CN105623462A - Epoxy resin spray-coating method and special-purpose epoxy resin spray-coating liquid thereof - Google Patents
Epoxy resin spray-coating method and special-purpose epoxy resin spray-coating liquid thereof Download PDFInfo
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- CN105623462A CN105623462A CN201410619256.0A CN201410619256A CN105623462A CN 105623462 A CN105623462 A CN 105623462A CN 201410619256 A CN201410619256 A CN 201410619256A CN 105623462 A CN105623462 A CN 105623462A
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- China
- Prior art keywords
- epoxy resin
- spray
- iron core
- spraying
- resin spray
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- 238000005507 spraying Methods 0.000 title claims abstract description 64
- 239000003822 epoxy resin Substances 0.000 title claims abstract description 61
- 229920000647 polyepoxide Polymers 0.000 title claims abstract description 61
- 239000007788 liquid Substances 0.000 title abstract 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical group [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 43
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 19
- 238000000034 method Methods 0.000 claims abstract description 14
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000004593 Epoxy Substances 0.000 claims description 21
- 239000011159 matrix material Substances 0.000 claims description 15
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 10
- -1 phenolic aldehyde amine Chemical class 0.000 claims description 5
- 230000007306 turnover Effects 0.000 claims description 2
- 239000007921 spray Substances 0.000 abstract description 42
- 239000013078 crystal Substances 0.000 abstract 3
- 239000008096 xylene Substances 0.000 abstract 1
- 230000000630 rising effect Effects 0.000 description 12
- 239000003292 glue Substances 0.000 description 10
- 239000000084 colloidal system Substances 0.000 description 9
- 238000000576 coating method Methods 0.000 description 7
- 238000001514 detection method Methods 0.000 description 7
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 6
- 238000012856 packing Methods 0.000 description 6
- 238000004806 packaging method and process Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 229920006334 epoxy coating Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000012958 reprocessing Methods 0.000 description 1
Landscapes
- Manufacturing Cores, Coils, And Magnets (AREA)
Abstract
The invention discloses an epoxy resin spray-coating method and a special-purpose epoxy resin spray-coating liquid thereof. The epoxy resin spray-coating liquid comprises, by weight, 100 parts of epoxy resin, 30 parts of a curing agent and 10-30 parts of xylene. The method comprises 1, spray-coating one side of a base, which is baked at a temperature of 110 DEG C for 15min and is to be spray-coated, with the epoxy resin spray-coating liquid, 2, baking the spray-coated base at a temperature of 100-120 DEG C for 15-30min, and 3, turning over the base baked through the step 2 and spray-coating the other side of the base through the steps 1 and 2. The epoxy resin spray-coating method accelerates amorphous nanometer crystal iron core package treatment time, reduces an amorphous nanometer crystal iron core package cost and improves performances of the amorphous nanometer crystal iron core spray-coated with epoxy resin.
Description
Technical field
The present invention relates to a kind of epoxy resin spraying method, particularly to a kind of amorphous nano-crystalline iron core spray epoxy method.
Background technology
Little iron core packaging is generally adopted two kinds of manner of packings: one, protect box packaging. This manner of packing waste of manpower, raw material, production cost is high, improves product price. And it is high to introduce cost when reprocessing. This manner of packing is unfavorable for producing on the whole. Two, spraying packaging. Existing spraying manner of packing includes spray epoxy, spray coating powder paint etc.
Existing epoxy resin spraying method many employings pressure air sprays. When spraying amorphous nano-crystalline iron core by the method merely, adhesion of epoxy resin degree is less, and after spraying, iron core hydraulic performance decline is more, is difficult to obtain the amorphous nano-crystalline iron core that performance is qualified.
Summary of the invention
Spray little iron core for realizing epoxy resin, it is an object of the invention to provide a kind of spraying effect good, save the time, the epoxy resin spray coating liquor reducing cost and the method utilizing this epoxy resin spray coating liquor to carry out epoxy resin spraying. Pressure air spray epoxy need to being improved, namely before spraying, little iron core to toast, and adopts the proportioning that this patent draws when joining glue.
A kind of epoxy resin spray coating liquor provided by the present invention, is made up of the component of following portions by weight ratio:
Epoxy resin 100 weight portion,
Firming agent 30 weight portion,
Dimethylbenzene 10-30 weight portion.
Described firming agent is the phenolic aldehyde amine epoxy curing agent meeting HG/T3875-2006.
Described epoxy resin is preferably the bisphenol A type epoxy resin meeting GB/T13657 1992.
A kind of epoxy resin spraying method provided by the invention, comprises the steps:
1) one side of matrix to be sprayed is sprayed the epoxy resin spray coating liquor described in any one in claim 1-3;
2) by the matrix after spraying at 100 DEG C 120 DEG C baking time 15min 30min;
3) by step 2) baking after matrix turn-over after according to step 1)-2) and method spraying another side.
Preferably, described in step 2) terminate after, repeat step 1) and step 2) 4-5 time, it is preferable that 4 times; Described step 3) terminate after, repeat step 3) 3-5 time, it is preferable that 3 times.
Preferably, described step 1) in also include, in spraying claim 1-3 before epoxy resin spray coating liquor described in any one, matrix to be sprayed is toasted 15min 30min at 100 DEG C 120 DEG C.
In a technical scheme of the present invention, described matrix to be sprayed is amorphous iron core.
The useful technique effect of the present invention: the present invention have passed through one or many spraying process, prepares epoxy coating at matrix surface; Coating after-baking procedure of processing. The present invention is by adopting the spray coating liquor spray epoxy layer of the present invention, it is possible to spray epoxy layer on such as amorphous nano-crystalline iron core matrix.
Original amorphous nano-crystalline iron core adopts and protects box packaging, not only waste material but also take a lot of work and client uses and can waste copper cash. Reduced the packing cost of amorphous nano-crystalline iron core by spray epoxy technology, accelerate the packing processes time of amorphous nano-crystalline iron core.
It addition, present invention optimizes the proportioning of the technique of spraying and spray coating liquor, improve the performance after the spray epoxy of amorphous nano-crystalline iron core.
Detailed description of the invention
Embodiment 1,
30 amorphous nano-crystalline iron cores that the present embodiment is 16/21*10 with model do matrix, carry out spray epoxy, heat treated iron core are turned over direct pallet after heat treatment complete primary school iron core, spray ring epoxy resins after turning over.
The operation of concrete spray ring epoxy resins is:
1, joining glue: according to part by weight be: epoxy resin: firming agent: dimethylbenzene=100:30:30 joins glue, mix homogeneously obtains epoxy resin colloid. Firming agent is the phenolic aldehyde amine epoxy curing agent meeting HG/T3875-2006, and the present embodiment uses the 7002B firming agent rising insulant company limited purchased from Boluo County's rising sun. Above-mentioned epoxy resin is the bisphenol A type epoxy resin meeting GB/T13657 1992, and the present embodiment uses the 7001AG epoxy resin rising insulant company limited purchased from Boluo County's rising sun.
2, with the naked amorphous iron core of HT35 iron core measuring instrument detection 16/21*10. After the naked amorphous iron core that model is 16,/21,*10 110 DEG C toasts, (adopting aerial spraying, spray parameters is the epoxy resin colloid that direct spraying step 1 is joined: air pump pressure is 0.55MPa, and gun slot and iron core vertical dimension are 30cm. During spray epoxy, S line walked by spray gun, and the often time used by dish iron core that sprays is 45 seconds.
3, after spray epoxy, toast 15 minutes at 110 DEG C.
4, step operation described in this 2-3 repeats 4 times for another example.
5, sprayed after one side dries according to step 1-4, turned over, then with epoxy resin colloid spray another side described in step 1, spraying coating process with step 2, each after spray all 110 DEG C of bakings 15 minutes, repeat 3 times this step glue sprayings and terminate.
6, by properties of sample after the detection spraying of HT35 iron core measuring instrument. Wherein the performance of 10 samples is as shown in table 3, and result shows the spraying coating process by the present invention, it is thus achieved that the performance change of the iron core after spraying is small, still conforms to requirement.
Table 1: sample detection result
Wherein sample passes standard is: 0.3mV.
Embodiment 2,
The present embodiment with model be 16/21*10 30 amorphous iron cores for matrix, carry out spray epoxy, heat treated iron core turned over by direct pallet after heat treatment complete primary school iron core, spray ring epoxy resins after turning over.
The operation of concrete spray ring epoxy resins is:
1, joining glue: according to part by weight be: epoxy resin: firming agent: dimethylbenzene=100:30:10 joins glue, mix homogeneously obtains epoxy resin colloid. Firming agent is the phenolic aldehyde amine epoxy curing agent meeting HG/T3875-2006, and the present embodiment uses the 7002B firming agent rising insulant company limited purchased from Boluo County's rising sun. Above-mentioned epoxy resin is the bisphenol A type epoxy resin meeting GB/T13657 1992, and the present embodiment uses the 7001AG epoxy resin rising insulant company limited purchased from Boluo County's rising sun.
2, after naked amorphous iron core 120 DEG C toasts, (adopting aerial spraying, spray parameters is the epoxy resin colloid that direct spraying step 1 is joined: air pump pressure is 0.55MPa, and gun slot and iron core vertical dimension are 30cm. During spray epoxy, S line walked by spray gun, and the often time used by dish iron core that sprays is 45 seconds).
3, after spray epoxy, toast 15 minutes at 120 DEG C.
4, step operation described in this 1-3 repeats 4 times for another example.
5, sprayed after one side dries according to step 1-4, turned over, then with epoxy resin colloid spray another side described in step 1, spraying coating process with step 2, each after spray all 120 DEG C of bakings 15 minutes, repeat 3 times this step glue sprayings and terminate.
6, by properties of sample after the detection spraying of HT35 iron core measuring instrument. Wherein the performance of 10 samples is as shown in table 2, and result shows the spraying coating process by the present invention, it is thus achieved that the performance change of the iron core after spraying is small, still conforms to requirement.
Table 2: sample detection result
Wherein sample passes standard is: 0.3mV.
Embodiment 3,
The present embodiment with model be 16/21*10 30 amorphous iron cores for matrix, carry out spray epoxy, heat treated iron core turned over by direct pallet after heat treatment complete primary school iron core, spray ring epoxy resins after turning over.
The operation of concrete spray ring epoxy resins is:
1, joining glue: according to part by weight be: epoxy resin: firming agent: dimethylbenzene=100:30:20 joins glue, mix homogeneously obtains epoxy resin colloid. Firming agent is the phenolic aldehyde amine epoxy curing agent meeting HG/T3875-2006, and the present embodiment uses the 7002B firming agent rising insulant company limited purchased from Boluo County's rising sun. Above-mentioned epoxy resin is the bisphenol A type epoxy resin meeting GB/T13657 1992, and the present embodiment uses the 7001AG epoxy resin rising insulant company limited purchased from Boluo County's rising sun.
2, after naked amorphous iron core 100 DEG C toasts, (adopting aerial spraying, spray parameters is the epoxy resin colloid that direct spraying step 1 is joined: air pump pressure is 0.55MPa, and gun slot and iron core vertical dimension are 30cm. During spray epoxy, S line walked by spray gun, and the often time used by dish iron core that sprays is 45 seconds).
3, after spray epoxy, toast 30 minutes at 100 DEG C.
4, step operation described in this 1-3 repeats 4 times for another example.
5, sprayed after one side dries according to step 1-4, turned over, then with epoxy resin colloid spray another side described in step 1, spraying coating process with step 2, each after spray all 100 DEG C of bakings 30 minutes, repeat 3 times this step glue sprayings and terminate.
6, by properties of sample after the detection spraying of HT35 iron core measuring instrument. Wherein the performance of 10 samples is as shown in table 3, and result shows the spraying coating process by the present invention, it is thus achieved that the performance change of the iron core after spraying is small, still conforms to requirement.
Table 3: sample detection result
Wherein sample passes standard is: 0.3mV.
Claims (7)
1. an epoxy resin spray coating liquor, is made up of the component of following portions by weight ratio:
Epoxy resin 100 weight portion,
Firming agent 30 weight portion,
Dimethylbenzene 10-30 weight portion.
2. epoxy resin spray coating liquor according to claim 1, it is characterised in that: described firming agent is phenolic aldehyde amine epoxy curing agent.
3. epoxy resin spray coating liquor according to claim 1 and 2, it is characterised in that: described epoxy resin is bisphenol A type epoxy resin.
4. an epoxy resin spraying method, comprises the steps:
1) one side of matrix to be sprayed is sprayed the epoxy resin spray coating liquor described in any one in claim 1-3;
2) matrix after spraying is toasted 15min 30min at 100 DEG C 120 DEG C;
3) by step 2) baking after matrix turn-over after according to step 1)-2) and method spraying another side.
5. method according to claim 4, it is characterised in that: described in step 2) terminate after, repeat step 1) and step 2) 4-5 time, it is preferable that 4 times; Described step 3) terminate after, repeat step 3) 3-5 time, it is preferable that 3 times.
6. method according to claim 5, it is characterised in that: described step 1) in also include, in spraying claim 1-3 before epoxy resin spray coating liquor described in any one, matrix to be sprayed is toasted 15min 30min at 100 DEG C 120 DEG C.
7. method according to any one in claim 4-6, described matrix to be sprayed is amorphous iron core.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410619256.0A CN105623462A (en) | 2014-11-06 | 2014-11-06 | Epoxy resin spray-coating method and special-purpose epoxy resin spray-coating liquid thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410619256.0A CN105623462A (en) | 2014-11-06 | 2014-11-06 | Epoxy resin spray-coating method and special-purpose epoxy resin spray-coating liquid thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105623462A true CN105623462A (en) | 2016-06-01 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410619256.0A Pending CN105623462A (en) | 2014-11-06 | 2014-11-06 | Epoxy resin spray-coating method and special-purpose epoxy resin spray-coating liquid thereof |
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| Country | Link |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115820186A (en) * | 2022-11-29 | 2023-03-21 | 无锡荷雨新能源科技有限公司 | Preparation method of novel spray glue for wind power blade |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2796044Y (en) * | 2005-05-16 | 2006-07-12 | 黄付贵 | Shock-proof structure of nano crystal soft magnetic core |
| CN102069062A (en) * | 2011-01-26 | 2011-05-25 | 湘潭市台日电气科技有限公司 | Paint dipping process for amorphous CD type iron core |
| CN102755955A (en) * | 2012-07-31 | 2012-10-31 | 东莞市晶磁科技有限公司 | Amorphous magnetic core surface coating process |
| CN103128039A (en) * | 2011-12-01 | 2013-06-05 | 上海电气集团股份有限公司 | Coating method of winding amorphous iron core insulating coating |
-
2014
- 2014-11-06 CN CN201410619256.0A patent/CN105623462A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2796044Y (en) * | 2005-05-16 | 2006-07-12 | 黄付贵 | Shock-proof structure of nano crystal soft magnetic core |
| CN102069062A (en) * | 2011-01-26 | 2011-05-25 | 湘潭市台日电气科技有限公司 | Paint dipping process for amorphous CD type iron core |
| CN103128039A (en) * | 2011-12-01 | 2013-06-05 | 上海电气集团股份有限公司 | Coating method of winding amorphous iron core insulating coating |
| CN102755955A (en) * | 2012-07-31 | 2012-10-31 | 东莞市晶磁科技有限公司 | Amorphous magnetic core surface coating process |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115820186A (en) * | 2022-11-29 | 2023-03-21 | 无锡荷雨新能源科技有限公司 | Preparation method of novel spray glue for wind power blade |
| CN115820186B (en) * | 2022-11-29 | 2024-08-20 | 无锡荷雨新能源科技有限公司 | Preparation method of novel spray adhesive for wind power blade |
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Application publication date: 20160601 |
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