry method baking ceramsite, specifically comprising the following steps that of the described method with cattle manure dry method baking ceramsite
Step1, batch mixing;Adding adjuvant cattle manure in major ingredient bentonite, form material, this material includes bentonite, cattle manure, and bentonite, cattle manure are the ratio stirring mixing of 4:1 by weight, namely select bentonite 80 parts, cattle manure 20 parts, stirring mixing;The used discarded cattle manure that cattle manure is vaccary, dries cattle manure at 105 DEG C, then pulverizes with pulverizer, then filters out, with sieve, the cattle manure that size is 100 orders;
Step2, pelletize;The material powder compressing machine that mixes is compressing, and briquetting pressure is 7.5Mpa, and the dwell time is 30s, and being pressed into diameter is 30mm, and height is the cylinder of 10mm;
Step3, pretreatment;Compressing material is placed in crucible, then moves in Muffle furnace, be at 350 DEG C, dry expanded 20min in temperature;
Step4, high-temperature roasting;Make Muffle furnace be warming up to 1200 DEG C, the material constant temperature after expanded for drying is burnt swollen 15min;
Step5, cooling;The material of high-temperature roasting is naturally cooled to room temperature, obtains haydite finished product.
Performance indications such as table 4 after testing:
Table 4
It can be seen that the haydite density burnt out with this understanding is less from the performance of table 4, internal void is many, and water absorption rate is relatively low, and comprcssive strength is higher, and form and composition uniform.Owing to sintering time is excessively suitable, the micropore of Shi Bu UNICOM will not being connected with each other, thus forming big pore, making comprcssive strength not reduce.
Above the specific embodiment of the present invention is explained in detail, but the present invention is not limited to above-mentioned embodiment, in the ken that those of ordinary skill in the art possess, it is also possible under the premise without departing from present inventive concept, make various change.

Claims (1)

1. the method with cattle manure dry method baking ceramsite, it is characterised in that: specifically comprising the following steps that of the described method with cattle manure dry method baking ceramsite
Step1, batch mixing;Adding adjuvant cattle manure in major ingredient bentonite, form material, this material includes bentonite, cattle manure, and bentonite, cattle manure are the ratio stirring mixing of 4:1 by weight;The used discarded cattle manure that cattle manure is vaccary, dries cattle manure at 100~110 DEG C, then pulverizes with pulverizer, then filters out, with sieve, the cattle manure that size is 80~120 orders;
Step2, pelletize;The material powder compressing machine that mixes is compressing, and briquetting pressure is 6.5~8.0Mpa, and the dwell time is 20~35s, and being pressed into diameter is 30mm, and height is the cylinder of 10mm;
Step3, pretreatment;Compressing material is placed in crucible, then moves in Muffle furnace, be at 300~400 DEG C, dry expanded 10~30min in temperature;
Step4, high-temperature roasting;Make Muffle furnace be warming up to 1180~1220 DEG C, the material constant temperature after expanded for drying is burnt swollen 10~20min;
Step5, cooling;The material of high-temperature roasting is naturally cooled to room temperature, obtains haydite finished product.
CN201610014497.1A 2016-01-11 2016-01-11 A method of with cow dung dry method baking ceramsite Active CN105732083B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107311587A (en) * 2017-06-28 2017-11-03 昆明理工大学 A kind of method that use ardealite and cow dung make ceramsite board
CN109400108A (en) * 2018-11-06 2019-03-01 海安南京大学高新技术研究院 A kind of preparation method of light, and high-strength fly-ash haydite
CN111302762A (en) * 2020-03-09 2020-06-19 重庆财山建材有限公司合川分公司 Expanded ceramsite and manufacturing method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008136134A1 (en) * 2007-04-24 2008-11-13 Environmental Science Co., Ltd. Method of treating animal feces
CN101613219A (en) * 2009-07-31 2009-12-30 柳树 A kind of method of utilizing mud and cow dung to make haydite
CN105130397A (en) * 2015-07-13 2015-12-09 昆明理工大学 Novel ceramisite and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008136134A1 (en) * 2007-04-24 2008-11-13 Environmental Science Co., Ltd. Method of treating animal feces
CN101613219A (en) * 2009-07-31 2009-12-30 柳树 A kind of method of utilizing mud and cow dung to make haydite
CN105130397A (en) * 2015-07-13 2015-12-09 昆明理工大学 Novel ceramisite and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘景明等: "由化工脱水污泥烧制陶粒", 《北京科技大学学报》 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107311587A (en) * 2017-06-28 2017-11-03 昆明理工大学 A kind of method that use ardealite and cow dung make ceramsite board
CN107311587B (en) * 2017-06-28 2019-11-08 昆明理工大学 A method of ceramsite board is made with ardealite and cow dung
CN109400108A (en) * 2018-11-06 2019-03-01 海安南京大学高新技术研究院 A kind of preparation method of light, and high-strength fly-ash haydite
CN111302762A (en) * 2020-03-09 2020-06-19 重庆财山建材有限公司合川分公司 Expanded ceramsite and manufacturing method thereof

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