CN105695063A - Electric appliance insulating oil prepared from paraffin oil - Google Patents

Electric appliance insulating oil prepared from paraffin oil Download PDF

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Publication number
CN105695063A
CN105695063A CN201610153447.1A CN201610153447A CN105695063A CN 105695063 A CN105695063 A CN 105695063A CN 201610153447 A CN201610153447 A CN 201610153447A CN 105695063 A CN105695063 A CN 105695063A
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CN
China
Prior art keywords
parts
oil
paraffin oil
electric appliance
sufficiently mixed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610153447.1A
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Chinese (zh)
Inventor
黄帮义
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Haydite Oil Chemical Co Ltd
Original Assignee
Anhui Haydite Oil Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Haydite Oil Chemical Co Ltd filed Critical Anhui Haydite Oil Chemical Co Ltd
Priority to CN201610153447.1A priority Critical patent/CN105695063A/en
Publication of CN105695063A publication Critical patent/CN105695063A/en
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06—Metal compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/10—Compounds containing silicon
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/10—Compounds containing silicon
    • C10M2201/102—Silicates
    • C10M2201/103—Clays; Mica; Zeolites
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
    • C10M2205/163—Paraffin waxes; Petrolatum, e.g. slack wax used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/20—Natural rubber; Natural resins
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C10M2207/402—Castor oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/102—Polyesters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/12—Polysaccharides, e.g. cellulose, biopolymers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/14—Electric or magnetic purposes
    • C10N2040/16—Dielectric; Insulating oil or insulators

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses electric appliance insulating oil prepared from paraffin oil and relates to the technical field of petro-chemical engineering. The electric appliance insulating oil is prepared from, by weight, 80-100 parts of the paraffin oil, 20-25 parts of castor oil, 15-20 parts of turpentine, 15-20 parts of terpene resin, 10-15 parts of hydrogenated rosin, 8-12 parts of polyester resin, 6-10 parts of sodium carboxymethylcellulose, 6-10 parts of methyl silicone oil, 5-8 parts of sodium bentonite, 4-7 parts of polyoxyethylene lauryl ether, 3-5 parts of zeolite powder, 3-5 parts of silica gel powder and 2-3 parts of nano-ceramics powder. The insulating oil is clear and transparent, small in viscosity at the low temperature and capable of achieving autoconvection in electric appliance and guiding out heat and excellent in antioxidation, is not changed at all under the action of an electric field for a long time, and is good in stability and novel electric appliance insulating oil.

Description

A kind of electrical apparatus insulation oil utilizing paraffin oil to prepare
Technical field:
The present invention relates to technical field of petrochemical industry, be specifically related to a kind of electrical apparatus insulation utilizing paraffin oil to prepare oil。
Background technology:
Electrical apparatus insulation oil is a kind of lubricating oil, is generally added antioxidant modulation by the lube base oil of deep refining and forms, is mainly used as the electrolyte of electric equipment。The main performance of electrical apparatus insulation oil is cryogenic property, oxidation stability and dielectric loss。At present, the electrical apparatus insulation oil used oil based on naphthene base crude oil mostly, although its performance can substantially meet instructions for use, but production cost is higher, thus improving commercially available price。
Summary of the invention:
The technical problem to be solved is in that to provide a kind of electrical apparatus insulation utilizing paraffin oil to prepare with low cost, excellent performance oily。
The technical problem to be solved adopts following technical scheme to realize:
A kind of electrical apparatus insulation oil utilizing paraffin oil to prepare, is made up of the raw material of following parts by weight:
Paraffin oil 80-100 part, Oleum Ricini 20-25 part, Oleum Terebinthinae 15-20 part, terpene resin 15-20 part, hydrogenated rosin 10-15 part, polyester resin 8-12 part, sodium carboxymethyl cellulose 6-10 part, methyl-silicone oil 6-10 part, sodium bentonite 5-8 part, polyoxyethylene lauryl ether 4-7 part, zeolite powder 3-5 part, silica white 3-5 part, nano-ceramic powder 2-3 part。
Its preparation method comprises the steps:
(1) adding in Oleum Terebinthinae by hydrogenated rosin, heating adds sodium bentonite and zeolite powder after being completely dissolved, and is sufficiently mixed post-heating to 100-110 DEG C of insulation mixing 15min, obtains material I；
(2) in paraffin oil, terpene resin and polyoxyethylene lauryl ether are added, after mix homogeneously under microwave frequency 2450MHz, power 800W microwave treatment 10min, supersound process 15min under supersonic frequency 40kHz, power 100W, it is subsequently adding polyester resin and silica white, at 0-5 DEG C, stand 1h after being sufficiently mixed, obtain material II；
(3) in material II, add material I, Oleum Ricini, sodium carboxymethyl cellulose, methyl-silicone oil and nano-ceramic powder, be sufficiently mixed uniformly。
The invention has the beneficial effects as follows: the present invention is with paraffin oil for primary raw material, it is aided with the multiple auxiliary agents such as Oleum Ricini, Oleum Terebinthinae and terpene resin and prepares electrical apparatus insulation oil, this insulating oil is clear and bright bright, during low temperature, viscosity is less, can in electric equipment automatic convection current and derive heat, and have excellence non-oxidizability, any change will not be there is under long-time electric field action, good stability, is a kind of Novel electric appliance insulating oil。
Detailed description of the invention:
For the technological means making the present invention realize, creation characteristic, reach purpose and effect and be easy to understand, below in conjunction with specific embodiment, the present invention is expanded on further。
Embodiment 1
(1) adding in 15 parts of Oleum Terebinthinaes by 10 parts of hydrogenated rosins, heating adds 6 parts of sodium bentonites and 3 parts of zeolite powders after being completely dissolved, and is sufficiently mixed post-heating to 100-110 DEG C of insulation mixing 15min, obtains material I；
(2) in 90 parts of paraffin oil, 15 parts of terpene resins and 5 parts of polyoxyethylene lauryl ether are added, after mix homogeneously under microwave frequency 2450MHz, power 800W microwave treatment 10min, supersound process 15min under supersonic frequency 40kHz, power 100W, it is subsequently adding 12 parts of polyester resin and 3 parts of silica whites, at 0-5 DEG C, stand 1h after being sufficiently mixed, obtain material II；
(3) in material II, add material I, 20 parts of Oleum Ricini, 8 parts of sodium carboxymethyl cellulose, 8 parts of methyl-silicone oils and 2 parts of nano-ceramic powders, be sufficiently mixed uniformly。
Embodiment 2
(1) adding in 20 parts of Oleum Terebinthinaes by 15 parts of hydrogenated rosins, heating adds 8 parts of sodium bentonites and 4 parts of zeolite powders after being completely dissolved, and is sufficiently mixed post-heating to 100-110 DEG C of insulation mixing 15min, obtains material I；
(2) in 100 parts of paraffin oil, 20 parts of terpene resins and 7 parts of polyoxyethylene lauryl ether are added, after mix homogeneously under microwave frequency 2450MHz, power 800W microwave treatment 10min, supersound process 15min under supersonic frequency 40kHz, power 100W, it is subsequently adding 10 parts of polyester resin and 5 parts of silica whites, at 0-5 DEG C, stand 1h after being sufficiently mixed, obtain material II；
(3) in material II, add material I, 25 parts of Oleum Ricini, 10 parts of sodium carboxymethyl cellulose, 6 parts of methyl-silicone oils and 3 parts of nano-ceramic powders, be sufficiently mixed uniformly。
The ultimate principle of the present invention and principal character and advantages of the present invention have more than been shown and described。Skilled person will appreciate that of the industry; the present invention is not restricted to the described embodiments; described in above-described embodiment and description is that principles of the invention is described; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements both fall within the claimed scope of the invention。Claimed scope is defined by appending claims and equivalent thereof。

Claims (2)

1. the electrical apparatus insulation oil that one kind utilizes paraffin oil to prepare, it is characterised in that be made up of the raw material of following parts by weight:
Paraffin oil 80-100 part, Oleum Ricini 20-25 part, Oleum Terebinthinae 15-20 part, terpene resin 15-20 part, hydrogenated rosin 10-15 part, polyester resin 8-12 part, sodium carboxymethyl cellulose 6-10 part, methyl-silicone oil 6-10 part, sodium bentonite 5-8 part, polyoxyethylene lauryl ether 4-7 part, zeolite powder 3-5 part, silica white 3-5 part, nano-ceramic powder 2-3 part。
2. the electrical apparatus insulation oil utilizing paraffin oil to prepare according to claim 1, it is characterised in that its preparation method comprises the steps:
(1) adding in Oleum Terebinthinae by hydrogenated rosin, heating adds sodium bentonite and zeolite powder after being completely dissolved, and is sufficiently mixed post-heating to 100-110 DEG C of insulation mixing 15min, obtains material I；
(2) in paraffin oil, terpene resin and polyoxyethylene lauryl ether are added, after mix homogeneously under microwave frequency 2450MHz, power 800W microwave treatment 10min, supersound process 15min under supersonic frequency 40kHz, power 100W, it is subsequently adding polyester resin and silica white, at 0-5 DEG C, stand 1h after being sufficiently mixed, obtain material II；
(3) in material II, add material I, Oleum Ricini, sodium carboxymethyl cellulose, methyl-silicone oil and nano-ceramic powder, be sufficiently mixed uniformly。
CN201610153447.1A 2016-03-16 2016-03-16 Electric appliance insulating oil prepared from paraffin oil Pending CN105695063A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610153447.1A CN105695063A (en) 2016-03-16 2016-03-16 Electric appliance insulating oil prepared from paraffin oil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610153447.1A CN105695063A (en) 2016-03-16 2016-03-16 Electric appliance insulating oil prepared from paraffin oil

Publications (1)

Publication Number Publication Date
CN105695063A true CN105695063A (en) 2016-06-22

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Country Status (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106298241A (en) * 2016-10-09 2017-01-04 安徽四新电子有限责任公司 A kind of high-voltage pulse capacitor
CN113549482A (en) * 2021-06-09 2021-10-26 广西大学 Low-conductivity olive insulating oil modified by nanocellulose and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104130827A (en) * 2014-07-02 2014-11-05 马鞍山市万鑫铸造有限公司 Aluminium nitride-titanium oxide nanoparticle transformer oil with high anti-corrosion property and preparation method thereof
CN104130830A (en) * 2014-07-02 2014-11-05 马鞍山市万鑫铸造有限公司 Suspension-stabilizer-added nanometer aluminium-nitride transformer oil and preparation method thereof
CN104194885A (en) * 2014-08-13 2014-12-10 铜陵日科电子有限责任公司 Transformer oil containing lanthanum oxide-aluminum nitride nano-particles and preparation method of transformer oil
CN105296102A (en) * 2015-10-22 2016-02-03 铜陵三佳变压器有限责任公司 Transformer oil with high corrosion resistance

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104130827A (en) * 2014-07-02 2014-11-05 马鞍山市万鑫铸造有限公司 Aluminium nitride-titanium oxide nanoparticle transformer oil with high anti-corrosion property and preparation method thereof
CN104130830A (en) * 2014-07-02 2014-11-05 马鞍山市万鑫铸造有限公司 Suspension-stabilizer-added nanometer aluminium-nitride transformer oil and preparation method thereof
CN104194885A (en) * 2014-08-13 2014-12-10 铜陵日科电子有限责任公司 Transformer oil containing lanthanum oxide-aluminum nitride nano-particles and preparation method of transformer oil
CN105296102A (en) * 2015-10-22 2016-02-03 铜陵三佳变压器有限责任公司 Transformer oil with high corrosion resistance

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Title
华东电力试验研究院、科学技术信息所编: "《国外高压输变电设备绝缘运行经验专辑》", 31 January 1996, 华东电力试验研究院 *
咸日常: "《电力变压器运行与维修》", 31 August 2014, 中国电力出版社 *
石敬炜: "《电气工程常用公式与数据速查手册》", 31 January 2015, 知识产权出版社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106298241A (en) * 2016-10-09 2017-01-04 安徽四新电子有限责任公司 A kind of high-voltage pulse capacitor
CN106298241B (en) * 2016-10-09 2018-07-24 安徽四新电子有限责任公司 A kind of high-voltage pulse capacitor
CN113549482A (en) * 2021-06-09 2021-10-26 广西大学 Low-conductivity olive insulating oil modified by nanocellulose and preparation method thereof

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Application publication date: 20160622