CN105625029B - A kind of foaming agent and preparation method thereof for foam starching of weaving - Google Patents

A kind of foaming agent and preparation method thereof for foam starching of weaving Download PDF

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Publication number
CN105625029B
CN105625029B CN201610049140.7A CN201610049140A CN105625029B CN 105625029 B CN105625029 B CN 105625029B CN 201610049140 A CN201610049140 A CN 201610049140A CN 105625029 B CN105625029 B CN 105625029B
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parts
foaming agent
weaving
foam
water
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CN105625029A (en
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周继东
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Guangdong Kefeng New Material Technology Co Ltd
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/188Monocarboxylic acids; Anhydrides, halides or salts thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/325Amines
    • D06M13/342Amino-carboxylic acids; Betaines; Aminosulfonic acids; Sulfo-betaines
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402Amides imides, sulfamic acids
    • D06M13/425Carbamic or thiocarbamic acids or derivatives thereof, e.g. urethanes
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46Compounds containing quaternary nitrogen atoms
    • D06M13/463Compounds containing quaternary nitrogen atoms derived from monoamines

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)

Abstract

The present invention relates to a kind of foaming agents and preparation method thereof for foam starching of weaving, by weight, including following component:12 25 parts of palmitic acid, 12 18 parts of ethylenediamine tetra-acetic acid, 20 35 parts of dodecyldimethylammonium hydroxide inner salt, 18 28 parts of octyl dodecanol lauroyl glutamate ester, 75 8 parts of polyquaternium, 47 parts of stabilizer, 20 30 parts of water.The foaming agent by safe and harmless at being grouped as, it is environmentally protective.Such foaming agent using can make slurry fully foam on a small quantity, and foam exquisiteness is stablized, and so that slurry is uniformly adhered on warp thread, so that the water consumption of sizing process is substantially reduced and improve the rate of sizing of warp thread, reduce energy consumption.

Description

A kind of foaming agent and preparation method thereof for foam starching of weaving
Technical field:
The present invention relates to textile technology fields, more particularly to a kind of foaming agent for foam starching of weaving and its preparation Method.
Background technology:
Warp thread foam starching is that after fully blistering using the slurries that can generate foam, foam is evenly distributed in warp thread On, then use device destroys blistering, makes bubbles burst, gas release.Slurries are attached on warp thread, can to make warp thread have Knitting property.Such foam Sizing Technology has many characteristics, such as that low energy consumption, drying are quick, can save processing water while reduce sewage row High-volume, it is a kind of energy-saving and environment-friendly Sizing Technology.
Foaming agent is a kind of surface reactive material, is generated between mainly a kind of surface or interface that can make different material special Different adsorption can form bubble to can significantly reduce the substance on surface or interfacial tension, and ensure that bubble rises shape At froth bed.Report about the research country being applied to foaming agent in weaving is less, Chinese patent CN201410059305.x discloses a kind of foaming agent of promotion slurry foaming, and this method is made using foaming agent water solution in machinery The effect that a large amount of foams are generated in the case of firmly introducing air, promotes Slurry bubble performance and foam stability, develops one Kind can in cotton, wash and its mixed yarn warp yarn sizing, weaving in the novel high-performance foamed slurry applied, keep slurry foaming properties steady It is fixed, reduce usage of sizing agent, improves the rate of sizing of warp thread.But the inadequate safety and environmental protection of blowing agent component belonging to it, it is right Human injury has injury.
Invention content:
The present invention relates to a kind of foaming agents and preparation method thereof for foam starching of weaving, and the foaming agent is by safe and harmless At being grouped as, it is environmentally protective.Such foaming agent using can make slurry fully foam on a small quantity, and foam exquisiteness is stablized, and makes Slurry is uniformly adhered on warp thread, so that the water consumption of sizing process is substantially reduced and is improved the rate of sizing of warp thread, reduces Energy consumption.
It is a further object of the present invention to provide the preparation methods of the foaming agent.
To achieve the above object, the present invention uses following technical scheme:
A kind of foaming agent for foam starching of weaving, by weight, including following component:
12-25 parts of palmitic acid,
12-18 parts of ethylenediamine tetra-acetic acid,
20-35 parts of dodecyldimethylammonium hydroxide inner salt,
18-28 parts of octyl dodecanol lauroyl glutamate ester,
- 7 5-8 parts of polyquaternium,
4-7 parts of stabilizer,
20-30 parts of water.
As a preferred embodiment of the above technical solution, a kind of foaming agent for foam starching of weaving, which is characterized in that by weight Part meter, including following component:
15-20 parts of palmitic acid,
15-18 parts of ethylenediamine tetra-acetic acid,
25-30 parts of dodecyldimethylammonium hydroxide inner salt,
20-25 parts of octyl dodecanol lauroyl glutamate ester,
- 7 6-7 parts of polyquaternium,
5-7 parts of stabilizer,
25-30 parts of water.
As a preferred embodiment of the above technical solution, the stabilizer is castor-oil plant sodium alkoxide, polyether silicone, sulfosuccinate In it is one or more.
A kind of preparation method of foaming agent for foam starching of weaving, includes the following steps:
By palmitic acid, ethylenediamine tetra-acetic acid, dodecyldimethylammonium hydroxide inner salt is dissolved in the water, and maintains the temperature at 50-60 DEG C, 10min is stirred with the velocity pulse of 15-25 turns/min, sequentially adds octyl dodecanol lauroyl glutamate ester, polyquaternary amine Salt -7 is stirred with the velocity pulse of 15-25 turns/min and stabilizer is added dropwise thereto, continues pulse stirring after being added dropwise to complete 5min obtains the foaming agent for foam starching of weaving.
As a preferred embodiment of the above technical solution, the preparation method of a kind of foaming agent for foam starching of weaving, feature It is, includes the following steps:
By 18 parts of palmitic acids, 18 parts of ethylenediamine tetra-acetic acids, 28 parts of dodecyldimethylammonium hydroxide inner salts are dissolved in 27 parts of water, 55 DEG C are maintained the temperature at, 10min is stirred with the velocity pulse of 15 turns/min, sequentially adds 23 parts of octyl dodecanol lauroyl paddy Propylhomoserin ester, 6 parts of polyquaterniums -7 are stirred with the velocity pulse of 15 turns/min and 7 parts of stabilizers are added dropwise thereto, after being added dropwise to complete Continue pulse and stir 5min, obtains the foaming agent for foam starching of weaving.
As a preferred embodiment of the above technical solution, the frequency of the pulse stirring is to suspend 20s after persistently stirring 10s.
The invention has the advantages that:
The foaming agent uses safe and harmless ingredient, is not injured to health, can be used for being in direct contact knitting for skin Object starching.Foam number is high, and using that slurry can be made fully to blister on a small quantity, foam is fine and smooth, and stabilization time is long, is conducive to the equal of slurry Even coating.The water consumption in sizing process is reduced, energy consumption is saved, is a kind of environmentally protective blistering for foam starching of weaving Agent.
Specific implementation mode:
In order to better understand the present invention, below by embodiment, the present invention is further described, and embodiment is served only for solving The present invention is released, any restriction will not be constituted to the present invention.
Embodiment 1
A kind of preparation method of foaming agent for foam starching of weaving, includes the following steps:
By 12 parts of palmitic acids, 13 parts of ethylenediamine tetra-acetic acids, 35 parts of dodecyldimethylammonium hydroxide inner salts are dissolved in 20 parts of water, 50 DEG C are maintained the temperature at, 10min is stirred with the velocity pulse of 20 turns/min, sequentially adds 18 parts of octyl dodecanol lauroyl paddy Propylhomoserin ester, 8 parts of polyquaterniums -7 are stirred with the velocity pulse of 20 turns/min and 7 parts of stabilizers are added dropwise thereto, after being added dropwise to complete Continue pulse and stir 5min, obtains the foaming agent for foam starching of weaving.
5ml foaming agents, blistering rate 89%, half-life period 30min are added into 1L water.
Embodiment 2
A kind of preparation method of foaming agent for foam starching of weaving, includes the following steps:
By 15 parts of palmitic acids, 16 parts of ethylenediamine tetra-acetic acids, 30 parts of dodecyldimethylammonium hydroxide inner salts are dissolved in 25 parts of water, 60 DEG C are maintained the temperature at, 10min is stirred with the velocity pulse of 20 turns/min, sequentially adds 25 parts of octyl dodecanol lauroyl paddy Propylhomoserin ester, 7 parts of polyquaterniums -7 are stirred with the velocity pulse of 20 turns/min and 6 parts of stabilizers are added dropwise thereto, after being added dropwise to complete Continue pulse and stir 5min, obtains the foaming agent for foam starching of weaving.
5ml foaming agents, blistering rate 91%, half-life period 45min are added into 1L water.
Embodiment 3
A kind of preparation method of foaming agent for foam starching of weaving, includes the following steps:
By 18 parts of palmitic acids, 18 parts of ethylenediamine tetra-acetic acids, 28 parts of dodecyldimethylammonium hydroxide inner salts are dissolved in 27 parts of water, 55 DEG C are maintained the temperature at, 10min is stirred with the velocity pulse of 15 turns/min, sequentially adds 23 parts of octyl dodecanol lauroyl paddy Propylhomoserin ester, 6 parts of polyquaterniums -7 are stirred with the velocity pulse of 15 turns/min and 7 parts of stabilizers are added dropwise thereto, after being added dropwise to complete Continue pulse and stir 5min, obtains the foaming agent for foam starching of weaving.
5ml foaming agents, blistering rate 95%, half-life period 60min are added into 1L water.
Embodiment 4
A kind of preparation method of foaming agent for foam starching of weaving, includes the following steps:
By 20 parts of palmitic acids, 15 parts of ethylenediamine tetra-acetic acids, 25 parts of dodecyldimethylammonium hydroxide inner salts are dissolved in 30 parts of water, 50-60 DEG C is maintained the temperature at, 10min is stirred with the velocity pulse of 25 turns/min, sequentially adds 20 parts of octyl dodecanol bays Acyl glutamate, 7 parts of polyquaterniums -7 are stirred with the velocity pulse of 25 turns/min and 5 parts of stabilizers are added dropwise thereto, dripped 5min is stirred at rear continuation pulse, obtains the foaming agent for foam starching of weaving.
5ml foaming agents, blistering rate 90%, half-life period 50min are added into 1L water.
Embodiment 5
A kind of preparation method of foaming agent for foam starching of weaving, includes the following steps:
By 23 parts of palmitic acids, 12 parts of ethylenediamine tetra-acetic acids, 23 parts of dodecyldimethylammonium hydroxide inner salts are dissolved in 22 parts of water, 50 DEG C are maintained the temperature at, 10min is stirred with the velocity pulse of 15 turns/min, sequentially adds 28 parts of octyl dodecanol lauroyl paddy Propylhomoserin ester, 8 parts of polyquaterniums -7 are stirred with the velocity pulse of 15 turns/min and 4 parts of stabilizers are added dropwise thereto, after being added dropwise to complete Continue pulse and stir 5min, obtains the foaming agent for foam starching of weaving.
5ml foaming agents, blistering rate 84%, half-life period 40min are added into 1L water.
Embodiment 6
A kind of preparation method of foaming agent for foam starching of weaving, includes the following steps:
By 25 parts of palmitic acids, 14 parts of ethylenediamine tetra-acetic acids, 20 parts of dodecyldimethylammonium hydroxide inner salts are dissolved in 25 parts of water, 55 DEG C are maintained the temperature at, 10min is stirred with the velocity pulse of 15 turns/min, sequentially adds 22 parts of octyl dodecanol lauroyl paddy Propylhomoserin ester, 5 parts of polyquaterniums -7 are stirred with the velocity pulse of 15 turns/min and 6 parts of stabilizers are added dropwise thereto, after being added dropwise to complete Continue pulse and stir 5min, obtains the foaming agent for foam starching of weaving.
5ml foaming agents, blistering rate 83%, half-life period 30min are added into 1L water.

Claims (3)

1. a kind of foaming agent for foam starching of weaving, which is characterized in that by weight, including following component:
12-25 parts of palmitic acid,
12-18 parts of ethylenediamine tetra-acetic acid,
20-35 parts of dodecyldimethylammonium hydroxide inner salt,
18-28 parts of octyl dodecanol lauroyl glutamate ester,
- 7 5-8 parts of polyquaternium,
4-7 parts of stabilizer,
20-30 parts of water;
The stabilizer is castor-oil plant sodium alkoxide, one or more in polyether silicone;
The preparation method of the foaming agent for foam starching of weaving, includes the following steps:
By palmitic acid, ethylenediamine tetra-acetic acid, dodecyldimethylammonium hydroxide inner salt is dissolved in the water, and maintains the temperature at 50-60 DEG C, with 15-25 turns/and the velocity pulse of min stirs 10min, sequentially add octyl dodecanol lauroyl glutamate ester, polyquaternium -7, It is stirred with the velocity pulse of 15-25 turns/min and stabilizer is added dropwise thereto, continued pulse after being added dropwise to complete and stir 5min, obtain Foaming agent for foam starching of weaving;
The frequency of the pulse stirring is to suspend 20s after persistently stirring 10s.
2. the foaming agent according to claim 1 for foam starching of weaving, which is characterized in that by weight, including Following component:
15-20 parts of palmitic acid,
15-18 parts of ethylenediamine tetra-acetic acid,
25-30 parts of dodecyldimethylammonium hydroxide inner salt,
20-25 parts of octyl dodecanol lauroyl glutamate ester,
- 7 6-7 parts of polyquaternium,
5-7 parts of stabilizer,
25-30 parts of water.
3. it is according to claim 1 for weave foam starching foaming agent preparation method, which is characterized in that including with Lower step:
By 18 parts of palmitic acids, 18 parts of ethylenediamine tetra-acetic acids, 28 parts of dodecyldimethylammonium hydroxide inner salts are dissolved in 27 parts of water, are kept Temperature stirs 10min at 55 DEG C, with the velocity pulse of 15 turns/min, sequentially adds 23 parts of octyl dodecanol lauroyl glutamates Ester, 6 parts of polyquaterniums -7 are stirred with the velocity pulse of 15 turns/min and 7 parts of stabilizers are added dropwise thereto, continued after being added dropwise to complete 5min is stirred in pulse, obtains the foaming agent for foam starching of weaving.
CN201610049140.7A 2016-01-25 2016-01-25 A kind of foaming agent and preparation method thereof for foam starching of weaving Active CN105625029B (en)

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Application Number Priority Date Filing Date Title
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CN105625029B true CN105625029B (en) 2018-09-14

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Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2048326B (en) * 1978-09-19 1983-06-15 United Merchants & Mfg Foam composition for treating textile materials
GB9011921D0 (en) * 1990-05-29 1990-07-18 Albright & Wilson Coating composition and process
CN101262842B (en) * 2005-09-16 2011-06-29 雷克特本克斯尔有限公司 Foaming topical compositions
AR073346A1 (en) * 2009-07-21 2010-11-03 Silva Pablo Cesar FOAM TRAINING COMPOSITION FOR THE GENERATION OF SHARED TEMPORARY DURATION SIGNALS
CN104862969A (en) * 2014-02-21 2015-08-26 江南大学 Foaming agent of foaming textile slurry

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Effective date of registration: 20180802

Address after: 318050 No. 65 new avenue, Xinqiao Town, Luqiao District, Taizhou, Zhejiang.

Applicant after: Xie Liping

Address before: 215000 2 Taishan Road, high tech Zone, Suzhou, Jiangsu (Room 101 and 201, zone A, test center, Poji science and Technology Pioneer Park)

Applicant before: SUZHOU INSILK DIGITAL TEXTILE SCIENCE & TECHNOLOGY CO., LTD.

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Effective date of registration: 20190801

Address after: Room 103, 60 Yangkeng Road, Changping Town, Dongguan City, Guangdong Province

Patentee after: Guangdong Kefeng New Material Technology Co., Ltd.

Address before: 318050 No. 65 Xinqiao Street, Luqiao Xinqiao Town, Luqiao District, Taizhou City, Zhejiang Province

Patentee before: Xie Liping