CN105647241A - Preparation method of fluorescent sericite cosmetics - Google Patents
Preparation method of fluorescent sericite cosmetics Download PDFInfo
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- CN105647241A CN105647241A CN201610072000.1A CN201610072000A CN105647241A CN 105647241 A CN105647241 A CN 105647241A CN 201610072000 A CN201610072000 A CN 201610072000A CN 105647241 A CN105647241 A CN 105647241A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/40—Compounds of aluminium
- C09C1/42—Clays
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/006—Combinations of treatments provided for in groups C09C3/04 - C09C3/12
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/04—Physical treatment, e.g. grinding, treatment with ultrasonic vibrations
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/06—Treatment with inorganic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
Abstract
The invention discloses a preparation method of fluorescent sericite cosmetics. The method includes the following steps that S1, paste is prepared, wherein mineral raw materials needed for preparing sericite are selected, high-quality mineral raw materials are selected manually, rough stripping is performed on the mineral raw materials, sericite is re-processed through wet process stripping and classification technologies, and therefore the sericite paste is obtained; S2, metallurgy is performed, wherein wet untrafine grinding is performed for the first time, the sericite paste is placed in a stirrer, an aqueous solution of acid media or alkali media is added into the stirrer for chemical processing, or organic solvents are added for extraction, impurity separation, metal extraction and extraction of compounds of metal, temperature is kept at 20-40 DEG C, full stirring is performed for 1-2 h, secondary classification is performed on the sericite paste, and high-purity sericite is obtained. The preparation method is simple, not only are the purity and the glossiness of the prepared fluorescent sericite high, but also cost is low, and the fluorescent sericite is very practical.
Description
Technical field
The present invention relates to sericite in powder technical field, the preparation method particularly relating to a kind of fluorescence sericitization cosmetic.
Background technology
Sericite (Sericite) is the one of Muscovitum, it belongs to the silicate mineral with layer structure and draws, sericite has purposes very widely, for industries such as rubber, plastics, coating, paint, pottery, insulation, cosmetics, pigment, papermaking, metallurgy, the outward appearance of sericite is translucent, is rich in the silky luster of texture, having the high radius-thickness ratio structure of uniqueness and excellent uv-shielding capacity, especially finely squamose laminate structure has soft smooth characteristic. China's sericite mica ore reserves are big, distribution is wide, but are worth the less of exploitation. Different according to origin of ore deposit, sericite mica ore can be divided into: sheet lithotype (Anhui Chuzhou), porphyry alteration type (Jing Dezhen, Jiangxi), volcanic rock alteration type (Fujian Nanan) etc. Wherein maximum with sheet lithotype sericite mica ore (Anhui Chuzhou) value of exploiting and utilizing, because the Muscovitum feature of such sericite mica ore is the most obvious, the coating mica powder of such as technical grade is a kind of new type functional environmental protection filler, the functions such as unique two-dimensional sheet intercepts, the stability of shielding ultraviolet light, chemical constitution are effectively improved the permeability resistance of film, weatherability, wearability and corrosion resistance, additionally, without any radioelement, lead the trend of paint field environmental protection. It is widely used in building external paint, anticorrosive paint, powdery paints, high-temperature resistant coating, coatings, water-repellent paint, marking paint, radiation shielding coating and some special coatings, such as marine paint, coating of holding temperature for spacecraft and food container coating etc.
Cosmetics-stage Muscovitum has the laminated structure of uniqueness, silky luster and soft and smooth texture, makes cosmetics opaque merrily and lightheartedly fine and smooth just as silkiness. Natural texture allows skin have splendid affinity and a sparkling and crystal-clear beautiful effect, the feature such as give cosmetics soft-touch, gloss is soft, affinity is good, patch skin power is strong, is the first-selected high-grade opaque raw material of cosmetic industry.Additionally the crystal transparency of mica powder can allow dressing color keep the intensity of coherency, is also suitable for various deep or light color. Unique essence of sericite also can increase silkiness flexible bright and give cosmetics manufacture. Product is widely used in the various fields such as muffin, honey powder, eye shadow, foundation emulsion, rouge, honey powder, but the development now with society, people not only simply meet common cosmetics, people start to pursue the change of cosmetic color etc. character, so needing a kind of novel cosmetics-stage sericite in powder to replace.
Summary of the invention
Based on the technical problem that background technology exists, the preparation method that the present invention proposes a kind of fluorescence sericitization cosmetic.
The preparation method of a kind of fluorescence sericitization cosmetic that the present invention proposes, comprises the following steps:
S1, slurrying: choose the raw mineral materials prepared needed for sericite, pick out superior in quality raw mineral materials by artificial mode, raw mineral materials is carried out shelling, then pass through wet method stripping, grading technology, sericite is reprocessed, obtains sericite slurry with this;
S2, metallurgical: first time wet method super-fine, sericite slurry is put in blender, then the aqueous solution adding acid medium or alkaline medium in blender carries out chemical treatment, or add organic solvent extraction, separate impurity, extract metal and compound thereof, and maintain the temperature at 20-40 DEG C, it is sufficiently stirred for 1-2h, sericite slurry is made to carry out the classification of secondary, obtain high-purity sericite, then again through the wet method super-fine of secondary, high-purity sericite is carried out the classification of third time, the sericite slurry of a kind of cosmetics-stage can be obtained;
S3, separate: the sericite slurry of the cosmetics-stage in S2 is put in blender, it is added thereto to luminous aluminate material, it is stirred mixing, stirring duration is 2-3h, then adds heavy metals removal agent in the mixture after stirring, carries out heavy metal accumulation removal, then carry out deionized water cleaning again, obtain the sericite after a kind of process;
S4, dry: the sericite in S3 is first carried out filter-press dehydration, it is then placed in high-temperature cabinet and carries out dehydrate, carry out high temperature drying sterilizing again, continue 1-3h, then the sericite after high temperature drying sterilizing is carried out depolymerization, finally the sericite after depolymerization is packed, a kind of fluorescence sericite can be obtained.
Preferably, in described S3, boric acid is added as flux.
Preferably, described in described S1, sericite slurry is put in blender, carry out first time wet method super-fine, sericite slurry is put in blender, then the aqueous solution adding acid medium or alkaline medium in blender carries out chemical treatment, or interpolation organic solvent extraction, separate impurity, extract metal and compound thereof, and maintain the temperature at 30 DEG C, it is sufficiently stirred for 2h, sericite slurry is made to carry out the classification of secondary, obtain high-purity sericite, then again through the wet method super-fine of secondary, high-purity sericite is carried out the classification of third time, the sericite slurry of a kind of cosmetics-stage can be obtained.
Preferably, the sericite slurry of the cosmetics-stage in described S2 is put in blender, it is added thereto to luminous aluminate material, it is stirred mixing, stirring duration is 2.5h, then adds heavy metals removal agent in the mixture after stirring, carries out heavy metal accumulation removal, then carry out deionized water cleaning again, obtain the sericite after a kind of process.
Preferably, sericite in described S3 first carries out filter-press dehydration, it is then placed in high-temperature cabinet and carries out dehydrate, carry out high temperature drying sterilizing again, continue 2h, then the sericite after high temperature drying sterilizing is carried out depolymerization, finally the sericite after depolymerization is packed, a kind of fluorescence sericite can be obtained.
Preferably, described blender adopts stirring frosted dispersion multiple purpose aeroplane.
The present invention is in preparation process, first sericite mica ore raw material is first carried out the artificial selection of primary, then select superior in quality raw mineral materials to decompose, and the raw material after decomposing is carried out slurrying, the sericite slurry obtained after slurrying is put in blender, by blender, it is sufficiently stirred for, the aqueous solution adding acid medium or alkaline medium in blender carries out chemical treatment or organic solvent extraction, separate impurity, extract metal and compound thereof, namely by twice wet method super-fine, sericite is carried out classification repeatedly, highly purified sericite is obtained with this, then in highly purified sericite, the luminescent materials such as aluminate are put into, it is stirred mixing, then in the mixture after stirring, heavy metals removal agent is added, carry out heavy metal accumulation removal, then deionized water cleaning is carried out again, obtain the sericite after a kind of process, finally sericite it is dried and packs, preparation method of the present invention is simple, operation is coherent, the fluorescence sericite purity not only prepared is high, glossiness is high, to skin very beneficial, and there is novelty, the demand of cosmetics-stage sericite can be met, and cost is not high, practicality very.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention done further explanation.
Embodiment one
The preparation method of a kind of fluorescence sericitization cosmetic that the present invention proposes, comprises the following steps:
S1, slurrying: choose the raw mineral materials prepared needed for sericite, pick out superior in quality raw mineral materials by artificial mode, raw mineral materials is carried out shelling, then pass through wet method stripping, grading technology, sericite is reprocessed, obtains sericite slurry with this;
S2, metallurgical: first time wet method super-fine, sericite slurry is put in blender, then the aqueous solution adding acid medium or alkaline medium in blender carries out chemical treatment, or add organic solvent extraction, separate impurity, extract metal and compound thereof, and maintain the temperature at 20 DEG C, it is sufficiently stirred for 1h, sericite slurry is made to carry out the classification of secondary, obtain high-purity sericite, then again through the wet method super-fine of secondary, high-purity sericite is carried out the classification of third time, the sericite slurry of a kind of cosmetics-stage can be obtained;
S3, separate: the sericite slurry of the cosmetics-stage in S2 is put in blender, it is added thereto to luminous aluminate material, it is stirred mixing, stirring duration is 2h, then adds heavy metals removal agent in the mixture after stirring, carries out heavy metal accumulation removal, then carry out deionized water cleaning again, obtain the sericite after a kind of process;
S4, dry: the sericite in S3 is first carried out filter-press dehydration, it is then placed in high-temperature cabinet and carries out dehydrate, carry out high temperature drying sterilizing again, continue 1h, then the sericite after high temperature drying sterilizing is carried out depolymerization, finally the sericite after depolymerization is packed, a kind of fluorescence sericite can be obtained.
Embodiment two
The preparation method of a kind of fluorescence sericitization cosmetic that the present invention proposes, comprises the following steps:
S1, slurrying: choose the raw mineral materials prepared needed for sericite, pick out superior in quality raw mineral materials by artificial mode, raw mineral materials is carried out shelling, then pass through wet method stripping, grading technology, sericite is reprocessed, obtains sericite slurry with this;
S2, metallurgical: first time wet method super-fine, sericite slurry is put in blender, then the aqueous solution adding acid medium or alkaline medium in blender carries out chemical treatment, or add organic solvent extraction, separate impurity, extract metal and compound thereof, and maintain the temperature at 25 DEG C, it is sufficiently stirred for 1.5h, sericite slurry is made to carry out the classification of secondary, obtain high-purity sericite, then again through the wet method super-fine of secondary, high-purity sericite is carried out the classification of third time, the sericite slurry of a kind of cosmetics-stage can be obtained;
S3, separate: the sericite slurry of the cosmetics-stage in S2 is put in blender, it is added thereto to luminous aluminate material, it is stirred mixing, stirring duration is 2.5h, then adds heavy metals removal agent in the mixture after stirring, carries out heavy metal accumulation removal, then carry out deionized water cleaning again, obtain the sericite after a kind of process;
S4, dry: the sericite in S3 is first carried out filter-press dehydration, it is then placed in high-temperature cabinet and carries out dehydrate, carry out high temperature drying sterilizing again, continue 2h, then the sericite after high temperature drying sterilizing is carried out depolymerization, finally the sericite after depolymerization is packed, a kind of fluorescence sericite can be obtained.
Embodiment three
The preparation method of a kind of fluorescence sericitization cosmetic that the present invention proposes, comprises the following steps:
S1, slurrying: choose the raw mineral materials prepared needed for sericite, pick out superior in quality raw mineral materials by artificial mode, raw mineral materials is carried out shelling, then pass through wet method stripping, grading technology, sericite is reprocessed, obtains sericite slurry with this;
S2, metallurgical: first time wet method super-fine, sericite slurry is put in blender, then the aqueous solution adding acid medium or alkaline medium in blender carries out chemical treatment, or add organic solvent extraction, separate impurity, extract metal and compound thereof, and maintain the temperature at 35 DEG C, it is sufficiently stirred for 2h, sericite slurry is made to carry out the classification of secondary, obtain high-purity sericite, then again through the wet method super-fine of secondary, high-purity sericite is carried out the classification of third time, the sericite slurry of a kind of cosmetics-stage can be obtained;
S3, separate: the sericite slurry of the cosmetics-stage in S2 is put in blender, it is added thereto to luminous aluminate material, it is stirred mixing, stirring duration is 3h, then adds heavy metals removal agent in the mixture after stirring, carries out heavy metal accumulation removal, then carry out deionized water cleaning again, obtain the sericite after a kind of process;
S4, dry: the sericite in S3 is first carried out filter-press dehydration, it is then placed in high-temperature cabinet and carries out dehydrate, carry out high temperature drying sterilizing again, continue 3h, then the sericite after high temperature drying sterilizing is carried out depolymerization, finally the sericite after depolymerization is packed, a kind of fluorescence sericite can be obtained.
The above; it is only the present invention preferably detailed description of the invention; but protection scope of the present invention is not limited thereto; any those familiar with the art is in the technical scope that the invention discloses; it is equal to replacement according to technical scheme and inventive concept thereof or is changed, all should be encompassed within protection scope of the present invention.
Claims (6)
1. the preparation method of a fluorescence sericitization cosmetic, it is characterised in that comprise the following steps:
S1, slurrying: choose the raw mineral materials prepared needed for sericite, pick out superior in quality raw mineral materials by artificial mode, raw mineral materials is carried out shelling, then pass through wet method stripping, grading technology, sericite is reprocessed, obtains sericite slurry with this;
S2, metallurgical: first time wet method super-fine, sericite slurry is put in blender, then the aqueous solution adding acid medium or alkaline medium in blender carries out chemical treatment, or add organic solvent extraction, separate impurity, extract metal and compound thereof, and maintain the temperature at 20-40 DEG C, it is sufficiently stirred for 1-2h, sericite slurry is made to carry out the classification of secondary, obtain high-purity sericite, then again through the wet method super-fine of secondary, high-purity sericite is carried out the classification of third time, the sericite slurry of a kind of cosmetics-stage can be obtained;
S3, separate: the sericite slurry of the cosmetics-stage in S2 is put in blender, it is added thereto to luminous aluminate material, it is stirred mixing, stirring duration is 2-3h, then adds heavy metals removal agent in the mixture after stirring, carries out heavy metal accumulation removal, then carry out deionized water cleaning again, obtain the sericite after a kind of process;
S4, dry: the sericite in S3 is first carried out filter-press dehydration, it is then placed in high-temperature cabinet and carries out dehydrate, carry out high temperature drying sterilizing again, continue 1-3h, then the sericite after high temperature drying sterilizing is carried out depolymerization, finally the sericite after depolymerization is packed, a kind of fluorescence sericite can be obtained.
2. the preparation method of a kind of fluorescence sericitization cosmetic according to claim 1, it is characterised in that add boric acid in described S3 as flux.
3. the preparation method of a kind of fluorescence sericitization cosmetic according to claim 1, it is characterized in that, described in described S1, sericite slurry is put in blender, carry out first time wet method super-fine, sericite slurry is put in blender, then the aqueous solution adding acid medium or alkaline medium in blender carries out chemical treatment, or interpolation organic solvent extraction, separate impurity, extract metal and compound thereof, and maintain the temperature at 30 DEG C, it is sufficiently stirred for 2h, sericite slurry is made to carry out the classification of secondary, obtain high-purity sericite, then again through the wet method super-fine of secondary, high-purity sericite is carried out the classification of third time, the sericite slurry of a kind of cosmetics-stage can be obtained.
4. the preparation method of a kind of fluorescence sericitization cosmetic according to claim 1, it is characterized in that, the sericite slurry of the cosmetics-stage in described S2 is put in blender, being added thereto to luminous aluminate material, be stirred mixing, stirring duration is 2.5h, then in the mixture after stirring, heavy metals removal agent is added, carry out heavy metal accumulation removal, then carry out deionized water cleaning again, obtain the sericite after a kind of process.
5. the preparation method of a kind of fluorescence sericitization cosmetic according to claim 1, it is characterized in that, sericite in described S3 first carries out filter-press dehydration, it is then placed in high-temperature cabinet and carries out dehydrate, carry out high temperature drying sterilizing again, continue 2h, then the sericite after high temperature drying sterilizing is carried out depolymerization, finally the sericite after depolymerization is packed, a kind of fluorescence sericite can be obtained.
6. the preparation method of a kind of fluorescence sericitization cosmetic according to claim 1, it is characterised in that described blender adopts stirring frosted dispersion multiple purpose aeroplane.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610072000.1A CN105647241A (en) | 2016-02-02 | 2016-02-02 | Preparation method of fluorescent sericite cosmetics |
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| CN201610072000.1A CN105647241A (en) | 2016-02-02 | 2016-02-02 | Preparation method of fluorescent sericite cosmetics |
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| CN105647241A true CN105647241A (en) | 2016-06-08 |
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| CN201610072000.1A Pending CN105647241A (en) | 2016-02-02 | 2016-02-02 | Preparation method of fluorescent sericite cosmetics |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107188193A (en) * | 2017-07-24 | 2017-09-22 | 安徽恒昊科技有限公司 | A kind of preparation method of high-purity mica powder of wet process used for cosmetic |
| CN107673363A (en) * | 2017-11-05 | 2018-02-09 | 滁州格锐矿业有限责任公司 | A kind of preparation method for preparing sericite in powder used for cosmetic |
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| CN101974200A (en) * | 2010-11-03 | 2011-02-16 | 哈尔滨工业大学 | Method for improving heat resistance of phenolic resin |
| CN104606072A (en) * | 2014-12-31 | 2015-05-13 | 安徽恒昊科技有限公司 | Preparation method of silicone-treated sericite powder |
| WO2015166895A1 (en) * | 2014-04-28 | 2015-11-05 | 堺化学工業株式会社 | Cosmetic |
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2016
- 2016-02-02 CN CN201610072000.1A patent/CN105647241A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101974200A (en) * | 2010-11-03 | 2011-02-16 | 哈尔滨工业大学 | Method for improving heat resistance of phenolic resin |
| WO2015166895A1 (en) * | 2014-04-28 | 2015-11-05 | 堺化学工業株式会社 | Cosmetic |
| CN104606072A (en) * | 2014-12-31 | 2015-05-13 | 安徽恒昊科技有限公司 | Preparation method of silicone-treated sericite powder |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107188193A (en) * | 2017-07-24 | 2017-09-22 | 安徽恒昊科技有限公司 | A kind of preparation method of high-purity mica powder of wet process used for cosmetic |
| CN107188193B (en) * | 2017-07-24 | 2019-05-03 | 安徽恒昊科技有限公司 | A kind of preparation method of high-purity mica powder of wet process used for cosmetic |
| CN107673363A (en) * | 2017-11-05 | 2018-02-09 | 滁州格锐矿业有限责任公司 | A kind of preparation method for preparing sericite in powder used for cosmetic |
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Application publication date: 20160608 |