CN105648636A - Blended yarn multifunctional fabric and making method thereof - Google Patents
Blended yarn multifunctional fabric and making method thereof Download PDFInfo
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- CN105648636A CN105648636A CN201610108906.4A CN201610108906A CN105648636A CN 105648636 A CN105648636 A CN 105648636A CN 201610108906 A CN201610108906 A CN 201610108906A CN 105648636 A CN105648636 A CN 105648636A
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
- D03D15/56—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads elastic
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2101/00—Inorganic fibres
- D10B2101/10—Inorganic fibres based on non-oxides other than metals
- D10B2101/12—Carbon; Pitch
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2101/00—Inorganic fibres
- D10B2101/20—Metallic fibres
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
- D10B2201/08—Ramie
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/10—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyurethanes
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
- Woven Fabrics (AREA)
Abstract
The invention relates to a blended yarn multifunctional fabric and a making method thereof, and belongs to the technical field of spinning engineering. Warp of the fabric is blended yarn spun by adopting spandex silk as a yarn core and wrapping the yarn core by stainless steel fibers, copper fibers and carbon fibers. Weft of the fabric is blended yarn spun by adopting spandex silk as a yarn core and wrapping the yarn core by stainless steel fibers, natural bamboo fibers and ramie. The content of the stainless steel fibers in the warp ranges from 5% to 10%, the content of the copper fibers in the warp ranges from 2% to 5%, the content of the carbon fibers in the warp ranges from 2% to 5%, and the content of the spandex silk in the warp ranges from 80% to 91%. The content of the stainless steel fibers in the weft ranges from 3% to 10%, the content of the natural bamboo fibers in the weft ranges from 3% to 8%, the content of the ramie in the weft ranges from 3% to 8%, and the content of the spandex silk in the weft ranges from 74% to 91%. The fabric has the environmental protection property and functionality on the aspects of bacteria resistance and bacteriostasis, moisture absorption and quick drying, biodegradation and the like, and has good strength, elasticity, tear resistance and tenacity, and a good radiation protection and shielding effect is further achieved. The cloth face is flat, soft and smooth, the radiation protection efficiency reaches 92% or above, the moisture regain ranges from 8% to 10%, and the fiber bacteriostasis rate is larger than or equal to 91%.
Description
Technical field
The present invention relates to a kind of mixed yarn multifunctional fabric and preparation method thereof, belong to spinning engineering technical field.
Background technology
Mixed yarn is the yarn being spun into by two or more fiber, such as fiber crops/cotton, hair/cotton, hair/fiber crops/thin,tough silk, polyester cotton, wash/hair etc., break the boundary between original cotton, fiber crops, hair, silk, chemical fibre, the deficiency of certain textile material single can be made up, embody the superiority of each component fibre, to improve the einnehmen function of fabric, expand the scope of application. But existing mixed yarn multifunctional fabric function is comparatively single, complete not enough.
Summary of the invention
The present invention is directed to the defect existing for prior art, it is provided that one has better radioprotective usefulness, bacteriostasis antibiosis effect, there is fabulous elastic mixed yarn multifunctional fabric simultaneously.
The above-mentioned purpose of the present invention can be carried out by the following technical programs: a kind of mixed yarn multifunctional fabric, the warp thread of described fabric is with spandex thread for yarn core, the mixed yarn that stainless steel outer packed fiber, copper fiber, carbon fiber are spun into, the weft yarn of described fabric is with spandex thread for yarn core, the mixed yarn that stainless steel outer packed fiber, bamboo fiber, ramee are spun into.
The present invention with spandex thread for yarn core, the specific composite fibre of outsourcing, make fabric have higher elasticity, when putting on the two ends of one section of spandex core-spun yarn with spinning tension, outer layer fiber is in tension, and yarn is in straight configuration; When tension force increases again, outer layer fiber will slip until rupturing, and core filaments elongation; When external force is less than spinning tension, the elastic shrinkage of spandex thread, make outer layer fiber swell, whole section of yarn shortens. And in the present invention, warp thread and weft yarn adopt different composite fibers encapsulation spandex thread yarn core, play the advantage between each fiber. Wherein, stainless steel fibre has certain anti-electromagnetic radiation effect, has good shield effectiveness in fabric; The excellent in mechanical performance of carbon fiber, being remarkably improved the crushing resistance of hybrid yams, tear resistance, to improve single carbon fiber toughness poor etc. simultaneously, and carbon fiber light weight;Copper fiber has antibacterial, deodorization preferably, uvioresistant, health care, the feature such as comfortable. With spandex thread for yarn core, stainless steel outer packed fiber, carbon fiber, copper fiber composite fiber mixed yarn make warp thread, not only there is the elasticity that covering yarn is fabulous, also merge the advantage of four, yarn feel is smooth, the advantage of existing good intensity and light weight, also improves the tear resistance of fabric, toughness, has again good antibacterial effect and good radiation-resistant glass effect.
And ramee has the property that one, antibacterial bacteriostatic function, same amount of antibacterial is examined under a microscope, and antibacterial can multiply in a large number in cotton, wool fibre goods, and the antibacterial on Boehmeria goods is killed about 75% after 24 hours. this is because ramee contain give repeated exhortations, the trace element such as pyrimidine, purine, staphylococcus aureus, bacillus pyocyaneus, escherichia coli etc. are played inhibition, there is natural bacteriostatic, anti-demodicid mite, deodorant function. tests prove that, after 50 cyclic washings, its sterilization effect still reaches more than 98%, can effectively check the antibacterial of textile, acarid secondary pollution problem. two, deodorization adsorption function, the internal special ultrafine micropore structure of ramee makes it have powerful absorbability, can formaldehyde in absorbed air, benzene, toluene, the harmful substance such as ammonia, eliminate bad smell. after Exposure to Sunlight, it is possible to the harmful substance of absorption is vapored away so that its adsorption function automatic regeneration. three, moisture absorption airing function, ramee has the good reputation of " king of natural fiber ", its exclusive active cavity leads antiperspirant fibre structure can make the sweat saturation of suction and quickly derive in cavity, it is allowed to have possessed superior breathability and conductivity of heat, absorb water many and wet dissipation is fast, there is the cooling feeling making people very pleasantly surprised, four, mildew-resistant wear-resisting functions, ramee is very tough and tensile, powerful big and ductility is little, plus being susceptible to mold corrosion and damaging by worms, it is described as " not rotten soft gold in thousand ", thus it is widely used in flight parachute, safety rope, the fields such as home textile, there is superpower mildew-resistant wear-resisting functions, extend the service life of article well. bamboo fiber not only has the characteristics such as good breathability, moment water absorption, stronger wearability and good dyeability, also has natural antibacterial, antibacterial, acaricide, deodorant and anti-ultraviolet function. with spandex thread for yarn core, the mixed yarn of stainless steel outer packed fiber, bamboo fiber and ramee composite fibre makes weft yarn, not only there is the elasticity that covering yarn is fabulous, also merge the advantage of four, yarn feel is smooth, existing antibacterial bacteriostatic, hydroscopic fast-drying, the aspect such as biodegradable the feature of environmental protection with functional, have again good wearability, also there is good radiation-resistant glass effect.
In above-mentioned mixed yarn multifunctional fabric, the content respectively 5-10% of stainless steel fibre, copper fiber, carbon fiber and spandex thread, 2-5%, 2-5% and 80-91% in warp thread. Stainless steel fibre content is more high, then during blending, arranging density is more big, fabric radioprotective usefulness is more good, if but stainless steel fibre content is more than 10%, because the factors such as the characteristic of itself and spinnability difference, the blending uniformity can be caused on the contrary to reduce, yarn strength declines, production efficiency is low, if stainless steel fibre content is lower than 5%, does not have good radiation-proof effect. In warp thread of the present invention, if the content of copper fiber is too low, the antibacterial bacteriostatic weak effect of warp thread, the sucting wet air permeability of fabric is poor;If copper fiber content is too high, the radiation-proof effect of stainless steel fibre can be affected, affect the tear resistance of carbon fiber, and then reduce the performance of fabric. If the tear resistance of the too low warp thread of carbon fiber content is poor; If carbon fiber content is too high, higher than 5%, causing that warp thread toughness is poor on the contrary, fragility is bigger, it is easy to damage. Therefore, comprehensive each side factor, through constantly testing discovery, stainless steel fibre, copper fiber, carbon fiber by content 5-10%, 2-5%, 2-5% and 80-91%, are mixed resultant yarn with spandex thread and make warp thread best results.
In above-mentioned mixed yarn multifunctional fabric, in weft yarn, the content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 3-10%, 3-8%, 3-8% and 74-91%.
Stainless steel fibre content is more high, then during blending, arranging density is more big, fabric radioprotective usefulness is more good, but stainless steel fibre and ramee need equably by spandex thread parcel in weft yarn, stainless steel fibre is not easily too much, if stainless steel fibre content is more than 10%, because the factor such as the characteristic of itself and spinnability difference, not only result in the reduction of the blending uniformity, yarn strength flexibility decrease, production efficiency lowly, also can affect antibacterial bacteriostatic effect and the hygroscopicity of ramee; If but stainless steel fibre content is lower than 3%, not having good radiation-proof effect. In weft yarn of the present invention, ramee and bamboo fiber synergism, all there is fabulous antibacterial effect, and the antibacterial effect of both compound uses is higher than the use of Single Fiber, and mechanical property is more preferably. If ramee or bamboo fiber content are too low, the antibacterial bacteriostatic weak effect of weft yarn, the sucting wet air permeability of fabric is poor; If ramee or bamboo fiber too high levels, the radiation-proof effect of stainless steel fibre can be affected, also can reduce the performance of weft yarn simultaneously. Therefore, comprehensive each side factor, through constantly testing discovery, stainless steel fibre, bamboo fiber, ramee by content 3-10%, 3-8%, 3-8% and 74-91%, are mixed resultant yarn with spandex thread and make weft yarn best results.
As preferably, in above-mentioned mixed yarn multifunctional fabric, its fabric tissue is highly dense plain weave. Highly dense plain weave is adopted to be to ensure that the performance of fabric, especially radiation-proof effect and toughness. In warp thread weft yarn, the common stainless steel fibre existed runs through whole fabric; Carbon fiber in warp thread crosses fabric, further increases the toughness of fabric, resistance to impact; Ramee in weft yarn is perpendicular wears fabric, further increases antibacterial bacteriostatic effect and the sucting wet air permeability of fabric. And by contrast test, better by its radiation-proof effect of highly dense plain weave and toughness compared to twill, satin weave, warp thread different in fabric of the present invention and weft yarn.
The preparation method that the invention also discloses a kind of above-mentioned mixed yarn multifunctional fabric, described preparation method comprises the steps:
Warping yarn: cylinder yarn, warping, batch, warp thread coiled hair, starching, batch and through, coiled hair of weaving cotton cloth; And in operation, stainless steel fibre, copper fiber, carbon fiber are progressively wrapped in outside spandex thread yarn core and are spun into warp thread mixed yarn;
Whole weft yarn: cylinder yarn, warping, batch, warp thread coiled hair, starching, batch and through, coiled hair of weaving cotton cloth; And in operation, stainless steel fibre, bamboo fiber, ramee are progressively wrapped in outside spandex thread yarn core and are spun into weft yarn mixed yarn;
Weaving: warp thread mixed yarn and weft yarn mixed yarn are woven into fabric, fabric tissue adopts plain weave;
Final finishing: dyed, soft, sizing can be prepared by mixed yarn multifunctional fabric of the present invention.
As preferably, ramee adding before blending antistatic additive and antilubricant.
The present invention changes the deficiency that conventional Single Fiber fabric exists, by adopting the stainless steel fibre in covering yarn and rational proportion warp thread, copper fiber, carbon fiber and spandex thread, stainless steel fibre in rational proportion weft yarn, bamboo fiber, ramee and spandex thread, not only with multiple fiber composite resultant yarn, and warp thread is different from weft yarn, improve the performance of fabric further, make its existing antibacterial bacteriostatic, hydroscopic fast-drying, the feature of environmental protection of the aspect such as biodegradable is with functional, increase substantially again the intensity of fabric, elastic, tear resistance and toughness, also make it have good radiation-resistant glass effect. and fabric cloth cover of the present invention is smooth, soft smooth, radioprotective usefulness reaches more than 92%, regain 8%-10%, fiber bacteriostasis rate >=91%. therefore, application of dress material of the present invention is extensive, is especially suitable for makeing child, anemia of pregnant woman's protective garment or household electrical appliance, Medical Instruments protective cover etc.
Detailed description of the invention
The following is specific embodiments of the invention, technical scheme is further described, but the present invention is not limited to these embodiments.
Embodiment 1
Warping yarn: cylinder yarn, warping, batch, warp thread coiled hair, starching, batch and through, coiled hair of weaving cotton cloth; And in operation, stainless steel fibre, copper fiber, carbon fiber are progressively wrapped in outside spandex thread yarn core and are spun into warp thread mixed yarn; The content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 8%, 3%, 4% and 85%;
Whole weft yarn: cylinder yarn, warping, batch, warp thread coiled hair, starching, batch and through, coiled hair of weaving cotton cloth; And in operation, stainless steel fibre, bamboo fiber, ramee are progressively wrapped in outside spandex thread yarn core and are spun into weft yarn mixed yarn; The content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 5%, 6%, 5% and 84%;
Weaving: warp thread mixed yarn and weft yarn mixed yarn are woven into fabric, fabric tissue adopts plain weave; Final finishing: dyed, soft, sizing can be prepared by mixed yarn multifunctional fabric of the present invention.
Embodiment 2
The content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 6%, 4%, 4% and 86% in warp thread in the present embodiment; The content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 8%, 4%, 4% and 84%; Other techniques as described in Example 1, are not repeated herein.
Embodiment 3
The content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 9%, 3%, 3% and 85% in warp thread in the present embodiment; The content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 6%, 7%, 5% and 82%; Other techniques as described in Example 1, are not repeated herein.
Embodiment 4
The content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 5%, 2%, 2% and 91% in warp thread in the present embodiment; The content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 10%, 8%, 8% and 74%; Other techniques as described in Example 1, are not repeated herein.
Embodiment 5
The content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 10%, 5%, 5% and 80% in warp thread in the present embodiment;The content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 3%, 3%, 3% and 91%; Other techniques as described in Example 1, are not repeated herein.
Comparative example 1
In this comparative example, the warp thread of fabric, weft yarn are single spandex thread.
Comparative example 2
Differing only in of this comparative example and embodiment 1, the content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 4%, 3%, 4% and 89% in fabric warp thread in this comparative example 2.
Comparative example 3
Differing only in of this comparative example and embodiment 1, the content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 12%, 3%, 4% and 81% in fabric warp thread in this comparative example 3.
Comparative example 4
Differing only in of this comparative example and embodiment 1, the content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 8%, 1%, 4% and 87% in fabric warp thread in this comparative example 4.
Comparative example 5
Differing only in of this comparative example and embodiment 1, the content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 8%, 6%, 4% and 82% in fabric parallel in this comparative example 5.
Comparative example 6
Differing only in of this comparative example and embodiment 1, the content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 8%, 3%, 1% and 82% in fabric parallel in this comparative example 6.
Comparative example 7
Differing only in of this comparative example and embodiment 1, the content of stainless steel fibre, copper fiber, carbon fiber and spandex thread respectively 8%, 3%, 6% and 82% in fabric parallel in this comparative example 7.
Comparative example 8
Differing only in of this comparative example and embodiment 1, the content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 2%, 6%, 5% and 87% in fabric parallel in this comparative example 8.
Comparative example 9
Differing only in of this comparative example and embodiment 1, the content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 10%, 6%, 5% and 79% in fabric parallel in this comparative example 9.
Comparative example 10
Differing only in of this comparative example and embodiment 1, the content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 5%, 6%, 2% and 87% in fabric parallel in this comparative example 10.
Comparative example 11
Differing only in of this comparative example and embodiment 1, the content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 5%, 6%, 10% and 79% in fabric parallel in this comparative example 11.
Technique that the technique not clearly stated in the embodiment of the present invention and reagent are in prior art normal conventional and reagent, such as the reagent such as antistatic additive, antilubricant.
The fabric of embodiment 1-5 and comparative example 1-11 is carried out performance test, and test result is as shown in table 1.
Table 1: embodiment 1-5 and the performance of fabric in comparative example 1-11
In sum, the present invention changes the deficiency that conventional Single Fiber fabric exists, by adopting the stainless steel fibre in covering yarn and rational proportion warp thread, copper fiber, carbon fiber and spandex thread, stainless steel fibre in rational proportion weft yarn, bamboo fiber, ramee and spandex thread, not only with multiple fiber composite resultant yarn, and warp thread is different from weft yarn, improve the performance of fabric further, make its existing antibacterial bacteriostatic, hydroscopic fast-drying, the feature of environmental protection of the aspect such as biodegradable is with functional, increase substantially again the intensity of fabric, elastic, tear resistance and toughness, also make it have good radiation-resistant glass effect.And fabric cloth cover of the present invention is smooth, soft smooth, radioprotective usefulness reaches more than 92%, regain 8%-10%, fiber bacteriostasis rate >=91%. Therefore, application of dress material of the present invention is extensive, is especially suitable for makeing child, anemia of pregnant woman's protective garment or household electrical appliance, Medical Instruments protective cover etc.
Above example is merely to illustrate technical scheme but not limiting the scope of the invention; although the present invention being explained in detail with reference to preferred embodiment; it will be understood by those within the art that; technical scheme can be modified or equivalent replacement, without deviating from the spirit and scope of technical solution of the present invention.
Claims (8)
1. a mixed yarn multifunctional fabric, it is characterized in that, the warp thread of described fabric is with spandex thread for yarn core, the mixed yarn that stainless steel outer packed fiber, copper fiber, carbon fiber are spun into, the weft yarn of described fabric is with spandex thread for yarn core, the mixed yarn that stainless steel outer packed fiber, bamboo fiber, ramee are spun into.
2. mixed yarn multifunctional fabric according to claim 1, it is characterised in that the content respectively 5-10% of stainless steel fibre, copper fiber, carbon fiber and spandex thread, 2-5%, 2-5% and 80-91% in warp thread.
3. mixed yarn multifunctional fabric according to claim 1, it is characterised in that the content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 3-10%, 3-8%, 3-8% and 74-91% in weft yarn.
4. the mixed yarn multifunctional fabric according to claim 1 or 2 or 3, it is characterised in that the fabric tissue of fabric is highly dense plain weave.
5. the preparation method of a mixed yarn multifunctional fabric, it is characterised in that described preparation method comprises the steps:
Warping yarn: cylinder yarn, warping, batch, warp thread coiled hair, starching, batch and through, coiled hair of weaving cotton cloth; And in operation, stainless steel fibre, copper fiber, carbon fiber are progressively wrapped in outside spandex thread yarn core and are spun into warp thread mixed yarn;
Whole weft yarn: cylinder yarn, warping, batch, warp thread coiled hair, starching, batch and through, coiled hair of weaving cotton cloth; And in operation, stainless steel fibre, bamboo fiber, ramee are progressively wrapped in outside spandex thread yarn core and are spun into weft yarn mixed yarn;
Weaving: warp thread mixed yarn and weft yarn mixed yarn are woven into fabric, fabric tissue adopts plain weave;
Final finishing: dyed, soft, sizing can be prepared by mixed yarn multifunctional fabric of the present invention.
6. the preparation method of mixed yarn multifunctional fabric according to claim 5, it is characterised in that add antistatic additive and antilubricant before blending in ramee.
7. the preparation method of mixed yarn multifunctional fabric according to claim 5, it is characterised in that the content respectively 5-10% of stainless steel fibre, copper fiber, carbon fiber and spandex thread, 2-5%, 2-5% and 80-91% in warp thread mixed yarn.
8. the preparation method of mixed yarn multifunctional fabric according to claim 5, it is characterised in that the content of stainless steel fibre, bamboo fiber, ramee and spandex thread respectively 3-10%, 3-8%, 3-8% and 74-91% in weft yarn mixed yarn.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610108906.4A CN105648636A (en) | 2016-02-26 | 2016-02-26 | Blended yarn multifunctional fabric and making method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610108906.4A CN105648636A (en) | 2016-02-26 | 2016-02-26 | Blended yarn multifunctional fabric and making method thereof |
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| CN105648636A true CN105648636A (en) | 2016-06-08 |
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| CN109267356A (en) * | 2017-07-17 | 2019-01-25 | 射阳县华宏丝绸有限公司 | A kind of production method of silk composite material |
| CN110565234A (en) * | 2019-09-02 | 2019-12-13 | 福建七匹狼实业股份有限公司 | multifunctional yarn fabric containing mint fibers and preparation method thereof |
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| CN109267356A (en) * | 2017-07-17 | 2019-01-25 | 射阳县华宏丝绸有限公司 | A kind of production method of silk composite material |
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| CN110565234B (en) * | 2019-09-02 | 2021-10-08 | 福建七匹狼实业股份有限公司 | Multifunctional yarn fabric containing mint fibers and preparation method thereof |
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Application publication date: 20160608 |