CN105506563B - A kind of and manufacture craft of the supporting nanometer silver antimicrobial filter screen of vacuum cup - Google Patents
A kind of and manufacture craft of the supporting nanometer silver antimicrobial filter screen of vacuum cup Download PDFInfo
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- CN105506563B CN105506563B CN201510876411.1A CN201510876411A CN105506563B CN 105506563 B CN105506563 B CN 105506563B CN 201510876411 A CN201510876411 A CN 201510876411A CN 105506563 B CN105506563 B CN 105506563B
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- stainless steel
- silver
- filtering net
- steel filtering
- target
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Classifications
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
-
- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47G—HOUSEHOLD OR TABLE EQUIPMENT
- A47G19/00—Table service
- A47G19/22—Drinking vessels or saucers used for table service
- A47G19/2205—Drinking glasses or vessels
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/02—Pretreatment of the material to be coated
- C23C14/021—Cleaning or etching treatments
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/02—Pretreatment of the material to be coated
- C23C14/021—Cleaning or etching treatments
- C23C14/022—Cleaning or etching treatments by means of bombardment with energetic particles or radiation
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
- C23C14/14—Metallic material, boron or silicon
- C23C14/16—Metallic material, boron or silicon on metallic substrates or on substrates of boron or silicon
Abstract
A kind of and manufacture craft of the supporting nanometer silver antimicrobial filter screen of vacuum cup, belong to household utensils manufacturing technology and field of nanometer technology, be application technology of the nanometer technology on vacuum cup.It is characterized in：Stainless steel filtering net product is flat bottom straight edge disk, and aperture is dispersed with horizontal plane, and nanometer silver antimicrobial film layer is covered with surface.Manufacture craft is：The decontamination of stainless steel filtering net product, the cleaning of paraffin removal and drying；Pre-sputtering and bias Bombardment and cleaning are carried out respectively to target chromium and silver；The plated film of stainless steel filtering net product, including filter screen product restocking after drying, into vacuum coating area；Distance between adjustment and target；The surface coating layers of chrome of filter screen product, then in layers of chrome surface coating silver layer.Its good effect is：There has been the Nano Silver cup of plated film in our company, solves the technical matters of plug plated film Nano Silver in filter screen and cup lid again now, can so provide that silver consuming amount is few, and cost is low for market, and the acceptable entirety of consumer has the vacuum cup and glass of antibacterial functions.
Description
Technical field
Category household utensils manufacturing technology and field of nanometer technology are exactly nanometer technologies on household utensils vacuum cup
Application technology.
Background technology
Antibacterial is to be destroyed the fertility of bacterium such as by physics, chemistry or biology means using external means, realized
The growth of bacterium is destroyed and suppresses, so as to reach the purpose of disinfecting.With the development of vacuum cup technology, existing market
Upper sale has been achieved with preferable heat insulation function, but cup does not possess antibacterial functions in itself.The useful fine silver of in the market is made
Cup, there are some antibacterial effects, but silver consuming amount is more, and cost is very high, and ordinary consumer is beyond affordability.
The content of the invention
The present invention provides silver consuming amount has a kind of supporting nanometer silver antimicrobial filter screen of the and vacuum cup of antibacterial functions and it again less
Manufacture craft.
The technical solution adopted by the present invention：
A kind of and supporting nanometer silver antimicrobial filter screen of vacuum cup, comprising stainless steel filtering net product, its scheme is：Stainless steel is filtered
Net product is flat bottom straight edge disk, disk along port to surrounding in the horizontal direction, then vertically upward, and horizontally outward extension plane structure
Into；It is uniform-distribution with the horizontal plane of disk and penetrates aperture composition stainless steel filtering net product；In stainless steel filtering net article surface
It is covered with and is evenly distributed, arranges close nanometer silver antimicrobial film layer.
It is a kind of to be with the manufacture craft of the supporting nanometer silver antimicrobial filter screen of vacuum cup, its scheme：Comprise the steps of：
（1）The decontamination of stainless steel filtering net product, the cleaning of paraffin removal and drying,
（2）Pre-sputtering and bias Bombardment and cleaning are carried out respectively to target chromium and silver,
（3）Implement plated film by the plating run of the stainless steel filtering net product of setting, be included in the table of stainless steel filtering net product
Face plated film layers of chrome, and in layers of chrome surface coating silver layer.
The positive effect of the present invention：
There has been the cup of plated film Nano Silver in our company, and has patent（The patent No.：ZL201110051519.9）, it is existing
In the technical matters for solving filter screen coating film Nano Silver again, consequently also solve plug plated film in the cup lid similar with filter structure and receive
Meter Yin technical matters；So company could provide that silver consuming amount is few, and cost is very low for market, the acceptable entirety of ordinary consumer
Vacuum cup and glass with antibacterial functions.This cup is due to cup body plated film Nano Silver (Nano Silver), now again
Plated film Nano Silver will be filled in filter screen and cup lid, so as to eliminate dead angle.Nano Silver is that particle diameter is accomplished into nano level argent
Simple substance, Nano Silver particle diameter is mostly in 25 rans, to tens of kinds of micro- lifes of causing a disease such as Escherichia coli, gonococcus, chlamydia trachomatis
Thing has strong suppression and killing action, and will not produce drug resistance.Early in《Compendium of Materia Medica》Described in：Raw silver is nontoxic；
American Public Health office nineteen ninety《The survey report walked alone on silver》Middle explanation：Silver is to human body without obvious toxic-side effects；Nanometer
Silver is local application, and silver content is few, is safest application method.Find mouse in oral maximal tolerance dose through experiment investigation
925mg/kg, that is, at 4625 times of Clinical practice dosage, on without any toxic reaction, in the skin irritation test of rabbit
In, also without any stimulate the reaction of discovery.It also has to impaired epithelial cell simultaneously promotes repair.It is worth mentioning
It is that the product, which meets water antibacterial effect, more to be strengthened, the more conducively treatment of disease.
Nano-Ag particles are directly entered thalline and oxygen metabolism enzyme（-SH）With reference to the unique effect machine for making thalline be choked to death
System, can kill the microorganisms such as the most of bacteriums being in contact with it, fungi, mould, spore.Through the big authoritative institution's research hair in the country eight
It is existing；It is to pathogenic bacteria of drug-resistant such as antibiotic-resistance E. coli, resistance golden staphylococci, drug-resistant pseudomonas aeruginosa, streptococcus pyogenes, resistance intestines
Coccus, anaerobic bacteria etc. have comprehensive antibacterial activity；It is the bacterium such as staphylococcus aureus common to burn and scald and wound surface, big
Enterobacteria, Pseudomonas aeruginosa, Candida albicans and other G+, G- pathogenic bacteria have bactericidal action;To chlamydia trachomatis, causing property
The gonococcus of transmissible disease also has powerful bactericidal action.
Brief description of the drawings
Fig. 1, it is nano silver antibacterial vacuum cup filter structure schematic diagram,
Fig. 2, view is hung when being nano silver antibacterial vacuum cup filter screen coating film,
Fig. 3, it is plug structure schematic diagram in the cup lid similar with filter structure,
Fig. 4, to fill in the cup lid similar with filter structure hang view during plated film.
Embodiment
In conjunction with accompanying drawing, the invention will be further described
A kind of and supporting nanometer silver antimicrobial filter screen of vacuum cup, comprising stainless steel filtering net product, its structure is：Stainless steel is filtered
Net product is flat bottom straight edge disk, disk along port to surrounding in the horizontal direction, vertically upward and horizontally outward extension plane structure again
Into；It is uniform-distribution with the horizontal plane of disk and penetrates aperture, forms stainless steel filtering net product；In stainless steel filtering net article surface
It is covered with and is evenly distributed, arranges close nanometer silver antimicrobial film layer.
A kind of and manufacture craft of the supporting nanometer silver antimicrobial filter screen of vacuum cup, is comprised the steps of：
（1）The cleaning and drying of stainless steel filtering net product decontamination paraffin removal：Deionized water is prepared by water making device, by deionization
Water is transported to the water box slot on automatic Cleaning Line, in stainless steel filtering net product restocking to cleaning jig；Opening is automatically brought into operation interface,
Setting operation program, cleaning jig is transported to water box slot by the belt pulley of operation sequence control, implements oil removing and goes wax to clean；Profit
The attached wax of greasy dirt on stainless steel filtering net product is removed for the first time with ultrasonic wave and removed, scavenging period was at 5 to 10 minutes；And from traverse
Sequence, which enters, implements the first cleanings of Guo Shui tri-, then implements to be cleaned 5 to 10 minutes by second of paraffin removal decontamination of ultrasonic wave again, and in fact
The cleanings of Guo Shui tri- again are applied, the attached wax of oil stain on stainless steel filtering net product is removed；It is clear in 100 DEG C of high temperature above pure water by temperature
Wash 10 minutes；Cleaned 5 to 10 minutes by ultrasonic pure water afterwards, then by giant auto-flushing, be into baking temperature
80 DEG C of baking oven baking time 30 minutes, stainless steel filtering net product is dried, it is stand-by；
（2）Pre-sputtering and bias Bombardment and cleaning are carried out respectively to target chromium and silver, operating parameter is respectively：
1. pre-sputtering target
A. current limliting valve angle, 180~400sccm of argon flow amount are adjusted；
B. treat that vacuum reaches 1.0~9.0x10-1Pa, it is 3.5~9.6KW slowly to adjust target power；
C. sputter 5~20 minutes, regulation target power is 0KW；
2. bias Bombardment and cleaning
A. current limliting valve angle, 250~600sccm of argon flow amount are adjusted；
B. treat that vacuum reaches 0.5~20Pa, slowly adjust voltage to 280~680V, work 5~50 minutes；
~50 minute c.5 after, slowly adjust voltage to 0V, slowly adjust dutycycle to 0, by voltage-regulation voltage to 250~
450V, dutycycle is slowly adjusted to 60%~90%；
（3）The plating run of stainless steel filtering net product is：Stainless steel filtering net product restocking after drying is plated to coating clamp
Film fixture enters vacuum coating area；Adjust distance between coating clamp and target；Airtight vacuum room, opening operation interface, setting behaviour
Make program, into automation, PIC is transferred to by operation sequence, command each step of operation interface, target is 99.9 ﹪ purity
Silver, plated film concrete technology are as follows：
1, in the surface coating layers of chrome of stainless steel filtering net product：
A. chromium material is loaded onto at target；
B. stainless steel filtering net loads is rotated by 360 ° special fixture automatically；
C. current limliting valve angle, 50~150sccm of argon flow amount are adjusted；
D. treat that vacuum reaches 0.2~0.6x10-1Pa, it is 1.0~8.5KW slowly to adjust planar targets power；
E. 0.3~2.0h of plated film time；
2, in layers of chrome surface coating silver layer：
A. the silver-colored material of 99.9 ﹪ purity is loaded onto at target；
B. current limliting valve angle, 150~380sccm of argon flow amount are adjusted；
C. treat that vacuum reaches 0.8~9.0x10-1Pa, it is 1.0~4.5KW slowly to adjust filtered arc source target power；
D. 0.3~1.0h of plated film time；
E. shutdown operation is entered.
Claims (1)
1. a kind of and supporting nanometer silver antimicrobial filter screen of vacuum cup manufacture craft, it is characterized in that：Nanometer silver antimicrobial filter screen is received
Rice silver film makes, and comprises the steps of：（1）The decontamination of stainless steel filtering net product, the cleaning of paraffin removal and drying：By water making device
Deionized water, water box slot deionized water being transported on automatic Cleaning Line are prepared, the restocking of stainless steel filtering net product is pressed from both sides to cleaning
On tool；Opening is automatically brought into operation interface, setting operation program, and cleaning jig is transported to water tank by the belt pulley controlled by operation sequence
Groove, implement oil removing and go wax to clean；The attached wax of greasy dirt on stainless steel filtering net product is removed for the first time using ultrasonic wave and removed, during cleaning
Between at 5 to 10 minutes；And auto-programming enters the first Guo Shui tri- of implementation and cleaned, then implement again by second of paraffin removal of ultrasonic wave
Decontamination is cleaned 5 to 10 minutes, and is implemented Guo Shui tri- again and cleaned, and the attached wax of oil stain on stainless steel filtering net product is removed；By temperature
Degree cleans 10 minutes in 100 DEG C of high temperature pure water；Cleaned 5 to 10 minutes by ultrasonic pure water afterwards, then it is automatic by giant
Rinse, into the baking oven baking time 30 minutes that baking temperature is 80 DEG C, dry stainless steel filtering net product, it is stand-by；（2）To target
Chromium and silver carry out pre-sputtering and bias Bombardment and cleaning respectively, and operating parameter is respectively：1. pre-sputtering target a. adjustment flow-limiting valves angle
Degree, 180~400sccm of argon flow amount；B. treat that vacuum reaches 1.0~9.0x10-1Pa, slowly adjust target power be 3.5~
9.6KW；C. sputter 5~20 minutes, regulation target power is 0KW；2. bias Bombardment and cleaning a. adjustment current limliting valve angles, argon gas stream
Measure 250~600sccm；B. treat that vacuum reaches 0.5~20Pa, slowly adjust voltage to 280~680V, work 5~50 minutes；
~50 minute c.5 after, voltage is slowly adjusted to 0V, slowly adjusts dutycycle, by voltage-regulation to 250~450V, slowly to adjust and account for 0
Sky compares to 60%~90%；（3）The plating run of stainless steel filtering net product is：Stainless steel filtering net product restocking after drying is to plated film
Fixture, coating clamp enter vacuum coating area；Adjust distance between coating clamp and target；Airtight vacuum room, opening operation interface,
Setting operation program, into automation, PIC is transferred to by operation sequence, commands each step of operation interface, target is
The silver of 99.9 ﹪ purity, plated film concrete technology are as follows：1, in the surface coating layers of chrome of stainless steel filtering net product：A. loaded onto at target
Chromium material；B. stainless steel filtering net loads is rotated by 360 ° special fixture automatically；C. adjustment current limliting valve angle, argon flow amount 50~
150sccm；D. treat that vacuum reaches 0.2~0.6x10-1Pa, it is 1.0~8.5KW slowly to adjust planar targets power；E. plated film
0.3~2.0h of time；2, in layers of chrome surface coating silver layer：A. the silver-colored material of 99.9 ﹪ purity is loaded onto at target；B. flow-limiting valve is adjusted
Angle, 150~380sccm of argon flow amount；C. treat that vacuum reaches 0.8~9.0x10-1Pa, slowly adjust filtered arc source target work(
Rate is 1.0~4.5KW；D. 0.3~1.0h of plated film time；E. shutdown operation is entered.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510876411.1A CN105506563B (en) | 2015-12-03 | 2015-12-03 | A kind of and manufacture craft of the supporting nanometer silver antimicrobial filter screen of vacuum cup |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510876411.1A CN105506563B (en) | 2015-12-03 | 2015-12-03 | A kind of and manufacture craft of the supporting nanometer silver antimicrobial filter screen of vacuum cup |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105506563A CN105506563A (en) | 2016-04-20 |
| CN105506563B true CN105506563B (en) | 2018-01-26 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510876411.1A Active CN105506563B (en) | 2015-12-03 | 2015-12-03 | A kind of and manufacture craft of the supporting nanometer silver antimicrobial filter screen of vacuum cup |
Country Status (1)
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1865487A (en) * | 2005-05-19 | 2006-11-22 | 中华联合半导体设备制造股份有限公司 | Process for making bacteriostatic backing material with silver film |
| CN101067196A (en) * | 2007-06-14 | 2007-11-07 | 上海交通大学 | Method for raising common steel antibiotic and rust resisting performance |
| CN102108484A (en) * | 2011-01-18 | 2011-06-29 | 厦门建霖工业有限公司 | Preparation method of double-layer antimicrobial plating |
| CN103526175A (en) * | 2013-11-06 | 2014-01-22 | 武汉科技大学 | Antibacterial hard stainless steel tool and preparation method thereof |
| CN203914558U (en) * | 2013-12-31 | 2014-11-05 | 江苏希诺实业有限公司 | A kind of filter screen sub-assembly for glass |
| US8968529B2 (en) * | 2012-03-29 | 2015-03-03 | Ever Brite Technology Products Inc. | Production method for forming an antibacterial film on the surface of an object |
-
2015
- 2015-12-03 CN CN201510876411.1A patent/CN105506563B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1865487A (en) * | 2005-05-19 | 2006-11-22 | 中华联合半导体设备制造股份有限公司 | Process for making bacteriostatic backing material with silver film |
| CN101067196A (en) * | 2007-06-14 | 2007-11-07 | 上海交通大学 | Method for raising common steel antibiotic and rust resisting performance |
| CN102108484A (en) * | 2011-01-18 | 2011-06-29 | 厦门建霖工业有限公司 | Preparation method of double-layer antimicrobial plating |
| US8968529B2 (en) * | 2012-03-29 | 2015-03-03 | Ever Brite Technology Products Inc. | Production method for forming an antibacterial film on the surface of an object |
| CN103526175A (en) * | 2013-11-06 | 2014-01-22 | 武汉科技大学 | Antibacterial hard stainless steel tool and preparation method thereof |
| CN203914558U (en) * | 2013-12-31 | 2014-11-05 | 江苏希诺实业有限公司 | A kind of filter screen sub-assembly for glass |
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| Publication number | Publication date |
|---|---|
| CN105506563A (en) | 2016-04-20 |
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Address after: 226146 No.1, Xinuo Road, Haimen District, Nantong City, Jiangsu Province Patentee after: SINOSURE Co.,Ltd. Address before: 226146 No.1 Xinuo Road, Shuxun Industrial Park, Haimen City, Nantong City, Jiangsu Province Patentee before: JIANGSU HEENOOR INDUSTRIAL Co.,Ltd. |
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Address after: 226146 No.1, Xinuo Road, Haimen District, Nantong City, Jiangsu Province Patentee after: SINOSURE Co.,Ltd. Address before: 226146 No.1 Xinuo Road, Shuxun Industrial Park, Haimen City, Nantong City, Jiangsu Province Patentee before: JIANGSU HEENOOR INDUSTRIAL Co.,Ltd. |
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