CN105519611A - Nanometer microcapsule biological compound master batch of rodent repellent and preparation method thereof - Google Patents
Nanometer microcapsule biological compound master batch of rodent repellent and preparation method thereof Download PDFInfo
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- CN105519611A CN105519611A CN201510871686.6A CN201510871686A CN105519611A CN 105519611 A CN105519611 A CN 105519611A CN 201510871686 A CN201510871686 A CN 201510871686A CN 105519611 A CN105519611 A CN 105519611A
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- master batch
- mouse agent
- expelling mouse
- biological compound
- condensed cream
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing within the same carbon skeleton a carboxylic group or a thio analogue, or a derivative thereof, and a carbon atom having only two bonds to hetero atoms with at the most one bond to halogen, e.g. keto-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
Abstract
The invention relates to a rodent repellent, especially to a biological compound master batch of a rodent repellent. The nanometer microcapsule biological compound master batch of the rodent repellent comprises 1.5 to 2.0% of capsaicin, 1.0 to 1.5% of cinnamamide, 1.5 to 2.5% of concentrated aqueous extract of wild ginger, 0.8 to 1.2% of concentrated organic solvent extract of digitalis, 0.7 to 1.2% of actidione, 0.5 to 1.0% of an embedding capsule wall material and 0.1 to 0.3% of an antiseptic, with the balance being water. The master batch tastes pungent and gives off offensive odor when chewed; meanwhile, the master batch simulates the flavor of urine of predators and has no toxicity when eaten by animals or people; every component has different action mechanisms and cooperated with each other, and the master batch has long-lasting rodent-repelling effect; and the master batch has the advantages of usage of local materials, low cost, convenience in preparation and usage, no pollution to the environment, safety to people and poultry and good rodent-repelling effect.
Description
Technical field
The present invention relates to a kind of expelling mouse agent, particularly one biological compound expelling mouse agent masterbatch.
Background technology
Current rat plague control mainly contains protection against rodents, kills mouse, rat destruction three kinds of methods, is also one of method of administering the plague of rats.Biological activity is the material that natural world itself exists, and easily degrades, free from environmental pollution, not easily develops immunity to drugs, is therefore subject to extensive concern.Plant has much defensive chemicals mass-energy to suppress animal to take food, and therefore has the potentiality of exploitation repellant.The Plant Secondary Metabolites of existing more than 100,000 kinds is used to screen repellant in the world, but the business expelling mouse agent coming from plant component is at present still little.China's plant resources is very abundant, long to the research history of botanical pesticide, and research and development vegetalitas rat destruction medicament is a direction of rat destruction medicament research from now on.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of Nano type microcapsules biological compound expelling mouse agent masterbatch, has good repellent effect.
Technical problem to be solved by this invention is achieved by the following technical programs:
A kind of Nano type microcapsules biological compound expelling mouse agent masterbatch, is characterized in that, be made up of the component of following percentage by weight:
Capsaicine 1.5 ~ 2.0%; Cinnamamide 1.0 ~ 1.5%; Rhizoma Polygonati water extract condensed cream 1.5 ~ 2.5%;
Digitalis extractive with organic solvent condensed cream 0.8 ~ 1.2%; Cycloheximide 0.7 ~ 1.2%; Embedding capsule material 0.5 ~ 1.0%;
Preservative 0.1% ~ 0.3%; Surplus is water.
Further, described embedding capsule material is the casein sodium of 0.20 ~ 0.50% and the zeins of 0.30 ~ 0.50%.
Further, be made up of the component of following percentage by weight:
Capsaicine 1.8%; Cinnamamide 1.3%; Rhizoma Polygonati water extract condensed cream 2.0%;
Digitalis extractive with organic solvent condensed cream 1.0%; Cycloheximide 0.9%;
Embedding capsule material: the casein sodium of 0.20 ~ 0.50% and the zeins of 0.30 ~ 0.50%;
Preservative 0.1% ~ 0.3%; Surplus is water.
The preparation method of above-mentioned Nano type microcapsules biological compound expelling mouse agent masterbatch is:
Step one, capsaicine, cinnamamide, Rhizoma Polygonati water extract condensed cream, digitalis ethanol extract condensed cream to be dissolved in certain water respectively, then to add cycloheximide, preservative etc., stir, finally add water to 100%, make compound expelling mouse agent masterbatch;
Step 2, nanometer technology embed: with embedding capsule material, step one gained compound expelling mouse agent masterbatch is made nanometer-sized microcapsules expelling mouse agent masterbatch.
Masterbatch of the present invention is primarily of capsaicine, cinnamamide, Rhizoma Polygonati water extract, digitalis extractive with organic solvent, cycloheximide composition, chew and have taste that is pungent, stench, imitate the taste of carnivore urine simultaneously, but taken in rear also avirulence by animal or human, the mechanism of action of each component is different, and mutual coordinated, obvious and lasting to the repellent action of mouse, can gather materials on the spot, cost is low, prepare and easy to use, free from environmental pollution, person poultry safety, repellent effect is good.
The present invention can be used for:
(1) rat destruction pulvis, coating is made: can be used for warehouse, shop, the upper and lower pipeline mouse of newly-built construction move under water part, also to the wall such as kitchen, food storage, ground, the mouse road in warehouse can spray.In addition, also can be used to protect the plastic products of cable, optical fiber, pipeline, outdoor facilities and so on and bin to bite from muroid.
(2) the gloomy seed dressing of agriculture: be mixed with certain density liquid, is dressed seed by seed or dips in slurry, for breeding and nursery.By sad pungent, offending smell, and make mouse eat difficult peace, do not drink and do not eat and in succession die.
(3) plant: as suitable hen house uses, there is the stacking of feed in plant, and have unrestrained feed inside hen house, this creates good condition for the huge of mouse colony.Make rat destruction pulvis or paint, on other article that need protect such as on the mouse road being sprayed on warehouse or warehouse, make mouse be unwilling near the article using medicament, to protect article not by damaged by rats.
Embodiment
Below in conjunction with embodiment, the present invention will be described in detail, and embodiment is only the preferred embodiment of the present invention, is not limitation of the invention.
Embodiment
A kind of Nano type microcapsules biological compound expelling mouse agent masterbatch, is made up of the component of following percentage by weight:
Capsaicine 1.8%, cinnamamide 1.3%, Rhizoma Polygonati water extract condensed cream 2.0%, digitalis ethanol extract condensed cream 1.0%, cycloheximide 0.9%; The casein sodium of 0.20 ~ 0.50% and the zeins of 0.30 ~ 0.50%; Preservative (potassium sorbate) 0.1% ~ 0.3%; Surplus is water.
The preparation method of these Nano type microcapsules biological compound expelling mouse agent masterbatch is:
Step one, capsaicine, cinnamamide, Rhizoma Polygonati water extract condensed cream, digitalis ethanol extract condensed cream are dissolved in certain water by formula rate respectively, then cycloheximide, preservative etc. is added, stir, finally add water to 100%, make compound expelling mouse agent masterbatch;
Step 2, nanometer technology embed: with embedding capsule material, zeins, step one gained compound expelling mouse agent masterbatch is made nanometer-sized microcapsules expelling mouse agent masterbatch.Concrete embedding techniques is general knowledge known in this field, does not elaborate at this, specifically can with reference to " capsule of nano technology and application thereof, Chinese spices and essence scientific seminar collection of thesis in 2006,208 ~ 212 pages, Ye Lin; Xiao Zuobing ".
Above-mentioned Nano type microcapsules biological compound expelling mouse agent masterbatch conventional method is added the conven-tional adjuvants making coating, is made into the rat destruction coating that masterbatch content is 10%, for subsequent use.
Year April in May, 2013 to 2014, our company was in certain communication building and the tunnel that communicates, and Warehouse of Chinese Medicinal, chicken plant etc. have carried out Nano type microcapsules biology compound expelling mouse agent coating prepared by above-described embodiment to the test of cable protection effect.
Materials and methods
1.1 medicine
For examination expelling mouse agent: Nano type microcapsules biological compound expelling mouse agent coating prepared by embodiment 1.
Contrast expelling mouse agent: contrast rat destruction coating is provided by preclinical medicine institute of Wuhan University, the thick emulsion of appearance white, component content: 2% synthetic capsaicin, 5%2.2.4 mono-trimethyl alkane, 3%1.3 First Five-Year Plan two isobutyric acids, 90% moisture.
1.2 test site
1.2.1 communicate totally 9 layers, building, and wherein one deck is common Work place, and two, three floor are program control room, machine room, microcomputer, 30cm × 50cm cable trough that the 120m that inside has an appointment is long, has a large amount of cable to pass through in groove, and more than 4th floors employee stays.Broken by damaged by rats there to be cable habitually in the past, bite phenomenon broken.Communication tunnel: there are 2 access doors in tunnel, and generally all keep closed condition, muroid not easily enters.Near back door, tunnel, have a telecommunications cable inlet place, have 16, the hole of 12cm, every hole is at a distance of about 20cm, and every hole has 1 cable to pass through, and leave the gap that 3 ~ 5cm is wide between cable and hole wall, mouse can enter tunnel thus.
1.2.2 the existing test site of Warehouse of Chinese Medicinal first is selected in a 15m
2warehouse of Chinese Medicinal.Nei Youyi pond, warehouse, its downcomer is diameter 8cm, the portion of basseting is point S type bend pipe being about 50cm.The plastics thickness of pipe is about 0.3cm.Before test, plastic tube bend is stung out a diameter by mouse and is about 6cm round mouth, and in sewer, mouse enters people Ku Nei robber food medicinal material by this mouth every day, and depositary management personnel once used the blocking hole, east of hardboard, rag, wooden unit and so on, but were all broken by damaged by rats; Second testing ground is selected in another area and is about 18m
2between waste pure water purification is produced, have a pure water production machine in room, on machine, 4 are respectively about 1.5 ~ .2cm, the rubber tube of diameter 2.cm all gnawed by mouse, stings, have broken by the teeth, have have indentation.Through Powder mark method investigation, prove in room, to also have mouse movable.
1.2.3 chicken plant
Scene is positioned at chicken farm, masonry dam town, northeast, Huizhou City, and distance needs about 4 kilometers, city, floor space about 20,000 square metres, point living area, feed manufacturing district and culture zone in institute.There are the kitchen of brick mix structure, dormitory, office and foreign material storehouse in living area; Feed manufacturing district has between semi-enclosed crushing vehicle and feed storehouse; There are 2 meters high brick enclosure walls cultivation place, and fresh rat hole, mouse excrement are found everywhere; Also have a large amount of fruit trees, foreign material, feed everywhere, soft earth ground, these are all that muroid provides good food source, water source and habitat.
1.3 application process
1.3.1 communicate building
(1) communicate building: by communication cable by the place of breaking by the teeth, wrap up 60 places with medical proof fabric, often locate area and be about 1cm × 3cm, wherein 20 places brush the confession examination expelling mouse agent of embodiment 1,20 places brush contrast rat destruction coating, another 20 places not brush rat destruction coating as blank.This test, experimental group and control group carry out in same room, and often place is at a distance of 3 ~ 20cm.
(2) communication tunnel: use Plastic screen cloth, what brush embodiment 1 respectively supplies examination expelling mouse agent, contrast rat destruction coating, and after coating dries, by gap, the hole blocking of 8 wherein, another 8 holes are used the Plastic screen cloth of not swabbing to block and made blank.Test first 3 months every 10d and observe 1 time, monthly observe 1 time later, observe totally 1 year altogether.
1.3.2 Warehouse of Chinese Medicinal
First scene of using is checked, chemicals kills mouse, determine in storehouse without after mouse existence, first use brown paper jam-pack sewer trap cut, carry out Continuous Observation, as paper is opened by damaged by rats, then with embodiment 1 for examination expelling mouse agent, that contrast rat destruction coating is spread evenly across brown paper is two-sided, roll into a ball into tight group after drying in the shade, fill in and observe spitball by the situation of biting in damaged hole; Then do not kill mouse in second scene of using.After confirming there is mouse activity with Powder mark method Investigation of Rat Density, with yellow pen, edging circle is treated at indentation place on 4 slat gum pipes and the place of breaking by the teeth entirely good.Select 4 pipes to test, with hairbrush by embodiment 1 for examination expelling mouse agent, contrast expelling mouse agent be spread evenly across be used as test four tube-surfaces, another two pipes, as experimental control, do not do any process.Regularly to the mouse active situation at two scenes and carry out procuratorial work to the situation of biting of observing article, newfound bite mark is performed with red pen and marks and perform record.
1.3.3 chicken plant
Simulated field is that our company is about 12m
2simulation laboratory; Field rat repel effect experimental mainly selects the place such as fodder store, dormitory dining room chicken farm, masonry dam town, Huizhou muroid is often movable to be about 200m
2the place of stacking house refuse is carried out.
Simulated field: during test, places 1 porcelain dish respectively in simulated field 4 corners (from wall 10-15cm), respectively puts 20g rice in dish, and brown paper parcel in outside is airtight, wherein presses 5mg/m on brown paper surface for 2
2dosage be coated with embodiment 1 for examination expelling mouse agent, make blank, lay in diagonal angle for another 2, experimental group and control group transposition every day, check supplement bait, Continuous Observation 7d drags food situation.Under the prerequisite that said method is constant, each porcelain dish limit increases that to lay a surface area be 130cm again
2/ carton only, 2 cartons on porcelain dish experimental group limit, still press 2.5mg/m
2dosage be coated with embodiment 1 for examination expelling mouse agent, 2 cartons on porcelain dish control group limit still make blank, all put into sunflower seed airtight, lay in diagonal angle in box, experimental group and control group transposition every day, check supplement bait, observe 7d drag food situation.
On-the-spot: choose 5 experimental points and 5 blank points, 10 surface areas are 50cm
2/ plastic casing only, all puts into sunflower seed in box, and airtight with brown paper parcel, wherein 5 plastic casings of experimental point, by 2.5mg/m
2dosage be coated with embodiment 1 for examination expelling mouse agent, make blank matched control for another 5, experimental group and control group transposition every day, check supplement bait, observe 7d drag food situation.Then 76cm is used
2/ carton only substitutes above-mentioned plastic casing, loads roast duck meat, adopt above-mentioned same method in box, and that observes 7d drags food situation.Repeat 1 time weekly, only change bait, do not change the overwrap for examination expelling mouse agent scribbling embodiment 1, Continuous Observation 4 weeks.
Drag food criterion outer packing material to have the vestige crossed by damaged by rats, be then judged as the positive (namely being dragged food).
2 results
2.1 communication buildings
When observing for the 1st time (May 21), in communication building blank group, trace is nibbled at 2 places, and in communication tunnel blank group, trace is nibbled at 1 place; And 2 local experimental group and rat destruction coating control group are all without nibbling trace, in the observing for each time of in April ,-2014 in September, 2013, experimental group, rat destruction coating control group and control group are all without nibbling trace.Analyze its reason: this rat destruction coating not only has effect to the sense of taste, also may work to sense of smell, and mouse is not reacceesed; Due to medicine group and control group close together, medicine group may have impact to control group.Mouse has group behavior, and when minority mouse is gnawed, oral cavity and gastrointestinal mucosal are subject to causing the pain sensation after capsaicine stimulates, and can notify other members of family, no longer go to gnaw.
2.2 Warehouse of Chinese Medicinal
2.2.1 first uses scene
The hole not being coated with expelling mouse agent brown paper is filled in primary scene, is namely broken by the teeth through 1 day brown paper, and warehouse-in steals food medicinal material, illustrates that in sewer, mouse is movable rampant.After filling in the brown paper being coated with expelling mouse agent, through Continuous Observation 1 year, paper was not broken by the teeth yet, and this illustrates that this expelling mouse agent has good and lasting thing repellent effect; If do not considered, the factor such as sunlight, high temperature affects, and under normal room conditions, rat destruction effective time should more than 1 year.
2.2.2 second uses scene
Powder mark method rodent density is investigated, cloth powder six pieces of total positiveses, confirms there is mouse and frequent activity.The protective effect of expelling mouse agent to rubber tube the results are shown in subordinate list 1.Two sebific ducts for examination expelling mouse agent, contrast pharmacy test group all do not find damaged by rats trace in 6 months after coating, and blank group two sebific ducts (not being coated with expelling mouse agent) then continue to be bitten (newly-increased bite mark 16 place) by mouse.This illustrates that the protective effect of expelling mouse agent to experimental group sebific duct is obvious.
Table 1 expelling mouse agent is to the protective effect result of rubber tube
2.3 chicken plants
2.3.1 simulated experiment
The experiment of rice bait is pressed 5mg/m2 dosage and is coated with after for examination expelling mouse agent on the brown paper of porcelain dish surface: Continuous Observation 7d, experimental group does not all drag food, and control group drags food every day, show as the brown paper that parcel fills rice porcelain dish and broken by the teeth, peripherally, have the rice be dispersed in.
Experimental group and the continuous 7d of control group of rice and sunflower seed pairing experiment rice bait do not drag food.The experimental group of sunflower seed bait does not drag food on the 1st day, within the 2nd day, then drags food; And control group all drags food on the 1st day, the sunflower seed wherein in 1 box are all eaten up, and within the 7th day, the sunflower seed then in 2 boxes are all eaten up (table 2).
Table 2 rice and sunflower seed pairing experimental result
2.3.2 no matter the on-the-spot experimental group scribbled for examination expelling mouse agent, put sunflower seed or roast duck meat bait in box, all do not dragged food in 4 weeks; And the blank group be not coated with for examination expelling mouse agent (adopting identical bait), then all dragged food (table 3).
Table 3 is for the field experiment of examination expelling mouse agent repellent effect
Claims (4)
1. a Nano type microcapsules biological compound expelling mouse agent masterbatch, is characterized in that, be made up of the component of following percentage by weight:
Capsaicine 1.5 ~ 2.0%; Cinnamamide 1.0 ~ 1.5%; Rhizoma Polygonati water extract condensed cream 1.5 ~ 2.5%;
Digitalis extractive with organic solvent condensed cream 0.8 ~ 1.2%; Cycloheximide 0.7 ~ 1.2%; Embedding capsule material 0.5 ~ 1.0%;
Preservative 0.1% ~ 0.3%; Surplus is water.
2. Nano type microcapsules according to claim 1 biological compound expelling mouse agent masterbatch, is characterized in that: described embedding capsule material is the casein sodium of 0.20 ~ 0.50% and the zeins of 0.30 ~ 0.50%.
3. Nano type microcapsules according to claim 1 biological compound expelling mouse agent masterbatch, is characterized in that, be preferably made up of the component of following percentage by weight:
Capsaicine 1.8%; Cinnamamide 1.3%; Rhizoma Polygonati water extract condensed cream 2.0%;
Digitalis extractive with organic solvent condensed cream 1.0%; Cycloheximide 0.9%;
Embedding capsule material: the casein sodium of 0.20 ~ 0.50% and the zeins of 0.30 ~ 0.50%;
Preservative 0.1% ~ 0.3%; Surplus is water.
4. a preparation method for the biological compound expelling mouse agent of Nano type microcapsules described in any one of claim 1 ~ 3 masterbatch, is characterized in that:
Step one, capsaicine, cinnamamide, Rhizoma Polygonati water extract condensed cream, digitalis ethanol extract condensed cream to be dissolved in certain water respectively, then to add cycloheximide, preservative etc., stir, finally add water to 100%, make compound expelling mouse agent masterbatch;
Step 2, nanometer technology embed: with embedding capsule material, step one gained compound expelling mouse agent masterbatch is made nanometer-sized microcapsules expelling mouse agent masterbatch.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510871686.6A CN105519611A (en) | 2015-12-02 | 2015-12-02 | Nanometer microcapsule biological compound master batch of rodent repellent and preparation method thereof |
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| CN201510871686.6A CN105519611A (en) | 2015-12-02 | 2015-12-02 | Nanometer microcapsule biological compound master batch of rodent repellent and preparation method thereof |
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| CN106057340A (en) * | 2016-06-08 | 2016-10-26 | 王小凤 | Electric wire applied in transformer substation |
| CN106128597A (en) * | 2016-06-08 | 2016-11-16 | 吴敏 | A kind of electric wire used in power equipment |
| IT201900004147A1 (en) * | 2019-03-21 | 2020-09-21 | Guglielmo Buonamici | RODENTICIDE |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106057340A (en) * | 2016-06-08 | 2016-10-26 | 王小凤 | Electric wire applied in transformer substation |
| CN106128597A (en) * | 2016-06-08 | 2016-11-16 | 吴敏 | A kind of electric wire used in power equipment |
| IT201900004147A1 (en) * | 2019-03-21 | 2020-09-21 | Guglielmo Buonamici | RODENTICIDE |
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| CN113677208A (en) * | 2019-03-21 | 2021-11-19 | 创新与可持续发展有限责任公司 | Rodenticide |
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Application publication date: 20160427 |