CN105542527A - Improved ultraviolet-proof coating and preparation method thereof - Google Patents
Improved ultraviolet-proof coating and preparation method thereof Download PDFInfo
- Publication number
- CN105542527A CN105542527A CN201511015542.7A CN201511015542A CN105542527A CN 105542527 A CN105542527 A CN 105542527A CN 201511015542 A CN201511015542 A CN 201511015542A CN 105542527 A CN105542527 A CN 105542527A
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- ultraviolet
- defoamer
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- benzyl dimethyl
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
- C09D4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09D159/00 - C09D187/00
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses an improved ultraviolet-proof coating, which is prepared from the following raw materials in parts by weight: 1.5-4 parts of benzyl dimethyl phenol polyoxyethylene ether, 0.35-0.66 part of mixed fatty alcoholsodium sulfate, 1.25-1.65 parts of an alpha-cyanoacrylate adhesive, 0.36-0.67 part of 2,4,6-trimethybenzoyl-diphenylphosphine oxide, 0.22-0.66 part of acolorant, 4-6.5 parts of potassium diphosphate, 1.23-3.25 parts of a defoaming agent, and 1.55-2.68 parts of sodium n-alkyl benzene sulfonate. The improved ultraviolet-proof coating has the following active effects: the improved ultraviolet-proof coating disclosed by the invention has a coating weight of 11.5g/cm<2>, an air permeability of 17.6kg/m<2>.s and an elongationpercentage of 45%, and has a good ultraviolet shielding effect, the transmittance of ultraviolet light with the wavelength of 40nm is 15%, and the transmittance of visible light with the wavelength of 600nm is 50%; and the alpha-cyanoacrylate adhesive has high refractivity and high optical activity, can be used as a sun screener to meet many actual needs, is suitable for various fabrics, has a certain ultraviolet shielding function, and does not influence the air and moisture permeability.
Description
Technical field
The present invention relates to a kind of coating, especially relate to anti-ultraviolet paint of a kind of improvement and preparation method thereof, belong to paint field.
Background technology
Ultraviolet is a kind of light wave larger to harm in sunlight, and during transition irradiation ultraviolet radiation, ultraviolet energy can cause skin aging, even easily cause skin carcinoma, also can cause various window curtain and floor, the fading of plastics and printed matter.Therefore people more and more pay close attention to the harm of resisting ultraviolet radiation, and particularly it can make skin produce erythema, blackspot, make skin aging, and even cause skin carcinoma, people wish that traditional clothing has certain function of shielding ultraviolet radiation, and do not affect breathable moisture permeability.
Summary of the invention
For the deficiencies in the prior art, technical problem to be solved by this invention is, provides anti-ultraviolet paint of a kind of improvement and preparation method thereof, improves ultraviolet resistance and the stability of coating, there is certain function of shielding ultraviolet radiation, and do not affect breathable moisture permeability.
For solving the problems of the technologies described above, the technical scheme that the present invention takes is, a kind of anti-ultraviolet paint of improvement, and it is made up of the raw material of following parts by weight:
Benzyl dimethyl phenol polyethenoxy ether 1.5-4 part; mixed fatty alcohol sodium sulfate 0.35-0.66 part; α-cyanoacrylate sizing agent 1.25-1.65 part; 2,4,6-trimethylbenzoy-dipheny phosphine oxide 0.36-0.67 part; tinting material 0.22-0.66 part; bisphosphate potassium 4-6.5 part, defoamer 1.23-3.25 part, linear alkylbenzene sulphonic acid 1.55-2.68 part.
Optimize, the anti-ultraviolet paint of above-mentioned improvement, it is made up of the raw material of following parts by weight:
Benzyl dimethyl phenol polyethenoxy ether 1.5 parts; 0.35 part, mixed fatty alcohol sodium sulfate; α-cyanoacrylate sizing agent 1.25 parts; 2,4,6-trimethylbenzoy-dipheny phosphine oxide 0.36 part; tinting material 0.22 part; 4 parts, bisphosphate potassium, defoamer 1.23 parts, linear alkylbenzene sulphonic acid 1.55 parts.
Optimize, the anti-ultraviolet paint of above-mentioned improvement, its tinting material is dispersed dye.
Optimize, the anti-ultraviolet paint of above-mentioned improvement, its defoamer is organic silicon modified by polyether.
A preparation method for the anti-ultraviolet paint of improvement, comprises the following steps:
1) according to said components proportioning, benzyl dimethyl phenol polyethenoxy ether, mixed fatty alcohol sodium sulfate and α-cyanoacrylate sizing agent are poured in container, adds defoamer, access heat-treating machine, keep vapor temperature >=100 DEG C, after 10-15min thermal treatment, naturally cool to room temperature;
2) then 2,4,6-trimethylbenzoy-dipheny phosphine oxide and tinting material are pressed formula rate, put in container, carry out initial filter with diatomite filter, its filter pressure is to≤0.1 MPa, and transmittance reaches more than 96%;
3) in reaction vessel, add bisphosphate potassium, carry out dispersion with 400-500r/min and stir 20-25min;
4) then reduce rotating speed and add linear alkylbenzene sulphonic acid, carry out dispersion with 300-400r/min and stir 15min;
5) with high pressure homogenizer under 8.8-9.6MPa pressure, make suspended particles pressurized and broken, suspension grain disperseed equably, after cooling, is finished product.
The present invention has following positive effect: paint coatings amount 11.5g/cm of the present invention
2, Air permenbility is 17.6kg/m
2s, elongation is 45%, has good ultraviolet shielding effect, and the uv transmittance of wavelength 40nm is 15%, is 50% to the transmitance of the visible ray of wavelength 600nm; α-cyanoacrylate sizing agent has high refractivity and high photolytic activity, can be used as sun-screening agent, solves a lot of actual needs, is applicable to various fabric, has certain function of shielding ultraviolet radiation, and do not affect breathable moisture permeability.
Embodiment
Below in conjunction with embodiment, invention is further described.
Embodiment 1
The present invention is a kind of anti-ultraviolet paint of improvement; it is made up of the raw material of following parts by weight: benzyl dimethyl phenol polyethenoxy ether 1.5 parts; 0.35 part, mixed fatty alcohol sodium sulfate, α-cyanoacrylate sizing agent 1.25 parts, 2; 4; 6-trimethylbenzoy-dipheny phosphine oxide 0.36 part, tinting material and dispersed dye 0.22 part, 4 parts, bisphosphate potassium; defoamer and organic silicon modified by polyether 1.23 parts, linear alkylbenzene sulphonic acid 1.55 parts.
A preparation method for the anti-ultraviolet paint of improvement, comprises the following steps:
1) according to said components proportioning, benzyl dimethyl phenol polyethenoxy ether, mixed fatty alcohol sodium sulfate and α-cyanoacrylate sizing agent are poured in container, adds defoamer, access heat-treating machine, keep vapor temperature >=100 DEG C, after 10min thermal treatment, naturally cool to room temperature;
2) then 2,4,6-trimethylbenzoy-dipheny phosphine oxide and tinting material are pressed formula rate, put in container, carry out initial filter with diatomite filter, its filter pressure is to≤0.1 MPa, and transmittance reaches more than 96%;
3) in reaction vessel, add bisphosphate potassium, carry out dispersion with 400r/min and stir 20min;
4) then reduce rotating speed and add linear alkylbenzene sulphonic acid, carry out dispersion with 300r/min and stir 15min;
5) with high pressure homogenizer under 8.8MPa pressure, make suspended particles pressurized and broken, suspension grain disperseed equably, after cooling, is finished product.
Embodiment 2
The present invention is a kind of anti-ultraviolet paint of improvement; it is made up of the raw material of following parts by weight: benzyl dimethyl phenol polyethenoxy ether 4 parts; 0.66 part, mixed fatty alcohol sodium sulfate, α-cyanoacrylate sizing agent 1.65 parts, 2; 4; 6-trimethylbenzoy-dipheny phosphine oxide 0.67 part, tinting material and dispersed dye 0.66 part, 6.5 parts, bisphosphate potassium; defoamer and organic silicon modified by polyether 3.25 parts, linear alkylbenzene sulphonic acid 2.68 parts.
A preparation method for the anti-ultraviolet paint of improvement, comprises the following steps:
1) according to said components proportioning, benzyl dimethyl phenol polyethenoxy ether, mixed fatty alcohol sodium sulfate and α-cyanoacrylate sizing agent are poured in container, adds defoamer, access heat-treating machine, keep vapor temperature >=100 DEG C, after 12min thermal treatment, naturally cool to room temperature;
2) then 2,4,6-trimethylbenzoy-dipheny phosphine oxide and tinting material are pressed formula rate, put in container, carry out initial filter with diatomite filter, its filter pressure is to≤0.1 MPa, and transmittance reaches more than 96%;
3) in reaction vessel, add bisphosphate potassium, carry out dispersion with 450r/min and stir 22min;
4) then reduce rotating speed and add linear alkylbenzene sulphonic acid, carry out dispersion with 350r/min and stir 15min;
5) with high pressure homogenizer under 8.9MPa pressure, make suspended particles pressurized and broken, suspension grain disperseed equably, after cooling, is finished product.
Embodiment 3
The present invention is a kind of anti-ultraviolet paint of improvement; it is made up of the raw material of following parts by weight: benzyl dimethyl phenol polyethenoxy ether 2.7 parts; 0.46 part, mixed fatty alcohol sodium sulfate, α-cyanoacrylate sizing agent 1.45 parts, 2; 4; 6-trimethylbenzoy-dipheny phosphine oxide 0.47 part, tinting material and dispersed dye 0.43 part, 5.6 parts, bisphosphate potassium; defoamer and organic silicon modified by polyether 2.37 parts, linear alkylbenzene sulphonic acid 2.25 parts.
A preparation method for the anti-ultraviolet paint of improvement, comprises the following steps:
1) according to said components proportioning, benzyl dimethyl phenol polyethenoxy ether, mixed fatty alcohol sodium sulfate and α-cyanoacrylate sizing agent are poured in container, adds defoamer, access heat-treating machine, keep vapor temperature >=100 DEG C, after 15min thermal treatment, naturally cool to room temperature;
2) then 2,4,6-trimethylbenzoy-dipheny phosphine oxide and tinting material are pressed formula rate, put in container, carry out initial filter with diatomite filter, its filter pressure is to≤0.1 MPa, and transmittance reaches more than 96%;
3) in reaction vessel, add bisphosphate potassium, carry out dispersion with 500r/min and stir 25min;
4) then reduce rotating speed and add linear alkylbenzene sulphonic acid, carry out dispersion with 400r/min and stir 15min;
5) with high pressure homogenizer under 9.6MPa pressure, make suspended particles pressurized and broken, suspension grain disperseed equably, after cooling, is finished product.
Respectively the anti-ultraviolet paint that embodiment 1-3 obtains is coated on polyester film, carries out photocuring with the ultraviolet lamp of 3kW, solidify completely within 5-10 second, obtain paint film.
Carry out performance test to above-mentioned paint film, the performance test results, in table 1, wherein carries out color inhibition test to paint film, be specially: paint film is sprayed on white base plate, after paint film ultraviolet light polymerization, carry out range estimation with there is no the white base plate of paint film and compare, see if there is aberration.
As can be seen from the data detected, the present invention has good sticking power and snappiness, and shock resistance is also very strong, has very high hardness and wear resistance.Paint coatings amount 11.5g/cm of the present invention
2, Air permenbility is 17.6kg/m
2s, elongation is 45%, has good ultraviolet shielding effect, and the uv transmittance of wavelength 40nm is 15%, is 50% to the transmitance of the visible ray of wavelength 600nm; α-cyanoacrylate sizing agent has high refractivity and high photolytic activity, can be used as sun-screening agent, solves a lot of actual needs, is applicable to various fabric, has certain function of shielding ultraviolet radiation, and do not affect breathable moisture permeability.
The explanation of above embodiment just understands method of the present invention and core concept thereof for helping.It should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention, can also carry out some improvement and modification to the present invention, these improve and modify and also fall in the protection domain of the claims in the present invention.To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the present invention.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein can without departing from the spirit or scope of the present invention, realize in other embodiments.Therefore, the present invention can not be restricted to these embodiments shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.
Claims (5)
1. the anti-ultraviolet paint improved, is characterized in that: be made up of the raw material of following parts by weight:
Benzyl dimethyl phenol polyethenoxy ether 1.5-4 part; mixed fatty alcohol sodium sulfate 0.35-0.66 part; α-cyanoacrylate sizing agent 1.25-1.65 part; 2,4,6-trimethylbenzoy-dipheny phosphine oxide 0.36-0.67 part; tinting material 0.22-0.66 part; bisphosphate potassium 4-6.5 part, defoamer 1.23-3.25 part, linear alkylbenzene sulphonic acid 1.55-2.68 part.
2. the anti-ultraviolet paint of improvement according to claim 1, is characterized in that:
Be made up of the raw material of following parts by weight: benzyl dimethyl phenol polyethenoxy ether 1.5 parts; 0.35 part, mixed fatty alcohol sodium sulfate; α-cyanoacrylate sizing agent 1.25 parts; 2,4,6-trimethylbenzoy-dipheny phosphine oxide 0.36 part; tinting material 0.22 part; 4 parts, bisphosphate potassium, defoamer 1.23 parts, linear alkylbenzene sulphonic acid 1.55 parts.
3. the anti-ultraviolet paint of improvement according to claim 1, is characterized in that: described tinting material is dispersed dye.
4. the anti-ultraviolet paint of improvement according to claim 1, is characterized in that: described defoamer is organic silicon modified by polyether.
5. the preparation method of the anti-ultraviolet paint of the improvement according to any one of claim 1-4, comprises the following steps:
1) according to said components proportioning, benzyl dimethyl phenol polyethenoxy ether, mixed fatty alcohol sodium sulfate and α-cyanoacrylate sizing agent are poured in container, adds defoamer, access heat-treating machine, keep vapor temperature >=100 DEG C, after 10-15min thermal treatment, naturally cool to room temperature;
2) then 2,4,6-trimethylbenzoy-dipheny phosphine oxide and tinting material are pressed formula rate, put in container, carry out initial filter with diatomite filter, its filter pressure is to≤0.1 MPa, and transmittance reaches more than 96%;
3) in reaction vessel, add bisphosphate potassium, carry out dispersion with 400-500r/min and stir 20-25min;
4) then reduce rotating speed and add linear alkylbenzene sulphonic acid, carry out dispersion with 300-400r/min and stir 15min;
5) with high pressure homogenizer under 8.8-9.6MPa pressure, make suspended particles pressurized and broken, suspension grain disperseed equably, after cooling, is finished product.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511015542.7A CN105542527A (en) | 2015-12-30 | 2015-12-30 | Improved ultraviolet-proof coating and preparation method thereof |
| PCT/CN2016/107289 WO2017114047A1 (en) | 2015-12-30 | 2016-11-25 | Improved ultraviolet-resistant coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511015542.7A CN105542527A (en) | 2015-12-30 | 2015-12-30 | Improved ultraviolet-proof coating and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105542527A true CN105542527A (en) | 2016-05-04 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201511015542.7A Pending CN105542527A (en) | 2015-12-30 | 2015-12-30 | Improved ultraviolet-proof coating and preparation method thereof |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN105542527A (en) |
| WO (1) | WO2017114047A1 (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017114047A1 (en) * | 2015-12-30 | 2017-07-06 | 曲少春 | Improved ultraviolet-resistant coating and preparation method thereof |
| CN108867099A (en) * | 2018-06-15 | 2018-11-23 | 合肥伊只门窗有限公司 | A kind of antiultraviolet dyestuff and preparation method thereof for curtain |
| CN109516749A (en) * | 2018-10-04 | 2019-03-26 | 南京航空航天大学溧水仿生产业研究院有限公司 | Bionical wave-absorbing and camouflage material and preparation method thereof |
| CN109921278A (en) * | 2019-03-28 | 2019-06-21 | 维沃移动通信有限公司 | Laser projection mould group |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120190777A1 (en) * | 2011-01-26 | 2012-07-26 | Elastikote, Llc | Coating composition containing biobased materials |
| CN103602252A (en) * | 2013-10-21 | 2014-02-26 | 青岛海伴诚远塑业有限公司 | Novel resin-type interior wall waterproof coating |
| CN103602123A (en) * | 2013-11-19 | 2014-02-26 | 青岛广联达精密机械有限公司 | Resin type water-resistant coating material |
| CN103602122A (en) * | 2013-10-25 | 2014-02-26 | 青岛海伴塑胶工贸有限公司 | Resin type waterproof coating material |
| CN104212259A (en) * | 2014-08-22 | 2014-12-17 | 青岛保利康新材料有限公司 | Waterproof paint for building |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TW369554B (en) * | 1995-10-19 | 1999-09-11 | Three Bond Co Ltd | Photocurable composition |
| US5922783A (en) * | 1997-02-27 | 1999-07-13 | Loctite Corporation | Radiation-curable, cyanoacrylate-containing compositions |
| US6867241B2 (en) * | 2002-01-31 | 2005-03-15 | Henkel Corporation | Radiation-curable, cyanoacrylate-containing compositions |
| CN105542527A (en) * | 2015-12-30 | 2016-05-04 | 曲少春 | Improved ultraviolet-proof coating and preparation method thereof |
-
2015
- 2015-12-30 CN CN201511015542.7A patent/CN105542527A/en active Pending
-
2016
- 2016-11-25 WO PCT/CN2016/107289 patent/WO2017114047A1/en active Application Filing
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120190777A1 (en) * | 2011-01-26 | 2012-07-26 | Elastikote, Llc | Coating composition containing biobased materials |
| CN103602252A (en) * | 2013-10-21 | 2014-02-26 | 青岛海伴诚远塑业有限公司 | Novel resin-type interior wall waterproof coating |
| CN103602122A (en) * | 2013-10-25 | 2014-02-26 | 青岛海伴塑胶工贸有限公司 | Resin type waterproof coating material |
| CN103602123A (en) * | 2013-11-19 | 2014-02-26 | 青岛广联达精密机械有限公司 | Resin type water-resistant coating material |
| CN104212259A (en) * | 2014-08-22 | 2014-12-17 | 青岛保利康新材料有限公司 | Waterproof paint for building |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017114047A1 (en) * | 2015-12-30 | 2017-07-06 | 曲少春 | Improved ultraviolet-resistant coating and preparation method thereof |
| CN108867099A (en) * | 2018-06-15 | 2018-11-23 | 合肥伊只门窗有限公司 | A kind of antiultraviolet dyestuff and preparation method thereof for curtain |
| CN109516749A (en) * | 2018-10-04 | 2019-03-26 | 南京航空航天大学溧水仿生产业研究院有限公司 | Bionical wave-absorbing and camouflage material and preparation method thereof |
| CN109921278A (en) * | 2019-03-28 | 2019-06-21 | 维沃移动通信有限公司 | Laser projection mould group |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2017114047A1 (en) | 2017-07-06 |
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