CN105561618A

CN105561618A - Simple laboratory rectifier

Info

Publication number: CN105561618A
Application number: CN201510947820.6A
Authority: CN
Inventors: 陆世红; 资炎
Original assignee: XUZHOU HUASHENG BIOLOGICAL TECHNOLOGY Co Ltd
Current assignee: XUZHOU HUASHENG BIOLOGICAL TECHNOLOGY Co Ltd
Priority date: 2015-12-17
Filing date: 2015-12-17
Publication date: 2016-05-11

Abstract

The invention relates to a simple laboratory rectifier. The simple laboratory rectifier comprises a distillation bottle, a bottle neck, a heat preservation jacket, a condensation pipe, a condenser, an overflow pipe, a thermometer, a heating jacket, a number-one stripping bottle, a number-two stripping bottle and a collection pipe, wherein the distillation bottle and the bottle neck collectively form a matrass, the heating jacket is arranged outside the distillation bottle, the heat preservation jacket is arranged on the periphery of the bottle neck, a bottle plug is arranged at a bottle opening of the matrass, the thermometer is inserted into the bottle plug, the overflow pipe is arranged at one side of the bottle neck and disposed on the top of the heat preservation jacket, the overflow pipe obliquely stretches upwards to form an angle of 30 to 50 degrees with the horizontal line, the overflow pipe, the condensation pipe (4) and the collection pipe form a herringbone structure, the axis of the condensation pipe is parallel to that of the bottle neck, and the number-one stripping bottle and the number-two stripping bottle are sequentially arranged at the lower side of the collection pipe. The simple laboratory rectifier is simple in structure and convenient to adjust; and the modification can be completed by utilizing the existing experimental apparatuses, so that the experimental requirements of a laboratory are met, and the cost is saved.

Description

A kind of simple experiment room rectifier

Technical field

The present invention relates to a kind of experiment rectifier.

Background technology

In chemical synthesis, the purification of some materials uses Distallation systm usually, all there is sale in common distillation equipment market, but then needs customized to some unconventional rectifying devices, be not the commodity of common wilderness demand in addition, therefore cost is higher, and not easily adjusts according to actual needs.

Summary of the invention

A kind of simple experiment room rectifier, disclose for solving the problem exactly and be a kind ofly different from routine and be easy to the experiment rectifier unit that adjusts, the present invention includes: cucurbit (1), bottleneck (2), insulation jacket (3), condenser pipe (4), condenser (4 '), discharger (5), thermometer (6), heating jacket (7), No. one carry heat up in a steamer bottle (8), No. two carry and heat up in a steamer bottle (9) and collecting pipe (10), it is characterized in that: described cucurbit (1) and bottleneck (2) form long-neck cucurbit jointly, its cucurbit (1) outer setting heating jacket (7), the periphery of bottleneck (2) arranges insulation jacket (3), the bottle mouth position of this long-neck cucurbit arranges bottle stopper, bottle stopper inserts thermometer (6), described discharger (5) is arranged on the side of bottleneck (2), and be in the top of insulation jacket (3), discharger (5) is upward to be stretched, it is 30 ~ 45 ° with horizontal line angle, discharger (5) forms " people " font structure with condenser pipe (4) and collecting pipe (10), described condenser pipe (4) its axial line and the axis parallel of bottleneck (2), junction between collecting pipe (10) and condenser pipe (4) and discharger (5) is a downward-sloping ramp shaped connecting portion, the end opening of condenser pipe (4) is in the scope suitable for reading of this connecting portion completely, condenser pipe arranges condenser (4 ') in (4), the downside of collecting pipe (10) once arranges No. one and carries and heat up in a steamer bottle (8) and No. two and carry and heat up in a steamer bottle (9).

The invention has the advantages that: structure is simple, easy to adjust, uses existing experiment equipment to complete transformation, meets the experiment demand in laboratory, cost-saving.

Accompanying drawing explanation

See accompanying drawing, Fig. 1 is structural representation of the present invention.

As shown in the figure, the present invention includes: (1) cucurbit, (2) bottleneck, (3) insulation jacket, (4) condenser pipe, (4 ') condenser, (5) discharger, (6) thermometer, (7) heating jacket, (8) No. one carry heat up in a steamer bottle, (9) No. two carry and heat up in a steamer bottle and (10) collecting pipe.

Detailed description of the invention

Below in conjunction with drawings and the specific embodiments, technical characteristic of the present invention is described further.

See accompanying drawing, carried by cucurbit (1), bottleneck (2), insulation jacket (3), condenser pipe (4), condenser (4 '), discharger (5), heating jacket (7), collecting pipe (10) and two and heat up in a steamer bottle and form main body of the present invention.

Embodiment, insert in cucurbit (1) by needing the liquid material of purifying by bottleneck, cover bottle stopper and plug thermometer (6), condenser (4 ') starts, heat to cucurbit (1) through heating jacket (7), insulation jacket (3) continues heat supply, guarantee that the temperature of steam in uphill process does not reduce because of the length of bottleneck (2), high-temperature steam is overflowed by discharger (5), rise in condenser pipe (4), liquid is condensed under the condensation of after-condenser (4 '), and along tube wall or condenser (4 ') dirty, enter the ramp shaped connecting portion of collecting pipe (10), continue to flow to collecting pipe, enter to carry and heat up in a steamer bottle, No. one, carry for No. two and heat up in a steamer the component that bottle can collect the difference section of heating up in a steamer.

Claims

1. a simple experiment room rectifier, the present invention includes: cucurbit (1), bottleneck (2), insulation jacket (3), condenser pipe (4), condenser (4 '), discharger (5), thermometer (6), heating jacket (7), No. one carry heat up in a steamer bottle (8), No. two carry and heat up in a steamer bottle (9) and collecting pipe (10), it is characterized in that: described cucurbit (1) and bottleneck (2) form long-neck cucurbit jointly, its cucurbit (1) outer setting heating jacket (7), the periphery of bottleneck (2) arranges insulation jacket (3), the bottle mouth position of this long-neck cucurbit arranges bottle stopper, bottle stopper inserts thermometer (6), described discharger (5) is arranged on the side of bottleneck (2), and be in the top of insulation jacket (3), discharger (5) is upward to be stretched, it is 30 ~ 45 ° with horizontal line angle, discharger (5) forms " people " font structure with condenser pipe (4) and collecting pipe (10).

2. a kind of simple experiment room according to claim 1 rectifier, it is characterized in that: described condenser pipe (4) its axial line and the axis parallel of bottleneck (2), junction between collecting pipe (10) and condenser pipe (4) and discharger (5) is a downward-sloping ramp shaped connecting portion, the end opening of condenser pipe (4) is in the scope suitable for reading of this connecting portion completely, condenser pipe arranges condenser (4 ') in (4), and the downside of collecting pipe (10) once arranges No. one and carries and heat up in a steamer bottle (8) and No. two and carry and heat up in a steamer bottle (9).