CN105561821B - A kind of mixer catalyst charging device - Google Patents

A kind of mixer catalyst charging device Download PDF

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Publication number
CN105561821B
CN105561821B CN201410532203.5A CN201410532203A CN105561821B CN 105561821 B CN105561821 B CN 105561821B CN 201410532203 A CN201410532203 A CN 201410532203A CN 105561821 B CN105561821 B CN 105561821B
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Prior art keywords
pipe
catalyst
feed pipe
feed
mixer
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CN201410532203.5A
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CN105561821A (en
Inventor
张英民
李德华
杨刚
田智英
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QINGDAO DOUBLE-PEACH SPECIALITY CHEMICALS GROUP Co Ltd
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QINGDAO DOUBLE-PEACH SPECIALITY CHEMICALS GROUP Co Ltd
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Abstract

The present invention relates to a kind of mixer catalyst charging devices, including the first feed pipe and catalyst commissioning pipe, one end of the catalyst commissioning pipe is stretched into first feed pipe, it is fixed with support device in one end that the catalyst commissioning pipe stretches into the first feed pipe, the support device and the inner wall of first feed pipe overlap.The present invention is by avoiding catalyst commissioning pipe from being broken, it effectively prevents making impact of the catalyst to mixer cover flange because of the fracture of catalyst commissioning pipe, and catalyst is prevented to mix the corrosion that uniformity formation phosphoric acid is not achieved to cover flange with acetic acid steam after the fracture of catalyst commissioning pipe, the service life of cover flange is improved, and improves mixed effect.

Description

A kind of mixer catalyst charging device
Technical field
The present invention relates to a kind of charging device, more particularly to a kind of mixer catalyst charging device.
Background technology
Acetic acid steam and diammonium hydrogen phosphate catalyst solution, which reach mean value and mix, at present needs to use mixer, the prior art In mixer catalyst commissioning pipe one end stretch into the first feed pipe and feed intake, find that catalyst commissioning pipe is easy afterwards by long-term use It produces fracture.It is that one end is fixed, and stretches into one end in the first feed pipe that the reason of it is broken, which is catalyst commissioning pipe, Do not fix, catalyst commissioning pipe forms the longer cantilever beam of length, vibrated under the higher flow velocity impact of acetic acid steam and Fracture.After its fracture, diammonium hydrogen phosphate catalyst solution can impact the cover flange of mixer, cause cover flange Corrosion, diammonium hydrogen phosphate catalyst solution, which mixes after the fracture of catalyst commissioning pipe with acetic acid steam, is not achieved uniformity formation phosphorus Acid exacerbates the corrosion of cover flange.It finds to need replacing the cover flange being once corroded in average every 2 to 3 months in use.
Invention content
Present invention is primarily aimed at solving the above problems, providing one kind can avoid catalyst commissioning pipe from being broken, and improve The mixer catalyst charging device of the mixed effect of mixer cover flange service life and catalyst in acetic acid steam.
To achieve the above object, the technical scheme is that:
A kind of mixer catalyst charging device, including the first feed pipe and catalyst commissioning pipe, the catalyst feed intake One end of pipe is stretched into first feed pipe, and support is fixed in one end that the catalyst commissioning pipe stretches into the first feed pipe Device, the support device and the inner wall of first feed pipe overlap.
Further, further include the second feed pipe, second feed pipe is fixed on the first charging pipe outer wall, described The catalyst commissioning pipe, the end of catalyst commissioning pipe one end and second feed pipe are provided in second feed pipe Fixed, the other end stretches into first feed pipe.
Further, the outer diameter of the catalyst commissioning pipe is equal with the inner diameter of the second feed pipe.
Further, the catalyst commissioning pipe stretches into the end setting of first feed pipe one end in first charging The discharging direction of the pipe axial location of pipe, the catalyst commissioning pipe is parallel with the discharging direction of the first feed pipe.
Further, there is certain angle, the catalyst to throw between the catalyst commissioning pipe and first feed pipe One end that expects pipe stretches into first feed pipe is bent in the pipe axial location of first feed pipe, and the catalyst feeds intake Part after pipe bending extends along the pipe axis of the first feed pipe.
Further, the end of the catalyst commissioning pipe is provided with fog-spray nozzle.
Further, the spray direction of the fog-spray nozzle is identical as the discharging direction of the first feed pipe.
Further, the support device includes two holders, the end of every holder one end and the catalyst commissioning pipe Fixed, the inner wall of the other end and first feed pipe overlaps, and the angle of two holders in the horizontal direction is 180 °.
Further, the support device includes three holders, the end of every holder one end and the catalyst commissioning pipe Fixed, the inner wall of the other end and first feed pipe overlaps.
Further, the angle of every two holders in the horizontal direction is 120 °.
A kind of to sum up content, mixer catalyst charging device of the present invention, has the following advantages that:
1, by stretching into one end fixed support device of the first feed pipe in catalyst commissioning pipe, to make catalyst feed intake Pipe is changed to simply supported beam form by original cantilever beam form, effectively avoids the fracture of catalyst commissioning pipe.
2, it is connected by the interference fit between catalyst commissioning pipe and the second feed pipe, makes the cantilever of catalyst commissioning pipe Beam shortens (its cantilever beam length is only to stretch into the part of the first feed pipe), if support device can not support catalyst to feed intake Pipe, then catalyst commissioning pipe also can effectively be avoided to be broken since cantilever beam is shorter.
3, it by avoiding catalyst commissioning pipe from being broken, effectively prevents making catalyst to mixing because of the fracture of catalyst commissioning pipe The impact of device cover flange, and prevent catalyst to be mixed with acetic acid steam after the fracture of catalyst commissioning pipe and be not achieved uniformly Degree forms corrosion of the phosphoric acid to cover flange, improves the service life of cover flange.
4, the pipe axial location by catalyst commissioning pipe in the first feed pipe is bent, and is extended along pipe axis, is made Catalyst solution from catalyst commissioning pipe outflow after be located at the first feed pipe shaft core position, and with the acetic acid of the first feed pipe Steam steam flow direction is parallel, is conducive to the mixing of catalyst solution and acetic acid steam, improves mixed effect.
Description of the drawings
Fig. 1 is the structural schematic diagram of the present invention.
As shown in Figure 1, the first feed pipe 1, the second feed pipe 2, catalyst commissioning pipe 3, holder 4, fog-spray nozzle 5, mixer Cylinder 6, shell flange 7, cover flange 8, mounting flange 9.
Specific implementation mode
Present invention is further described in detail with specific implementation mode below in conjunction with the accompanying drawings:
As shown in Figure 1, a kind of mixer catalyst charging device, including the first feed pipe 1, the second feed pipe 2 and catalysis Agent commissioning pipe 3, wherein the first feed pipe 1 is for conveying acetic acid steam, the second feed pipe 2 is for conveying diammonium hydrogen phosphate catalyst Solution.
Mixer tube 6 is fixed by the shell flange 7 being arranged on cylinder body outer wall with cover flange 8, in cover flange 8 Center location fix the first feed pipe 1, acetic acid steam passes through the first feed pipe 1 and enters mixer tube 6.In the first feed pipe The second feed pipe 2 is fixed on 1 outer wall, the second feed pipe 2 is arranged by certain angle of inclination, is provided in the second feed pipe 2 Catalyst commissioning pipe 3, the top end of catalyst commissioning pipe 3 and the top of the second feed pipe 2 are fixed by mounting flange 9, are urged The bottom end of agent commissioning pipe 3 is stretched into the first feed pipe 1, and diammonium hydrogen phosphate catalyst solution is conveyed into mixer tube 6.
Tip position in the bottom end of catalyst commissioning pipe 3 is fixed with support device, and support device includes two holders 4, 4 one end of holder and the bottom end end of catalyst commissioning pipe 3 are welded and fixed, the inner wall overlap joint of the other end and the first feed pipe 1, two The angle of holder 4 in the horizontal direction is 180 °.The bottom end of catalyst commissioning pipe 3 is set to be overlapped on by two holders 4 On the inner wall of one feed pipe 1, to make catalyst commissioning pipe 3 be changed to simply supported beam form by original cantilever beam form, first Shaking is not will produce in the case that 1 acetic acid steam flow rate of feed pipe is larger, effectively avoids the fracture of catalyst commissioning pipe 3.
Support device can also be that three holders 4, every 4 one end of holder and the bottom end end of catalyst commissioning pipe 3 weld Fixed, the inner wall of the other end and the first feed pipe 1 overlaps, and the angle of every two holders 4 in the horizontal direction is 120 °.Using three Root holder 4 can make overlap joint more secured.Holder 4 should not be arranged excessively, and excessive holder 4 can influence the charging of the first feed pipe 1 Effect.
Holder 4 is overlapped rather than is welded and fixed with the first feed pipe 1, is because the acetic acid vapor (steam) temperature of the first feed pipe 1 reaches To 300-400 DEG C, since acetic acid vapor (steam) temperature is higher, solder joint is caused to be broken so holder 4 will produce to expand with heat and contract with cold, and solder joint The corrosion of 1 inner wall of the first feed pipe and cover flange 8 is easily caused after fracture.
The outer diameter of catalyst commissioning pipe 3 is equal with the inner diameter of the second feed pipe 2, passes through catalyst commissioning pipe 3 With the interference fit of 2 holder of the second feed pipe, the expansion of catalyst commissioning pipe 3 is set to be connected in the second feed pipe 2, catalyst feeds intake The cantilever beam of pipe 3 shortens, and cantilever beam length is only to stretch into the part of the first feed pipe 1, if support device damage can not be Catalyst commissioning pipe 3 is supported, then can also effectively avoid catalyst since the cantilever beam of catalyst commissioning pipe 3 is shorter Commissioning pipe 3 is broken.
The end that catalyst commissioning pipe 3 stretches into 1 one end of the first feed pipe is arranged in the pipe axis position of the first feed pipe 1 It sets, the discharging direction of catalyst commissioning pipe 3 is parallel with the discharging direction of the first feed pipe 1, and catalyst solution is made to be thrown from catalyst Expects pipe 3 flow out position the first feed pipe 1 shaft core position, and catalyst solution from catalyst commissioning pipe 3 outflow after Discharging direction is parallel from the discharging direction after the outflow of the first feed pipe 1 with acetic acid steam, is conducive to catalyst and acetic acid steam Mixing.
As shown in Figure 1, by this present embodiment, the second feed pipe 2 and catalyst commissioning pipe 3 are set by certain angle of inclination It sets, there are certain angle between the first feed pipe 1, the acetic acid steam flowed out from the first feed pipe 1 feeds intake with from catalyst The catalyst that pipe 3 flows out flows to not parallel in mixing, affects mixed effect, so in the present embodiment, catalyst is thrown One end that expects pipe 3 stretches into the first feed pipe 1 is bent in the pipe axial location of the first feed pipe 1, and the catalyst after bending feeds intake Pipe 3 extends along the pipe axis of the first feed pipe 1, i.e., the axis and the first feed pipe 1 of part after the bending of catalyst commissioning pipe 3 Pipe axis overlap.Make catalyst solution after the outflow of catalyst commissioning pipe 3 with this configuration, is not only located at the first feed pipe 1 shaft core position, it is also parallel with the discharging direction of acetic acid steam flowed out from the first feed pipe 1, be conducive to catalyst and acetic acid The mixing of steam.
Support device also acts certain booster action herein, ensure that catalyst commissioning pipe 3 not by support device It shakes, the end of catalyst commissioning pipe 3 is enable to be maintained at the pipe axial location of the first feed pipe 1.
The part that catalyst commissioning pipe 3 extends after bending is stretched into mixer tube 6, is stretched into catalyst commissioning pipe 3 mixed Fog-spray nozzle 5, the discharging direction phase in the spray direction and the first feed pipe 1 of fog-spray nozzle 5 are provided on end in clutch cylinder 6 Together.
In conclusion since support device is arranged, keep catalyst commissioning pipe 3 not easy to break, by avoiding catalyst from feeding intake Pipe 3 is broken, and makes catalyst solution when entering mixer, will not carry out torrent impact to the first feed pipe 1 and cover flange 8, And since catalyst commissioning pipe 3 is not broken to make to be uniformly mixed so that the mixing of acetic acid steam and catalyst reaches uniform Degree avoids corroding cover flange 8 because mixing uneven formation phosphoric acid, greatly improves envelope to form ammonium phosphate The service life of head flange 8.Pipe axial location by catalyst commissioning pipe 3 in the first feed pipe 1 is bent, and along pipe axis Line extends, and so that catalyst solution is located at the shaft core position of the first feed pipe 1 after the outflow of catalyst commissioning pipe 3, and with first The acetic acid steam steam flow direction of feed pipe 1 is parallel, is conducive to the mixing of catalyst solution and acetic acid steam, improves mixing effect Fruit.
As described above, the plan content in conjunction with given by attached drawing, can derive similar technical solution.In every case it is not de- Content from technical solution of the present invention, according to the technical essence of the invention to made by above example it is any it is simple modification, etc. With variation and modification, in the range of still falling within technical solution of the present invention.

Claims (8)

1. a kind of mixer catalyst charging device, including the first feed pipe (1) and catalyst commissioning pipe (3), the catalyst One end of commissioning pipe (3) is stretched into first feed pipe (1), it is characterised in that:Is stretched into the catalyst commissioning pipe (3) One end of one feed pipe (1) is fixed with support device, and the support device and the inner wall of first feed pipe (1) overlap;
Further include the second feed pipe (2), second feed pipe (2) is fixed on the first feed pipe (1) outer wall, described It is provided with the catalyst commissioning pipe (3) in two feed pipes (2), the end of described catalyst commissioning pipe (3) one end and described the Two feed pipes (2) are fixed, and the other end stretches into first feed pipe (1);
The outer diameter of the catalyst commissioning pipe (3) is equal with the inner diameter of the second feed pipe (2);
The end of described catalyst commissioning pipe (3) one end is fixed by mounting flange (9) with the top of the second feed pipe (2).
2. a kind of mixer catalyst charging device according to claim 1, it is characterised in that:The catalyst commissioning pipe (3) the pipe axial location of the end setting in first feed pipe (1) of described first feed pipe (1) one end is stretched into, it is described The discharging direction of catalyst commissioning pipe (3) is parallel with the discharging direction of the first feed pipe (1).
3. a kind of mixer catalyst charging device according to claim 2, it is characterised in that:The catalyst commissioning pipe (3) there is certain angle, the catalyst commissioning pipe (3) to stretch into first feed pipe between first feed pipe (1) (1) one end is bent in the pipe axial location of first feed pipe (1), the portion after catalyst commissioning pipe (3) bending The pipe axis along the first feed pipe (1) is divided to extend.
4. a kind of mixer catalyst charging device according to claim 1, it is characterised in that:It feeds intake in the catalyst The end of pipe (3) is provided with fog-spray nozzle (5).
5. a kind of mixer catalyst charging device according to claim 4, it is characterised in that:The fog-spray nozzle (5) It is identical as the discharging direction of the first feed pipe (1) to spray direction.
6. a kind of mixer catalyst charging device according to claim 1, it is characterised in that:The support device includes Two holders (4), every holder (4) one end and the end of the catalyst commissioning pipe (3) are fixed, the other end with described first into The inner wall of expects pipe (1) overlaps, and the angle of two holders (4) in the horizontal direction is 180 °.
7. a kind of mixer catalyst charging device according to claim 1, it is characterised in that:The support device includes Three holders (4), every holder (4) one end and the end of the catalyst commissioning pipe (3) are fixed, the other end with described first into The inner wall of expects pipe (1) overlaps.
8. a kind of mixer catalyst charging device according to claim 7, it is characterised in that:Every two holders (4) angle in the horizontal direction is 120 °.
CN201410532203.5A 2014-10-10 2014-10-10 A kind of mixer catalyst charging device Active CN105561821B (en)

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Application Number Priority Date Filing Date Title
CN201410532203.5A CN105561821B (en) 2014-10-10 2014-10-10 A kind of mixer catalyst charging device

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Application Number Priority Date Filing Date Title
CN201410532203.5A CN105561821B (en) 2014-10-10 2014-10-10 A kind of mixer catalyst charging device

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CN105561821A CN105561821A (en) 2016-05-11
CN105561821B true CN105561821B (en) 2018-07-20

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0477846A1 (en) * 1990-09-25 1992-04-01 Praxair Technology, Inc. Improved in-line gas/liquid dispersion
CN1265338A (en) * 1999-01-26 2000-09-06 英国石油化学品有限公司 Apparatus for adding fluid into process material flow
CN201678720U (en) * 2010-05-17 2010-12-22 朝阳金达钛业有限责任公司 Titanium sponge reactor feeding tube structure
CN204121993U (en) * 2014-10-10 2015-01-28 青岛双桃精细化工(集团)有限公司 A kind of blender catalyst charging device

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0477846A1 (en) * 1990-09-25 1992-04-01 Praxair Technology, Inc. Improved in-line gas/liquid dispersion
CN1265338A (en) * 1999-01-26 2000-09-06 英国石油化学品有限公司 Apparatus for adding fluid into process material flow
CN201678720U (en) * 2010-05-17 2010-12-22 朝阳金达钛业有限责任公司 Titanium sponge reactor feeding tube structure
CN204121993U (en) * 2014-10-10 2015-01-28 青岛双桃精细化工(集团)有限公司 A kind of blender catalyst charging device

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Inventor after: Zhang Yingmin

Inventor after: Li Dehua

Inventor after: Yang Gang

Inventor after: Tian Zhiying

Inventor before: Zhang Yingmin

Inventor before: Li Dehua

Inventor before: Tian Zhiying

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