CN105525181B - A kind of capacity pump blade composite hard alloy and preparation method thereof - Google Patents

A kind of capacity pump blade composite hard alloy and preparation method thereof Download PDF

Info

Publication number
CN105525181B
CN105525181B CN201410560666.2A CN201410560666A CN105525181B CN 105525181 B CN105525181 B CN 105525181B CN 201410560666 A CN201410560666 A CN 201410560666A CN 105525181 B CN105525181 B CN 105525181B
Authority
CN
China
Prior art keywords
blade
hard alloy
alloy
composite hard
green body
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201410560666.2A
Other languages
Chinese (zh)
Other versions
CN105525181A (en
Inventor
蒋龙福
王岳平
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yixing Zhous Pump Industry Co Ltd
Original Assignee
Yixing Zhous Pump Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yixing Zhous Pump Industry Co Ltd filed Critical Yixing Zhous Pump Industry Co Ltd
Priority to CN201410560666.2A priority Critical patent/CN105525181B/en
Publication of CN105525181A publication Critical patent/CN105525181A/en
Application granted granted Critical
Publication of CN105525181B publication Critical patent/CN105525181B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Abstract

A kind of capacity pump blade composite hard alloy and preparation method thereof, component is by mass percentage are as follows: titanizing tungsten powder 80 ~ 92%, the enhancing cobalt powder 5 ~ 15%, liquid rubber 0.5 ~ 5% of 200 ~ 280 mesh of fineness, remaining is inevitable trace impurity.Solve the problems, such as that blade curve form is complicated, high, the difficult machine cut machine-shaping of Cemented Carbide Hardness, with PM technique one-pass molding, the satisfactory blade of curved surface inlays coating, improves technique, saves cost.It is not wear-resisting to overcome the problems, such as that blade is washed away by air-flow and impurity.

Description

A kind of capacity pump blade composite hard alloy and preparation method thereof
Technical field
The present invention relates to capacity pump blade production field more particularly to a kind of blades of surface recombination hard alloy.
Background technique
The capacity of the prior art pump in blade be generally common ironcasting, the pump is for conveying about 50% gas, about When the mixed material of 50% liquid (wherein 8 ~ 10% be crude oil, 40% be water) and 1% solid silt particle, when pump discharge pressure is greater than In the case where 0.8MPa, the high pressure gas in liquid outlet cavity is pumped, is mingled with dampening and silt particle, protrusion and separation from blade curved surface The matching part of disk backflows to the suction inlet position of pump chamber, since the gas of folder silt particle holds very much during backflowing at a high speed The surface of easy erosive wear blade and separator disc, and then increase gap between the two, make the volumetric efficiency decline of pump.In oil When the conveying of field production crew is containing gas and water, crude oil, which there is high-pressure working chamber and operating on low voltage chamber using after two months The phenomenon that gas blowby, affects the using effect of pump.Therefore, axisymmetric curved surface rotary volume-variable pump will succeed on national oilfield exploitation Using also needing to improve.
Original technology metal blade is washed away by air-flow and sand grains, and surface is easily worn, and then is damaged on slide damper Roller increases the gap between blade protrusion and middle separate disk, and then makes channelling between the high pressure chest of sliding vane rotary pump and low pressure chamber, pump efficiency Rate decline, until disabling damage.
Those skilled in the art change the wear-resisting property of blade in order to be promoted, and wear surface is changed to tungsten-cobalt alloy, can be made resistance to It grinds performance and rises 6 ~ 8 times from original tool steel T-12, but there are two disadvantages again for tungsten-cobalt alloy: first is that tungsten-cobalt alloy price is high, Integral manufacturing blade cost is very high, therefore contemplates the surface inserting tungsten-cobalt alloy piece in blade again, can save cost in this way 80%;Second is that tungsten-cobalt alloy extreme hardness, can reach 85-92, but machine-shaping is extremely difficult, especially machine cut processing system Make the working face of S type curved surface blade, it is very difficult, therefore contemplate again how the curved surface work of disposal molding blade tungsten-cobalt mold insert Make face, the method compression molding of preferable method powder metallurgy is sintered tungsten-cobalt alloy empiecement.
Summary of the invention
In view of the deficiencies of the prior art, the present invention provides one kind, and blade to be effectively prevent to wear, the change improved service life Positive displacement pump blade composite hard alloy and preparation method thereof.
Purpose to realize the present invention provides following technical scheme: a kind of capacity pump blade composite hard alloy, special Sign is component by mass percentage are as follows: titanizing tungsten powder 80 ~ 92%, the enhancing cobalt powder 5 ~ 15%, liquid rubber of 200 ~ 280 mesh of fineness 0.5 ~ 5%, remaining is inevitable trace impurity.
Preferably, liquid rubber is butadiene acrylonitrile rubber.
Preferably, titanizing tungsten powder is 92%, fineness is 210 ~ 220 mesh.
Preferably, enhancing cobalt powder is 7%.
Preferably, liquid rubber 1%.
Purpose to realize the present invention provides a kind of capacity pump blade composite hard alloy production method, including following Step: a. opens the metal die of compression moulding processed;B. the titanizing tungsten powder 80 ~ 96% of 200 ~ 280 mesh of fineness, enhancing cobalt powder 5 ~ 15%, liquid rubber 0.5 ~ 5%, remaining is inevitable trace impurity, is stirred well with blender, then is packed into gold by required weight Belong to mold, is press-formed on press machine, briquetting pressure is in 10 ~ 20m2It between/Kg, then demoulds, the alloy green body after demoulding, Shifting is put into made of graphite and on blade green body similar shape supporting mass, to prevent from deforming;C. firing is placed on alloy green body and base The graphite of body similar shape is held on body, is put into vacuum drying oven, specific firing temperature process curve be room temperature to 600 DEG C be a cycle, about 3 A hour, then 100 DEG C every liter of period is 2 hours, when temperature reaches 1450 ~ 1480 DEG C, constant temperature 5 hours or so, then It is gradually cooled to room temperature, is controlled between 20 ~ 30 hours cooling time;D. alloy green body sanding and polishing, firing furnace is down to 60 ~ When 80 DEG C of temperature, the product being burnt into can be taken out from vacuum drying oven, and collects graphite support tool, in case firing makes repeatedly later With;E. the alloy blank being burnt into, by polishing, weld bolt can couple installation with the matrix of blade, then with grinding machine to hard The outer circle and inner circle of alloy carry out grinding, to reach the requirement of installation;F. to the requirement of hard alloy be it is indeformable, without gas Hole, flawless, hardness is between 80 ~ 90 °, preferably between 86 ~ 88 °.
Preferably, metal die includes upper die and lower die, the die sleeve being placed on upper and lower mould and is set in upper and lower mould The plug of the heart, the upper and lower mould interface offer rotating sheet type chamber.
Beneficial effects of the present invention: it solves high, the difficult machine cut of blade curve form complexity, Cemented Carbide Hardness and is processed into The problem of type, with PM technique one-pass molding, the satisfactory blade of curved surface inlays coating, improves technique, saves cost.Gram It takes blade and is washed away not wear-resisting problem by air-flow and impurity.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of metal die.
Specific embodiment
Embodiment 1: a kind of capacity pump blade composite hard alloy, component is by mass percentage are as follows: fineness 200 ~ 280 Purpose titanizing tungsten powder 80%, enhancing cobalt powder 15%, butadiene acrylonitrile rubber 5%, remaining is inevitable trace impurity.
Embodiment 2: a kind of capacity pump blade composite hard alloy, component is by mass percentage are as follows: fineness 200 ~ 280 Purpose titanizing tungsten powder 92%, enhancing cobalt powder 5%, butadiene acrylonitrile rubber 3%, remaining is inevitable trace impurity.
Embodiment 3: a kind of capacity pump blade composite hard alloy, component is by mass percentage are as follows: fineness 200 ~ 280 Purpose titanizing tungsten powder 85%, enhancing cobalt powder 14.5%, butadiene acrylonitrile rubber: 0.5%, remaining is inevitable trace impurity.
Embodiment 4: a kind of capacity pump blade composite hard alloy, component is by mass percentage are as follows: fineness 200 ~ 280 Purpose titanizing tungsten powder 92%, enhancing cobalt powder 7%, butadiene acrylonitrile rubber: 1%, remaining is inevitable trace impurity.
Embodiment 5: referring to one of embodiment 1 ~ 4, a kind of capacity pump blade composite hard alloy production method, including with Lower step: a. opens the metal die of compression moulding processed;B. the titanizing tungsten powder 80 ~ 96% of 200 ~ 280 mesh of fineness, enhancing cobalt powder 5 ~ 15%, liquid rubber 0.5 ~ 5%, remaining is inevitable trace impurity, is stirred well with blender, then is packed into gold by required weight Belong to mold, is press-formed on press machine, briquetting pressure is in 10 ~ 20m2It between/Kg, then demoulds, the alloy green body after demoulding, Shifting is put into made of graphite and on blade green body similar shape supporting mass, to prevent from deforming;C. firing is placed on alloy green body and base The graphite of body similar shape is held on body, is put into vacuum drying oven, specific firing temperature process curve be room temperature to 600 DEG C be a cycle, about 3 A hour, then 100 DEG C every liter of period is 2 hours, when temperature reaches 1450 ~ 1480 DEG C, constant temperature 5 hours or so, then It is gradually cooled to room temperature, is controlled between 20 ~ 30 hours cooling time;D. alloy green body sanding and polishing, firing furnace is down to 60 ~ When 80 DEG C of temperature, the product being burnt into can be taken out from vacuum drying oven, and collects graphite support tool, in case firing makes repeatedly later With;E. the alloy blank being burnt into, by polishing, weld bolt can couple installation with the matrix of blade, then with grinding machine to hard The outer circle and inner circle of alloy carry out grinding, to reach the requirement of installation;F. to the requirement of hard alloy be it is indeformable, without gas Hole, flawless, hardness is between 80 ~ 90 °, preferably between 86 ~ 88 °.
Metal die includes upper mold 001 and lower die 002, the die sleeve 003 being placed on upper and lower mould (001,002) and is set to The plug 004 at upper and lower mould (001,002) center, upper and lower mould (the 001,002) interface offer rotating sheet type chamber 005.

Claims (5)

1. a kind of capacity pumps blade composite hard alloy production method, comprising the following steps:
A. the metal die of compression moulding processed is opened;
B. by percentage to the quality: the titanizing tungsten powder 80 ~ 92% of 200 ~ 280 mesh of fineness, enhancing cobalt powder 5 ~ 15%, butadiene acrylonitrile rubber 0.5 ~ 5%, remaining is inevitable trace impurity, is stirred well with blender, then is packed into metal die by required weight, in press machine Upper extrusion forming, briquetting pressure is in 10 ~ 20 kg/m2Between, it then demoulds, the alloy green body after demoulding, shifting is put into graphite system At on blade green body similar shape supporting mass, to prevent from deforming;
C. it is burnt into: the graphite of alloy green body and blade green body similar shape being held body and is put into vacuum drying oven, specific firing temperature process curve For room temperature to 600 DEG C be a cycle, 3 hours, then 100 DEG C every liter of period is 2 hours, temperature reaches 1450 ~ At 1480 DEG C, constant temperature 5 hours, it is then gradually cooled to room temperature, is controlled between 20 ~ 30 hours cooling time;
D. alloy green body sanding and polishing, when firing furnace is down to 60 ~ 80 DEG C of temperature, the product being burnt into is taken out from vacuum drying oven, And graphite support tool is collected, in case firing Reusability later;
E. the alloy blank being burnt into, by polishing, weld bolt can couple installation with the matrix of blade, then with grinding machine to hard The outer circle and inner circle of matter alloy carry out grinding, to reach the requirement of installation;
It f. is indeformable, pore-free, flawless to the requirement of hard alloy, hardness is between 80 ~ 90 degree.
2. a kind of capacity according to claim 1 pumps blade composite hard alloy production method, it is characterised in that metal Mold includes upper die and lower die, the die sleeve being placed on upper and lower mould and the plug for being set to upper and lower mould center, the upper and lower mould pair Junction offers rotating sheet type chamber.
3. a kind of capacity according to claim 1 pumps blade composite hard alloy production method, it is characterised in that titanizing Tungsten powder is 92%, and fineness is 210 ~ 220 mesh.
4. a kind of capacity according to claim 1 pumps blade composite hard alloy production method, it is characterised in that enhancing Cobalt powder is 7%.
5. a kind of capacity according to claim 1 pumps blade composite hard alloy production method, it is characterised in that Ding Qing Glue 1%.
CN201410560666.2A 2014-10-21 2014-10-21 A kind of capacity pump blade composite hard alloy and preparation method thereof Active CN105525181B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410560666.2A CN105525181B (en) 2014-10-21 2014-10-21 A kind of capacity pump blade composite hard alloy and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410560666.2A CN105525181B (en) 2014-10-21 2014-10-21 A kind of capacity pump blade composite hard alloy and preparation method thereof

Publications (2)

Publication Number Publication Date
CN105525181A CN105525181A (en) 2016-04-27
CN105525181B true CN105525181B (en) 2018-12-11

Family

ID=55767700

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410560666.2A Active CN105525181B (en) 2014-10-21 2014-10-21 A kind of capacity pump blade composite hard alloy and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105525181B (en)

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101748305A (en) * 2010-01-20 2010-06-23 中国科学院长春应用化学研究所 Preparation method of tungsten carbide-aluminum hard alloy sintering body

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014188598A (en) * 2013-03-26 2014-10-06 Mitsubishi Materials Corp Surface coated wc base super hard alloy cutting tool excellent in toughness and defect resistance

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101748305A (en) * 2010-01-20 2010-06-23 中国科学院长春应用化学研究所 Preparation method of tungsten carbide-aluminum hard alloy sintering body

Also Published As

Publication number Publication date
CN105525181A (en) 2016-04-27

Similar Documents

Publication Publication Date Title
CN107815580B (en) A kind of polycrystalline cubic boron nitride/diamond composite and preparation method thereof
CN102434665B (en) Light gradient hard-alloy sealing ring and manufacture method thereof
CN106984808A (en) A kind of localization strengthens the method for preparing powder metallurgy of composite
CN104148651B (en) A kind of preparation method of TiC carbide alloy composite grinding roll
JP2017042822A (en) Metal mold for molding power and method for manufacturing dust compact
CN103981419A (en) High-strength titanium carbonitride metal ceramic sealing material and preparation method thereof
CN102537510B (en) Pressureless sintering silicon carbide ceramic valve core and preparation process thereof
CN104400672A (en) Metallic bond diamond grinding wheel
CN103658638A (en) Manufacturing method of bar material of hard alloy end mill for machining stainless steel
CN104018017B (en) The recovery of waste and old Ti (C, N) base metal-ceramic material and renovation process
CN107236890A (en) A kind of concrete pump truck cheater plate and cut ring new material and preparation method thereof
CN105525181B (en) A kind of capacity pump blade composite hard alloy and preparation method thereof
CN205761448U (en) A kind of band is directed into the standing crusher impeller of hopper
CN103586474A (en) Method for manufacturing powder metallurgy shaped charge liner for oil-gas well jet cutter
CN103878886B (en) A kind of material prescription of diamond bit and manufacture method thereof
CN102029298B (en) Al2O3/TiC ceramic drawing die and manufacturing method thereof
CN106762808B (en) High-flow high-lift yellow-leading centrifugal water pump wear-resistant opening ring and preparation method thereof
CN104343681B (en) A kind of axisymmetric curved surface rotary volume-variable pump
CN104175237A (en) Diamond grinding wheel adopting rare-earth modified tungsten-based bond and manufacturing method thereof
CN104894452B (en) A kind of WC Fe Ni carbide roll rings and preparation method thereof
CN204175592U (en) A kind of axisymmetric curved surface rotary volume-variable pump
CN103231065B (en) Method for regenerating high-speed wire cemented carbide roll collar
CN209222197U (en) A kind of steel bonded carbide castingin jaw crusher liner plate
CN202833273U (en) Mining heavy slurry pump with water seal at suction inlet
CN105402139A (en) Abrasion-resistant and corrosion-resistant slurry pump

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant