CN105698955A - Temperature detector for hydro-thermal synthesis reaction still - Google Patents

Temperature detector for hydro-thermal synthesis reaction still Download PDF

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Publication number
CN105698955A
CN105698955A CN201610165332.4A CN201610165332A CN105698955A CN 105698955 A CN105698955 A CN 105698955A CN 201610165332 A CN201610165332 A CN 201610165332A CN 105698955 A CN105698955 A CN 105698955A
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CN
China
Prior art keywords
signal
synthesis reaction
thermosensitive
comparator
signal comparator
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Pending
Application number
CN201610165332.4A
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Chinese (zh)
Inventor
许月进
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Individual
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Individual
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Priority to CN201610165332.4A priority Critical patent/CN105698955A/en
Publication of CN105698955A publication Critical patent/CN105698955A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01KMEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
    • G01K7/00Measuring temperature based on the use of electric or magnetic elements directly sensitive to heat ; Power supply therefor, e.g. using thermoelectric elements
    • G01K7/16Measuring temperature based on the use of electric or magnetic elements directly sensitive to heat ; Power supply therefor, e.g. using thermoelectric elements using resistive elements

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Measuring Or Testing Involving Enzymes Or Micro-Organisms (AREA)

Abstract

The invention discloses a temperature detector for a hydro-thermal synthesis reaction still. The detector comprises a signal comparator; and a first thermosensitive probe and a second thermosensitive probe are arranged at the two ends of the signal comparator and are connected with the signal comparator by signal amplifier respectively. One pair of signal output ports is arranged on the signal comparator. The first thermosensitive probe and the second thermosensitive probe are made from thermosensitive ferrite material; and the signal comparator is a zero-crossing voltage comparator. According to the detector, the two thermosensitive probes arranged on the body sense temperatures and resistances of the two thermosensitive probes change; and on the basis of amplification by the signal amplifiers and access of the signal comparator, the internal bridge can convert slight resistance changes of the thermosensitive probes into large signal outputs. Therefore, measurement precision of the temperature detector for the hydro-thermal synthesis reaction still is substantially improved.

Description

Hydrothermal synthesis reaction still still temperature detector
Technical field
The present invention relates to a kind of temperature detector, more precisely, be a kind of hydrothermal synthesis reaction still still temperature detector。
Background technology
Hydrothermal synthesis reaction still is a kind of hermetic container that can decompose indissoluble material。Can be used for the molten sample pretreatment during atomic absorption spectrum and plasma emission etc. are analyzed;Can also be used for the synthetic reaction of low dose;It is also with in tank body strong acid or highly basic and high temperature high pressure enclosed environment are to reach the purpose of rapid-digestion indissoluble material。The chemical analysis methods such as gas phase, liquid phase, plasma spectrum mass spectrum, Atomic Absorption and atomic fluorescence do sample pre-treatments。The competent assistant of sample is cleared up when being and measure trace element and trace element。Can apply in the determining heavy metals such as lead, copper, cadmium, zinc, calcium, manganese, ferrum, hydrargyrum, be alternatively arranged as the aspects such as the reaction vessel that a kind of high-temperature-resistant high-pressure-resistant anticorrosion is high-purity, and organic synthesis, Hydrothermal Synthesis, crystal growth or Specimen eliminating extraction。Clear up in sample pre-treatments that heavy metal, agriculture be residual, food, mud, rare earth, aquatic products, Organic substance etc.。Therefore, it is widely used in the research of the departments such as petrochemical industry, biomedicine, material science, geologic chemistry, environmental science, Food Science, commodity inspection and production。
The detection of still cavity temperature is particularly important by hydrothermal synthesis reaction still in actual applications, and higher temperature detecting precision can ensure that the course of reaction of higher quality。The certainty of measurement of the still temperature detector of the hydrothermal synthesis reaction still that current industry commonly uses is not high enough。
Summary of the invention
The present invention mainly solves the technical problem existing for prior art, thus providing a kind of hydrothermal synthesis reaction still still temperature detector with relatively high measurement accuracy。
The above-mentioned technical problem of the present invention is addressed mainly by following technical proposals:
A kind of hydrothermal synthesis reaction still still temperature detector, described detector comprises a signal comparator, the two ends of described signal comparator are provided with one first temperature sensitive probes and one second temperature sensitive probes, the first described temperature sensitive probes and the second temperature sensitive probes are respectively connected with described signal comparator by a signal amplifier, and described signal comparator is additionally provided with a pair signal output socket。
As preferred embodiment of the present invention, the first described temperature sensitive probes and the second temperature sensitive probes are made up of heat sensitive ferrite material。
As preferred embodiment of the present invention, described signal comparator is zero passage voltage comparator。
Owing to the hydrothermal synthesis reaction still still temperature detector of the present invention is by two temperature sensitive probes temperature sensors of setting on body, the resistance of the two temperature sensitive probes changes, access by the amplification of signal amplifier and signal comparator, the faint resistance variations of temperature sensitive probes can be changed into bigger signal output by internal electric bridge, thus substantially increasing the certainty of measurement of hydrothermal synthesis reaction still still temperature detector。
Accompanying drawing explanation
In order to be illustrated more clearly that the embodiment of the present invention or technical scheme of the prior art, the accompanying drawing used required in embodiment or description of the prior art will be briefly described below, apparently, accompanying drawing in the following describes is only some embodiments of the present invention, for those of ordinary skill in the art, under the premise not paying creative work, it is also possible to obtain other accompanying drawing according to these accompanying drawings。
Fig. 1 is the perspective view of the hydrothermal synthesis reaction still still temperature detector of the present invention;
Fig. 2 is the perspective view of the hydrothermal synthesis reaction still still temperature detector in Fig. 1, is now another visual angle。
Detailed description of the invention
Below in conjunction with accompanying drawing, the preferred embodiments of the present invention are described in detail, so that advantages and features of the invention can be easier to be readily appreciated by one skilled in the art, thus protection scope of the present invention being made apparent clear and definite defining。
The invention provides a kind of hydrothermal synthesis reaction still still temperature detector with relatively high measurement accuracy。
As shown in Figure 1 and Figure 2, a kind of hydrothermal synthesis reaction still still temperature detector 1, described detector comprises a signal comparator 2, the two ends of described signal comparator 2 are provided with one first temperature sensitive probes 31 and one second temperature sensitive probes 32, the first described temperature sensitive probes 31 is respectively connected with described signal comparator 2 by a signal amplifier 4 with the second temperature sensitive probes 32, and described signal comparator 2 is additionally provided with a pair signal output socket 5。
As shown in Figure 1 and Figure 2, the first described temperature sensitive probes 31 and the second temperature sensitive probes 32 are made up of heat sensitive ferrite material。
As shown in Figure 1 and Figure 2, described signal comparator 2 is zero passage voltage comparator。
The hydrothermal synthesis reaction still still temperature detector of this invention two temperature sensitive probes temperature sensors by arranging on body, the resistance of the two temperature sensitive probes changes, access by the amplification of signal amplifier and signal comparator, the faint resistance variations of temperature sensitive probes can be changed into bigger signal output by internal electric bridge, thus substantially increasing the certainty of measurement of hydrothermal synthesis reaction still still temperature detector。
The mentality of designing of the present invention is below only described in one embodiment, and when system allows, the present invention can expand to external more functional module simultaneously, thus extending its function to greatest extent。
The above, be only the specific embodiment of the present invention, but protection scope of the present invention be not limited thereto, any change expected without creative work or replacement, all should be encompassed within protection scope of the present invention。Therefore, protection scope of the present invention should be as the criterion with claims protection defined。

Claims (3)

1. hydrothermal synthesis reaction still still temperature detector (1), it is characterized in that, described detector comprises a signal comparator (2), the two ends of described signal comparator (2) are provided with one first temperature sensitive probes (31) and one second temperature sensitive probes (32), described the first temperature sensitive probes (31) is respectively connected with described signal comparator (2) by a signal amplifier (4) with the second temperature sensitive probes (32), and described signal comparator (2) is additionally provided with a pair signal output socket (5)。
2. hydrothermal synthesis reaction still still temperature detector according to claim 1, it is characterised in that described the first temperature sensitive probes (31) and the second temperature sensitive probes (32) are made up of heat sensitive ferrite material。
3. hydrothermal synthesis reaction still still temperature detector according to claim 2, it is characterised in that described signal comparator (2) is zero passage voltage comparator。
CN201610165332.4A 2016-03-19 2016-03-19 Temperature detector for hydro-thermal synthesis reaction still Pending CN105698955A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610165332.4A CN105698955A (en) 2016-03-19 2016-03-19 Temperature detector for hydro-thermal synthesis reaction still

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610165332.4A CN105698955A (en) 2016-03-19 2016-03-19 Temperature detector for hydro-thermal synthesis reaction still

Publications (1)

Publication Number Publication Date
CN105698955A true CN105698955A (en) 2016-06-22

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CN201610165332.4A Pending CN105698955A (en) 2016-03-19 2016-03-19 Temperature detector for hydro-thermal synthesis reaction still

Country Status (1)

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CN (1) CN105698955A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080144415A1 (en) * 2006-12-14 2008-06-19 Micron Technology, Inc. On-chip temperature sensor
CN102323316A (en) * 2011-08-16 2012-01-18 浙江大学 High-temperature high-pressure calibration device and calibration method of pH electrode
CN104307448A (en) * 2014-10-22 2015-01-28 常州市江南环保设备有限公司 Temperature detection device of reaction kettle
CN104655298A (en) * 2013-11-19 2015-05-27 陕西龙海工程建设有限公司 High-precision water temperature monitoring system
CN205580617U (en) * 2016-03-19 2016-09-14 许月进 Hydro -thermal synthesis reation kettle cauldron temperature detector

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080144415A1 (en) * 2006-12-14 2008-06-19 Micron Technology, Inc. On-chip temperature sensor
CN102323316A (en) * 2011-08-16 2012-01-18 浙江大学 High-temperature high-pressure calibration device and calibration method of pH electrode
CN104655298A (en) * 2013-11-19 2015-05-27 陕西龙海工程建设有限公司 High-precision water temperature monitoring system
CN104307448A (en) * 2014-10-22 2015-01-28 常州市江南环保设备有限公司 Temperature detection device of reaction kettle
CN205580617U (en) * 2016-03-19 2016-09-14 许月进 Hydro -thermal synthesis reation kettle cauldron temperature detector

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Application publication date: 20160622