CN105672000A - Mending agent and preparation method thereof - Google Patents
Mending agent and preparation method thereof Download PDFInfo
- Publication number
- CN105672000A CN105672000A CN201610032078.0A CN201610032078A CN105672000A CN 105672000 A CN105672000 A CN 105672000A CN 201610032078 A CN201610032078 A CN 201610032078A CN 105672000 A CN105672000 A CN 105672000A
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- parts
- fixed
- storage box
- healant
- mixing drum
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- 238000002360 preparation method Methods 0.000 title abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000000463 material Substances 0.000 claims abstract description 25
- -1 benzyl ester Chemical class 0.000 claims abstract description 15
- 239000008367 deionised water Substances 0.000 claims abstract description 15
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 15
- 150000002148 esters Chemical class 0.000 claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 claims abstract description 15
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 15
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000003860 storage Methods 0.000 claims description 40
- 238000002156 mixing Methods 0.000 claims description 31
- 238000003756 stirring Methods 0.000 claims description 27
- 230000007246 mechanism Effects 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 17
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 14
- 238000005070 sampling Methods 0.000 claims description 14
- 230000003028 elevating effect Effects 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 3
- 239000011521 glass Substances 0.000 claims description 3
- 238000005304 joining Methods 0.000 claims description 3
- 230000008901 benefit Effects 0.000 abstract description 3
- 229920000728 polyester Polymers 0.000 abstract description 2
- 239000003795 chemical substances by application Substances 0.000 abstract 4
- 150000001412 amines Chemical class 0.000 abstract 1
- 239000000975 dye Substances 0.000 description 8
- 238000004043 dyeing Methods 0.000 description 7
- 239000004753 textile Substances 0.000 description 4
- 230000007547 defect Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000008439 repair process Effects 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 229920004933 Terylene® Polymers 0.000 description 2
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 229960002903 benzyl benzoate Drugs 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- JBSLOWBPDRZSMB-FPLPWBNLSA-N dibutyl (z)-but-2-enedioate Chemical compound CCCCOC(=O)\C=C/C(=O)OCCCC JBSLOWBPDRZSMB-FPLPWBNLSA-N 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/11—Stirrers characterised by the configuration of the stirrers
- B01F27/112—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
- D06P1/613—Polyethers without nitrogen
- D06P1/6138—Polymerisation products of glycols, e.g. Carbowax, Pluronics
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatment Of Fiber Materials (AREA)
Abstract
The invention provides a mending agent and a preparation method thereof, aiming at solving the technical problems that an existing mending agent can be used for polyester materials only, is single in function, lacks manufacturing methods and the like.The mending agent comprises, by weight, 20-70 parts of benzyl ester, 10-30 parts of dibutyl ester, 20-50 parts of ethanol, 5-20 parts of fatty amine polyoxyethylene ether and 10-30 parts of deionized water.The mending agent has the advantages of high practicality and high preparation efficiency.
Description
Technical field
The invention belongs to textile dyeing and finishing technical field, relate to healant and preparation method thereof.
Background technology
Conventional weaving face fabric is processed through dyeing and finishing technology flow process, can produce various dye defect. Wherein uneven dyeing is the most normal produced problem, needs dyeing and finishing again, causes certain environmental protection impact to environment. Healant is a kind of surfactant blend, has shifting dye ability and the through-dyeing of excellence, promotes the dyestuff on fabric to shift from high concentration to low concentration under high-temperature and high-pressure conditions, makes colouring everywhere on fiber tend to uniformly reach the purpose that color flower is repaired.
Through retrieval, as Chinese patent literature discloses a kind of environment-friendly type terylene dyeing healant [application number: 201310261989.7; Publication number: CN103343461A]. This environment-friendly type terylene dyeing healant, is prepared from by following raw material: benzyl benzoate 45-55 weight portion, dibutyl maleate 20-25 weight portion, isomery ten alcohol ether phosphate 15-25 weight portion, tween 80 5-10 weight portion.
Although the healant disclosed in this patent is especially advantageous for environmental protection, but, this healant can only only for polyester material, use single, and there is no manufacture method, therefore, it is necessary for designing a kind of healant and preparation method thereof.
Summary of the invention
First purpose of the present invention is to there are the problems referred to above for existing technology, it is proposed that a kind of healant, this healant has practical feature.
First purpose of the present invention can be realized by following technical proposal: healant, it is characterized in that, be made up of the component of following weight portion: benzyl ester 20～70 parts, dibutyl ester 10～30 parts, ethanol 20～50 parts, aliphatic amine polyoxyethylene ether 5～20 parts and deionized water 10～30 parts.
Adopt above component, by with benzyl ester, dibutyl ester for main component, add again ethanol, aliphatic amine polyoxyethylene ether and deionized water wherein, make it have excellent shifting dye, return something for repairs and the performance such as repairing, dye defect can be prevented and promote Color, the repairing of all kinds of textile can be applied to, practical.
The weight portion of described each component is as follows: benzyl ester 45, dibutyl ester 20 parts, ethanol 35 parts, aliphatic amine polyoxyethylene ether 12 parts and deionized water 20 parts.
Adopting above component, can reach the serviceability of the best, component is reasonable.
Second purpose of the present invention is to there are the problems referred to above for existing technology, it is proposed that the manufacture method of a kind of healant, this manufacture method has the advantages that make efficiency is high.
Second purpose of the present invention can be realized by following technical proposal: the manufacture method of healant, it is characterised in that comprise the steps:
A, joining in agitating device by deionized water, add ethanol while stirring, stirring is to mix homogeneously, and speed of agitator is 200～250r/min;
B, being separately added into benzyl ester, dibutyl ester and aliphatic amine polyoxyethylene ether in the step a solution prepared, heat while stirring to 52～54 DEG C, speed of agitator is 150～200r/min, stirs and is uniformly dispersed to solution, stands cooling, obtain healant.
Adopting above method, can quickly be mixed by various materials by agitating device, meanwhile, by sampling the effect that can quickly detect stirring, make efficiency is high.
Described agitating device in step a and b, including frame, frame is fixed with mixing drum, mixing drum is provided with shaft, shaft upper end can drive the actuating unit of its rotation to be connected with one, shaft lower end is stretched in mixing drum and is fixed with stirring vane, frame is provided with the sampling mechanism that can material in mixing drum be sampled, sampling mechanism includes storage box, suction pipe, first electromagnetic valve, delivery pump and controller, storage box can drive the elevating mechanism of its oscilaltion to be arranged in frame by one, and storage box can be in mixing drum, suction pipe one end is connected with storage box top, the suction pipe other end can be connected with the external world, first electromagnetic valve and delivery pump are arranged in suction pipe, controller is fixed in frame, first electromagnetic valve is all connected with this controller with delivery pump.
The operation principle of this agitating device is as follows: joined by material in mixing drum, shaft is driven to rotate by actuating unit, shaft drives stirring vane to rotate, rotation along with stirring vane, material stirring is uniform, storage box is driven to move down by elevating mechanism, it is in mixing drum, control the first electromagnetic valve by controller to be in and open shape body, control delivery pump work, material in mixing drum is transported in storage box by suction pipe by delivery pump, it may be achieved sampling operation, sampling is easily and fast.
Described elevating mechanism includes push-rod electric machine, slide block, guide rail, installing plate and support, support is fixed in frame, guide rail is vertically fixed on support, slide block is arranged on guide rail, push-rod electric machine is fixed on support, and the push rod of push-rod electric machine is arranged straight down, and the push rod end of push-rod electric machine is connected with slide block, installing plate is fixed on slide block, and storage box is fixing on a mounting board by connecting rod.
When needs make storage box move up and down, the push rod controlling push-rod electric machine moves up and down, the push rod band movable slider of push-rod electric machine moves up and down along guide rail, slide block drives installing plate to move up and down, installing plate drivening rod moves up and down, connecting rod drives storage box to move up and down, thus storage box can be made to move up and down.
Being additionally provided with indicating mechanism in described frame, indicating mechanism includes measuring bar and pointer, measures that bar is vertically fixing to be measured and has graduation mark on bar on a mounting board, and pointer is fixed on support, and pointer is towards the graduation mark measuring bar.
Adopt above structure, measured the graduation mark of bar by pointer instruction, can rapid examination to storage box location, observe directly perceived, conveniently.
Described actuating unit includes motor, active synchronization wheel, driven synchronizing wheel and Timing Belt, motor is arranged on mixing drum, the output shaft of motor sets up, active synchronization wheel is fixed on the output shaft of motor, driven synchronizing wheel is fixed on shaft, and Timing Belt is arranged between active synchronization wheel and driven synchronizing wheel.
When needs make shaft rotate, controlling the output shaft rotation of motor, the output shaft of motor drives active synchronization wheel to rotate, and active synchronization wheel drives driven synchronizing wheel by Timing Belt, driven synchronizing wheel drives shaft to rotate, thus shaft can be made to rotate.
Having cushion between described motor and mixing drum, the material of cushion is rubber.
Adopt above structure, can reduce, by cushion, the vibration that motor produces, use noise little.
Also being vertically arranged with delivery pipe on described storage box, delivery pipe one end is connected with storage box bottom, and the delivery pipe other end can be connected with the external world, is additionally provided with the second electromagnetic valve in delivery pipe.
When needing to take out the material in storage box, controlling the second electromagnetic valve and be in open mode, material under gravity, transports out, rapid operation in delivery pipe.
The material of described storage box is transparent glass.
Adopt above material, the working condition in storage box can be observed directly.
Compared with prior art, this healant and preparation method thereof has the advantage that
1, by with benzyl ester, dibutyl ester for main component in this healant, add again ethanol, aliphatic amine polyoxyethylene ether and deionized water wherein, make it have excellent shifting dye, return something for repairs and the performance such as repairing, it is possible to be applied to the repairing of all kinds of textile, practical.
2, can quickly being mixed by various materials by agitating device in this manufacture method, meanwhile, by sampling the effect that can quickly detect stirring, make efficiency is high.
3, driving storage box to move down by push-rod electric machine in this agitating device so that it is being in mixing drum, the material in mixing drum is transported in storage box by suction pipe by delivery pump, sampling is easily and fast.
4, measured the graduation mark of bar by pointer instruction, can rapid examination to storage box location, observe intuitively.
5, can reduce, by cushion, the vibration that motor produces, use noise little.
Accompanying drawing explanation
Fig. 1 is the planar structure schematic diagram of this agitating device.
Fig. 2 is the planar structure schematic diagram that this agitating device removes part.
In figure, 1, frame; 2, stirring vane; 3, shaft; 4, mixing drum; 5, support; 6, pointer; 7, bar is measured; 7a, graduation mark; 8, guide rail; 9, slide block; 10, push-rod electric machine; 11, installing plate; 12, connecting rod; 13, storage box; 14, driven synchronizing wheel; 15, Timing Belt; 16, active synchronization wheel; 17, motor; 18, cushion; 19, controller; 20, delivery pump; 21, suction pipe; 22, the first electromagnetic valve; 23, the second electromagnetic valve; 24, delivery pipe.
Detailed description of the invention
The following is specific embodiments of the invention and in conjunction with accompanying drawing, technical scheme is further described, but the present invention is not limited to these embodiments.
This healant, is made up of the component of following weight portion: benzyl ester 20～70 parts, dibutyl ester 10～30 parts, ethanol 20～50 parts, aliphatic amine polyoxyethylene ether 5～20 parts and deionized water 10～30 parts; Adopt this component, by with benzyl ester, dibutyl ester for main component, add again ethanol, aliphatic amine polyoxyethylene ether and deionized water wherein, make it have excellent shifting dye, return something for repairs and the performance such as repairing, dye defect can be prevented and promote Color, the repairing of all kinds of textile can be applied to, practical.
The weight portion of each component is as follows: benzyl ester 45, dibutyl ester 20 parts, ethanol 35 parts, aliphatic amine polyoxyethylene ether 12 parts and deionized water 20 parts, adopts this component, can reach the serviceability of the best, and component is reasonable; It is of course also possible to adopt this kind of embodiment, the weight portion of each component is as follows: benzyl ester 20 parts, dibutyl ester 10 parts, ethanol 20 parts, aliphatic amine polyoxyethylene ether 5 parts and deionized water 10 parts;Separately planting embodiment it is of course also possible to adopt, the weight portion of each component is as follows: benzyl ester 70 parts, dibutyl ester 30 parts, ethanol 50 parts, aliphatic amine polyoxyethylene ether 20 parts and deionized water 30 parts; In the present embodiment, every part is 100 grams.
The manufacture method of this healant, comprises the steps:
A, joining in agitating device by deionized water, add ethanol while stirring, stirring is to mix homogeneously, and speed of agitator is 200～250r/min; In the present embodiment, speed of agitator is 230r/min;
B, in the step a solution prepared, it is separately added into benzyl ester, dibutyl ester and aliphatic amine polyoxyethylene ether heats while stirring to 52～54 DEG C, speed of agitator is 150～200r/min, stirring to solution is uniformly dispersed, stand cooling, obtain healant, in the present embodiment, heating while stirring to 53 DEG C, speed of agitator is 180r/min.
Adopting the method, can quickly be mixed by various materials by agitating device, meanwhile, by sampling the effect that can quickly detect stirring, make efficiency is high.
As shown in Figure 1 and Figure 2, the agitating device in step a and b, including frame 1, frame 1 is fixed with mixing drum 4, the mode that frame 1 is bolted is fixed with mixing drum 4, being provided with shaft 3 on mixing drum 4, shaft 3 upper end can drive the actuating unit of its rotation to be connected with one, and shaft 3 lower end is stretched in mixing drum 4 and fixed with stirring vane 2, and mode and stirring vane 2 that the lower end of shaft 3 is bolted fix, frame 1 is provided with the sampling mechanism that can material in mixing drum 4 be sampled, sampling mechanism includes storage box 13, suction pipe the 21, first electromagnetic valve 22, delivery pump 20 and controller 19, the material of storage box 13 is transparent glass, adopt this material, the working condition in storage box 13 can be observed directly, storage box 13 can drive the elevating mechanism of its oscilaltion to be arranged in frame 1 by one, and storage box 13 can be in mixing drum 4, suction pipe 21 one end is connected with storage box 13 top, suction pipe 21 other end can be connected with the external world, first electromagnetic valve 22 and delivery pump 20 are arranged in suction pipe 21, controller 19 is fixed in frame 1, first electromagnetic valve 22 is all connected with this controller 19 with delivery pump 20, in the present embodiment, controller 19 adopts the single-chip microcomputer being commercially available on market, the program of Single-chip Controlling pump and electromagnetic valve is existing, its program need not update.
As shown in Figure 1 and Figure 2, elevating mechanism includes push-rod electric machine 10, slide block 9, guide rail 8, installing plate 11 and support 5, and support 5 is fixed in frame 1, and the mode that support 5 is bolted is fixed in frame 1; Guide rail 8 is vertically fixed on support 5, and the mode that guide rail 8 is bolted is fixed on support 5; Slide block 9 is arranged on guide rail 8, and slide block 9 can move up and down along guide rail 8; Push-rod electric machine 10 is fixed on support 5, and the mode that push-rod electric machine 10 is bolted is fixed on support 5; The push rod of push-rod electric machine 10 is arranged straight down, and the push rod end of push-rod electric machine 10 is connected with slide block 9, and the mode that the push rod end of push-rod electric machine 10 is bolted is connected with slide block 9; Installing plate 11 is fixed on slide block 9, and the mode that installing plate 11 is bolted is fixed on slide block 9; Storage box 13 is fixed on installing plate 11 by connecting rod 12.
As shown in Figure 1 and Figure 2, frame 1 being additionally provided with indicating mechanism, indicating mechanism includes measuring bar 7 and pointer 6, measures bar 7 and is vertically fixed on installing plate 11, and the mode that measurement bar 7 is bolted is fixed on installing plate 11;Measuring and have graduation mark 7a on bar 7, pointer 6 is fixed on support 5, and the mode that pointer 6 is bolted is fixed on support 5; And pointer 6 towards measure bar 7 graduation mark 7a; Adopt this structure, measured the graduation mark 7a of bar 7 by pointer 6 instruction, can rapid examination to storage box 13 location, observe directly perceived, conveniently.
As shown in Figure 1, actuating unit includes motor 17, active synchronization wheel 16, driven synchronizing wheel 14 and Timing Belt 15, motor 17 is arranged on mixing drum 4, the output shaft of motor 17 sets up, active synchronization wheel 16 is fixed on the output shaft of motor 17, and the mode that active synchronization wheel 16 is connected by key is fixed on the output shaft of motor 17; Driven synchronizing wheel 14 is fixed on shaft 3, and driven synchronizing wheel 14 is fixed on shaft 3 by the mode that key connects; Timing Belt 15 is arranged between active synchronization wheel 16 and driven synchronizing wheel 14; Having cushion 18 between motor 17 and mixing drum 4, the material of cushion 18 is rubber, adopts this structure, can reduce, by cushion 18, the vibration that motor 17 produces, and uses noise little.
As shown in Figure 1 and Figure 2, storage box 13 being also vertically arranged with delivery pipe 24, delivery pipe 24 one end is connected with storage box 13 bottom, and delivery pipe 24 other end can be connected with the external world, is additionally provided with the second electromagnetic valve 23 in delivery pipe 24.
The operation principle of this agitating device is as follows: joined by material in mixing drum 4, control the output shaft rotation of motor 17, the output shaft of motor 17 drives active synchronization wheel 16 rotation, active synchronization wheel 16 drives driven synchronizing wheel 14 by Timing Belt 15, driven synchronizing wheel 14 drives shaft 3 to rotate, shaft 3 drives stirring vane 2 to rotate, along with the rotation of stirring vane 2, material stirring is uniform; The push rod controlling push-rod electric machine 10 moves down, the push rod band movable slider 9 of push-rod electric machine 10 moves down along guide rail 8, slide block 9 drives installing plate 11 to move down, installing plate 11 drivening rod 12 moves down, connecting rod 12 drives storage box 13 to move down, it is in mixing drum 4, control the first electromagnetic valve 22 by controller 19 to be in and open shape body, control delivery pump 20 to work, material in mixing drum 4 is transported in storage box 13 by suction pipe 21 by delivery pump 20, can realizing sampling operation, sampling is easily and fast.
Specific embodiment described herein is only to present invention spirit explanation for example. Described specific embodiment can be made various amendment or supplements or adopt similar mode to substitute by those skilled in the art, but without departing from the spirit of the present invention or surmount the scope that appended claims is defined.
Claims (10)
1. healant, it is characterised in that be made up of the component of following weight portion: benzyl ester 20～70 parts, dibutyl ester 10～30 parts, ethanol 20～50 parts, aliphatic amine polyoxyethylene ether 5～20 parts and deionized water 10～30 parts.
2. healant according to claim 1, it is characterised in that the weight portion of described each component is as follows: benzyl ester 45, dibutyl ester 20 parts, ethanol 35 parts, aliphatic amine polyoxyethylene ether 12 parts and deionized water 20 parts.
3. the healant according to the claims 1～2 any one, it is characterised in that the manufacture method of healant comprises the steps:
A, joining in agitating device by deionized water, add ethanol while stirring, stirring is to mix homogeneously, and speed of agitator is 200～250r/min;
B, being separately added into benzyl ester, dibutyl ester and aliphatic amine polyoxyethylene ether in the step a solution prepared, heat while stirring to 52～54 DEG C, speed of agitator is 150～200r/min, stirs and is uniformly dispersed to solution, stands cooling, obtain healant.
4. the manufacture method of healant according to claim 3, it is characterized in that, described agitating device in step a and b, including frame, frame is fixed with mixing drum, mixing drum is provided with shaft, shaft upper end can drive the actuating unit of its rotation to be connected with one, shaft lower end is stretched in mixing drum and is fixed with stirring vane, frame is provided with the sampling mechanism that can material in mixing drum be sampled, sampling mechanism includes storage box, suction pipe, first electromagnetic valve, delivery pump and controller, storage box can drive the elevating mechanism of its oscilaltion to be arranged in frame by one, and storage box can be in mixing drum, suction pipe one end is connected with storage box top, the suction pipe other end can be connected with the external world, first electromagnetic valve and delivery pump are arranged in suction pipe, controller is fixed in frame, first electromagnetic valve is all connected with this controller with delivery pump.
5. the manufacture method of healant according to claim 4, it is characterized in that, described elevating mechanism includes push-rod electric machine, slide block, guide rail, installing plate and support, and support is fixed in frame, and guide rail is vertically fixed on support, slide block is arranged on guide rail, push-rod electric machine is fixed on support, and the push rod of push-rod electric machine is arranged straight down, and the push rod end of push-rod electric machine is connected with slide block, installing plate is fixed on slide block, and storage box is fixing on a mounting board by connecting rod.
6. the manufacture method of healant according to claim 5, it is characterized in that, described frame is additionally provided with indicating mechanism, indicating mechanism includes measuring bar and pointer, measure bar vertically to fix on a mounting board, measuring on bar and have graduation mark, pointer is fixed on support, and pointer is towards the graduation mark measuring bar.
7. the manufacture method of healant according to claim 4, it is characterized in that, described actuating unit includes motor, active synchronization wheel, driven synchronizing wheel and Timing Belt, motor is arranged on mixing drum, the output shaft of motor sets up, active synchronization wheel is fixed on the output shaft of motor, and driven synchronizing wheel is fixed on shaft, and Timing Belt is arranged between active synchronization wheel and driven synchronizing wheel.
8. the manufacture method of healant according to claim 7, it is characterised in that have cushion between described motor and mixing drum, the material of cushion is rubber.
9. the manufacture method of healant according to claim 4, it is characterized in that, described storage box is also vertically arranged with delivery pipe, and delivery pipe one end is connected with storage box bottom, the delivery pipe other end can be connected with the external world, is additionally provided with the second electromagnetic valve in delivery pipe.
10. the manufacture method of healant according to claim 4, it is characterised in that the material of described storage box is transparent glass.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610032078.0A CN105672000B (en) | 2016-01-18 | 2016-01-18 | Healant and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610032078.0A CN105672000B (en) | 2016-01-18 | 2016-01-18 | Healant and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105672000A true CN105672000A (en) | 2016-06-15 |
| CN105672000B CN105672000B (en) | 2017-09-05 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610032078.0A Active CN105672000B (en) | 2016-01-18 | 2016-01-18 | Healant and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105672000B (en) |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
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| CN105672000B (en) | 2017-09-05 |
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