CN105713284A - Production process of anti-blocking master batch - Google Patents

Production process of anti-blocking master batch Download PDF

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Publication number
CN105713284A
CN105713284A CN201610305129.2A CN201610305129A CN105713284A CN 105713284 A CN105713284 A CN 105713284A CN 201610305129 A CN201610305129 A CN 201610305129A CN 105713284 A CN105713284 A CN 105713284A
Authority
CN
China
Prior art keywords
polyethylene
mixing
master batch
production process
magnesium silicate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610305129.2A
Other languages
Chinese (zh)
Inventor
王立军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zibo Linzi Alinda Chemical Co Ltd
Original Assignee
Zibo Linzi Alinda Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zibo Linzi Alinda Chemical Co Ltd filed Critical Zibo Linzi Alinda Chemical Co Ltd
Priority to CN201610305129.2A priority Critical patent/CN105713284A/en
Publication of CN105713284A publication Critical patent/CN105713284A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/34Silicon-containing compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B9/00Making granules
    • B29B9/02Making granules by dividing preformed material
    • B29B9/06Making granules by dividing preformed material in the form of filamentary material, e.g. combined with extrusion
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/25Component parts, details or accessories; Auxiliary operations
    • B29C48/92Measuring, controlling or regulating
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/16Nitrogen-containing compounds
    • C08K5/20Carboxylic acid amides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2948/00Indexing scheme relating to extrusion moulding
    • B29C2948/92Measuring, controlling or regulating
    • B29C2948/92504Controlled parameter
    • B29C2948/9258Velocity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2948/00Indexing scheme relating to extrusion moulding
    • B29C2948/92Measuring, controlling or regulating
    • B29C2948/92504Controlled parameter
    • B29C2948/92704Temperature

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

The invention relates to a production process of an anti-blocking master batch, and belongs to the technical field of polyethylene additives. The production process of the anti-blocking master batch comprises the following steps: adding polyethylene and hydrated magnesium silicate into a stirring machine through a feeding machine, mixing for 2-4 minutes, subsequently adding erucyl amide into the stirring machine, continuously mixing for 4-6 minutes, and standing for 1.5-2.5 hours so as to obtain a standby substance; and adding the standby substance into a twin-screw extruder, sufficiently fusing at 50-110 DEG C, extruding, chopping by using a chopping machine, cooling with water, and dehydrating, thereby obtaining the anti-blocking master batch. The production process provided by the invention has the characteristics of low production cost and small raw material addition amount, and is environment-friendly and sanitary, low in working intensity, and applicable to development requirements of a production additive on environmental friendliness, simplicity and multiple functions, and the service lives of a grinding head, a cutter and a screw of production equipment can be prolonged.

Description

The production technology of tissue adhesion masterbatch
Technical field
The present invention relates to the production technology of a kind of tissue adhesion masterbatch, belong to polyethylene additive technology field.
Background technology
Polyolefin film is widely used in industrial goods and the aspect such as the packaging of daily necessities and agricultural production, but polyolefin is thin Film has one " adhesion " phenomenon, makes troubles during using polyolefin film to people.Existing in order to solve the adhesion of thin film As, people can add antiblocking agent or slipping agent in the manufacture process of polyolefin film.Slipping agent generally refers to fatty acid acyl amine, Such as oleamide, erucyl amide etc., this compounds can gradually surface from polyolefin film internal migration to polyolefin film, The surface of film forms a tunic, and this tunic can reduce the coefficient of friction between thin film, makes thin film be prone to interformational sliding, improves its opening Property.Simultaneously because aliphatic amide compounds has certain polarity, film surface hygroscopicity can be changed, thus play anti-quiet The effect of electricity, weakens the Electrostatic Absorption between thin film, improves the resistance to blocking of thin film equally.Existing tissue adhesion masterbatch product is single, Production cost is high, and easily equipment is caused damage in production process, therefore, it is necessary to further ground tissue adhesion masterbatch Study carefully.
Summary of the invention
It is an object of the invention to provide the production technology of a kind of tissue adhesion masterbatch, have that production cost is low, environmentally-friendly sanitary, work strong Spend feature low, that product is compound,
The production technology of tissue adhesion masterbatch of the present invention, comprises the following steps:
(1) mixing
Polyethylene and hydrated magnesium silicate are joined stirrer for mixing 2-4min through screw(-type) feeder, then erucyl amide is added In blender, continue mixing 4-6min, after standing 1.5-2.5h, obtain spares;
(2) pelletize
Spares is joined in double screw extruder, fully extrudes after fusion at 50-110 DEG C, then through pelleter pelletizing, After water cooling, dehydration, obtain tissue adhesion masterbatch.
Wherein, mass percent shared by polyethylene in tissue adhesion masterbatch, hydrated magnesium silicate and erucyl amide is: polyethylene 50-60%, Hydrated magnesium silicate 20-40%, erucyl amide 10-20%.
The concrete operation step of the present invention is as follows:
1, mixing
(1) according to the good various raw materials of recipe requirements accurate weighing, stand-by;
(2) fume recovery system is opened;
(3) open height and stir machine, and polyethylene and hydrated magnesium silicate are sufficiently mixed 2-4min through screw(-type) feeder addition high mixer;
(4) erucyl amide is added high mixer through screw(-type) feeder;
(5) after being sufficiently mixed 4-6min, material is put into hopper, standby after standing two hours;
2, pelletize
(1) granulating system each temperature controlled region temperature, from 1st district to 11 district's temperature from low to high, low temperature 50 DEG C, high temperature 110 DEG C are set;
(2) opening comminutor temperature control system, Dai Ge district temperature rises to design temperature, constant temperature 2 hours;
(3) material is added parallel dual-screw feeding machine;
(4) open water cooling, pelleter, dewaterer successively, blow machine;
(5) comminutor main frame is opened, and adjust rotating speed to 300r/min;
(6) parallel dual-screw feeding machine is opened, adjustment rotating speed to 500r/min;
(7) material is extruded after double screw extruder fully fuses, after pelleter pelletizing, water cooled but, give through blowing machine after dehydration Enter feed bin.
Beneficial effects of the present invention is as follows:
The production technology of the present invention has the advantages that production cost is low, raw material addition is few, and can extend production equipment bistrique, Cutting knife and the service life of screw rod, environmentally-friendly sanitary, labor strength are low simultaneously, adapt to produce auxiliary agent environmental protection brief multi-functional Demand for development.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further.
Embodiment 1
The production technology of tissue adhesion masterbatch, comprises the following steps:
(1) mixing
Polyethylene and hydrated magnesium silicate are joined stirrer for mixing 3min through screw(-type) feeder, then erucyl amide is joined Blender continues mixing 5min, after standing 2h, obtains spares;
(2) pelletize
Spares is joined in double screw extruder, fully extrudes after fusion at 50-110 DEG C, then through pelleter pelletizing, After water cooling, dehydration, obtain tissue adhesion masterbatch.
Wherein, mass percent shared by polyethylene in tissue adhesion masterbatch, hydrated magnesium silicate and erucyl amide is: polyethylene 55%, Hydrated magnesium silicate 30%, erucyl amide 15%.
Embodiment 2
The production technology of tissue adhesion masterbatch, comprises the following steps:
(1) mixing
Polyethylene and hydrated magnesium silicate are joined stirrer for mixing 2min through screw(-type) feeder, then erucyl amide is joined Blender continues mixing 4min, after standing 1.5h, obtains spares;
(2) pelletize
Spares is joined in double screw extruder, fully extrudes after fusion at 50-110 DEG C, then through pelleter pelletizing, After water cooling, dehydration, obtain tissue adhesion masterbatch.
Wherein, mass percent shared by polyethylene in tissue adhesion masterbatch, hydrated magnesium silicate and erucyl amide is: polyethylene 60%, Hydrated magnesium silicate 20%, erucyl amide 20%.
Embodiment 3
The production technology of tissue adhesion masterbatch, comprises the following steps:
(1) mixing
Polyethylene and hydrated magnesium silicate are joined stirrer for mixing 4min through screw(-type) feeder, then erucyl amide is joined Blender continues mixing 6min, after standing 2.5h, obtains spares;
(2) pelletize
Spares is joined in double screw extruder, fully extrudes after fusion at 50-110 DEG C, then through pelleter pelletizing, After water cooling, dehydration, obtain tissue adhesion masterbatch.
Wherein, mass percent shared by polyethylene in tissue adhesion masterbatch, hydrated magnesium silicate and erucyl amide is: polyethylene 50%, Hydrated magnesium silicate 40%, erucyl amide 10%.

Claims (2)

1. the production technology of a tissue adhesion masterbatch, it is characterised in that: comprise the following steps:
(1) mixing
Polyethylene and hydrated magnesium silicate are joined stirrer for mixing 2-4min through screw(-type) feeder, then erucyl amide is added In blender, continue mixing 4-6min, after standing 1.5-2.5h, obtain spares;
(2) pelletize
Spares is joined in double screw extruder, fully extrudes after fusion at 50-110 DEG C, then through pelleter pelletizing, After water cooling, dehydration, obtain tissue adhesion masterbatch.
The production technology of tissue adhesion masterbatch the most according to claim 1, it is characterised in that: polyethylene in tissue adhesion masterbatch, Shared by hydrated magnesium silicate and erucyl amide, mass percent is: polyethylene 50-60%, hydrated magnesium silicate 20-40%, erucyl amide 10-20%.
CN201610305129.2A 2016-05-09 2016-05-09 Production process of anti-blocking master batch Pending CN105713284A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610305129.2A CN105713284A (en) 2016-05-09 2016-05-09 Production process of anti-blocking master batch

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610305129.2A CN105713284A (en) 2016-05-09 2016-05-09 Production process of anti-blocking master batch

Publications (1)

Publication Number Publication Date
CN105713284A true CN105713284A (en) 2016-06-29

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Family Applications (1)

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CN201610305129.2A Pending CN105713284A (en) 2016-05-09 2016-05-09 Production process of anti-blocking master batch

Country Status (1)

Country Link
CN (1) CN105713284A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112300544A (en) * 2020-10-05 2021-02-02 江苏双星彩塑新材料股份有限公司 Preparation method of functional master batch for polyester film

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103849033A (en) * 2012-12-04 2014-06-11 青岛三利中德美水设备有限公司 Polyethylene anti-blocking smooth master batch and preparation method thereof
CN103849026A (en) * 2012-12-04 2014-06-11 青岛三利中德美水设备有限公司 Antistatic smooth fiber-added polyethylene and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103849033A (en) * 2012-12-04 2014-06-11 青岛三利中德美水设备有限公司 Polyethylene anti-blocking smooth master batch and preparation method thereof
CN103849026A (en) * 2012-12-04 2014-06-11 青岛三利中德美水设备有限公司 Antistatic smooth fiber-added polyethylene and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
《合成树脂及塑料技术全书》编委会: "《合成树脂及塑料技术全书》", 30 April 2006, 中国石化出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112300544A (en) * 2020-10-05 2021-02-02 江苏双星彩塑新材料股份有限公司 Preparation method of functional master batch for polyester film

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Application publication date: 20160629

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