CN105505492A - Efficient and stable biodiesel composite additive - Google Patents

Efficient and stable biodiesel composite additive Download PDF

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Publication number
CN105505492A
CN105505492A CN201610002732.3A CN201610002732A CN105505492A CN 105505492 A CN105505492 A CN 105505492A CN 201610002732 A CN201610002732 A CN 201610002732A CN 105505492 A CN105505492 A CN 105505492A
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parts
composite additive
biofuel
efficient
efficient stable
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CN105505492B (en
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车春玲
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Linyi Xinghuo Intellectual Property Service Co.,Ltd.
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SHANDONG TAIDE NEW ENERGY CO Ltd
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
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    • C10L1/16—Hydrocarbons
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    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/16—Hydrocarbons
    • C10L1/1608—Well defined compounds, e.g. hexane, benzene
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
    • C10L1/183—Organic compounds containing oxygen containing hydroxy groups; Salts thereof at least one hydroxy group bound to an aromatic carbon atom
    • C10L1/1832—Organic compounds containing oxygen containing hydroxy groups; Salts thereof at least one hydroxy group bound to an aromatic carbon atom mono-hydroxy
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/14—Organic compounds
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    • C10L1/19—Esters ester radical containing compounds; ester ethers; carbonic acid esters
    • C—CHEMISTRY; METALLURGY
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    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/19—Esters ester radical containing compounds; ester ethers; carbonic acid esters
    • C10L1/1915—Esters ester radical containing compounds; ester ethers; carbonic acid esters complex esters (at least 3 ester bonds)
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/14—Organic compounds
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    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/22—Organic compounds containing nitrogen
    • C10L1/222—Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond
    • C10L1/2222—(cyclo)aliphatic amines; polyamines (no macromolecular substituent 30C); quaternair ammonium compounds; carbamates
    • C10L1/2225—(cyclo)aliphatic amines; polyamines (no macromolecular substituent 30C); quaternair ammonium compounds; carbamates hydroxy containing
    • C—CHEMISTRY; METALLURGY
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    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/22—Organic compounds containing nitrogen
    • C10L1/222—Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond
    • C10L1/224—Amides; Imides carboxylic acid amides, imides
    • C—CHEMISTRY; METALLURGY
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    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
    • C10L1/2493—Organic compounds containing sulfur, selenium and/or tellurium compounds of uncertain formula; reactions of organic compounds (hydrocarbons, acids, esters) with sulfur or sulfur containing compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/26—Organic compounds containing phosphorus
    • C10L1/2608—Organic compounds containing phosphorus containing a phosphorus-carbon bond
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10L2200/00—Components of fuel compositions
    • C10L2200/02—Inorganic or organic compounds containing atoms other than C, H or O, e.g. organic compounds containing heteroatoms or metal organic complexes
    • C10L2200/0254—Oxygen containing compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10L2200/00—Components of fuel compositions
    • C10L2200/02—Inorganic or organic compounds containing atoms other than C, H or O, e.g. organic compounds containing heteroatoms or metal organic complexes
    • C10L2200/0259—Nitrogen containing compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10L2300/00—Mixture of two or more additives covered by the same group of C10L1/00 - C10L1/308
    • C10L2300/30—Mixture of three components

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Solid Fuels And Fuel-Associated Substances (AREA)

Abstract

The invention belongs to the field of fuel oil additives and particularly relates to an efficient and stable biodiesel composite additive. The efficient and stable biodiesel composite additive is composed of a complex solubilizer, oleic acid, butyl epoxystearate, double dodecyl phosphoric acid, an antioxidant, a dispersing agent, a cleanser and a combustion improver. According to the efficient and stable biodiesel composite additive, the biodiesel solidification temperature can be decreased by several degrees, the good low-temperature flow performance is kept for biodiesel, and diesel is conveniently stored and used; carbon deposition on a diesel engine can be effectively removed, and an oil way is kept smooth, so that the combustion performance and the economic performance of the diesel engine are improved, and the effects of environmental protection and energy conservation are achieved. According to the efficient and stable biodiesel composite additive, raw materials are easy to obtain, the preparation technology is simple, operation is convenient, and the cost is low.

Description

A kind of biofuel composite additive of efficient stable
Technical field
The invention belongs to fuel oil additive field, particularly relate to a kind of biofuel composite additive of efficient stable.
Background technology
Along with the quickening of China's modernization construction paces, the demand of the energy is risen fast, by the restriction of the resource reserve such as coal in China, oil and producing capacity, China is faced with the situation of power supply shortage, meanwhile, the Economic Development Mode of China has continued by the traditional development model consumed in a large number based on the energy, makes economic activity ask for the reproduction speed of speed considerably beyond resource itself of resource.Diesel oil is as a kind of important fuel, and large owing to itself having power, the advantages such as price is low, have become the major impetus fuel of main equipment.The petroleum diesel that the diesel oil of current application mainly refines from oil, it is low that petroleum diesel also exists combustionproperty relative to other fuel in application process, the problems such as CO2 emissions is larger, and atmospheric pollution is serious.Along with the continuous increase of diesel oil demand, the progressively raising of the day by day exhausted and environmental consciousness of fossil energy, novel environment friendly fuel is subject to people's attention and pays close attention to.
Biofuel (Biodiesel), refer to the lipid acid mono alkyl ester be obtained by reacting obtained by different chemical reactions by animal-plant oil (mainly referring to fatty acid triglycercide), most typical is fatty acid methyl ester.Physics and chemistry character and traditional petrifaction diesel of biofuel are closely similar; Simultaneously compared with traditional petrifaction diesel, sulphur and the aromaticity content of biofuel are low, flash-point is high, cetane value is high, have the advantages such as good oilness, are the desirable substitute energys of traditional fossil fuel, and are worldwide used widely.Usually biofuel described in the market, on Witconol 2301 subjective basis, add ignition dope form mostly, there is the defect that condensation point is high, cold filter clogging temperature is high, corrodibility is strong and cost performance is not enough, be badly in need of one can improve its combustionproperty especially compression ignite performance, improve its comprehensive cost performance, the additive of efficient stable.
Summary of the invention
The object of the invention is to: for above-mentioned Problems existing, provide one can improve its combustionproperty especially compression ignite performance, improve its comprehensive cost performance, the additive that efficient stable is clean, it is characterized in that, be made up of the raw material of following parts by weight:
Solubility promoter 40-60 parts
Oleic acid 10-20 parts
Butyl epoxy stearate 5-8 parts
Two alkylphosphonic acid carboxylic acid 5-15 parts
Antioxidant 1-5 parts
Dispersion agent 5-15 parts
Sanitising agent 5-15 parts
Ignition dope 10-15 parts
Solubility promoter described in said ratio is by isopropylcarbinol: acetone: normal hexane=5:3:2 quality proportioning forms.
Oxidation inhibitor described in said ratio is by N, N'-bis-salicylidene propylene diamine: BHT=2:1 quality proportioning forms.
Dispersion agent described in said ratio is one or more in vinyl bis-stearamides, glyceryl monostearate, Tristearoylglycerol.
Sanitising agent described in said ratio is by barium mahogany sulfonate: ethylene glycol alkyl phenylate=1:1 quality proportioning forms.
Ignition dope described in said ratio is by polyethylene polyamine hydramine: Di Iso Propyl Ether: mix light aromatic hydrocarbons=2:3:5 quality proportioning and form.
The present invention has following beneficial effect: additive prepared by (1) the present invention can make biofuel temperature of solidification reduce many degrees, and the low temperature flowability making biofuel keep good, facilitates accumulating and the use of diesel oil; (2) poison gas can not be produced after the additive burning that prepared by the present invention, can carbon distribution effectively on clean diesel machine, keep oil circuit unimpeded, thus the combustionproperty of raising diesel engine and economic performance; There is environmental protection and energy saving effect; (3) preparation technology of the present invention is simple, easy to operate, with low cost.
Embodiment
Embodiment 1
Solubility promoter 40 parts
Oleic acid 20 parts
Butyl epoxy stearate 5 parts
Two alkylphosphonic acid carboxylic acid 5 parts
Antioxidant 5 parts
Dispersion agent 5 parts
Sanitising agent 5 parts
Ignition dope 15 parts
Taking quality proportioning is isopropylcarbinol: acetone: normal hexane=5:3:2 solubility promoter 40 parts, oleic acid 20 parts, butyl epoxy stearate 5 parts, two alkylphosphonic acid carboxylic acid 5 parts, by N, N'-bis-salicylidene propylene diamine: 2, 6-di-t-butyl-4-cresols=2:1 quality proportioning composition antioxidant 5 parts, vinyl bis-stearamides 5 parts, by barium mahogany sulfonate: ethylene glycol alkyl phenylate=1:1 quality proportioning forms sanitising agent 5 parts, by polyethylene polyamine hydramine: Di Iso Propyl Ether: mix light aromatic hydrocarbons=2:3:5 quality proportioning and form ignition dope 15 parts, , raw material is added in reactor successively, heat, when component is heated to 30 DEG C, stir 30 minutes, after stirring and get final product.
Embodiment 2
Solubility promoter 40 parts
Oleic acid 15 parts
Butyl epoxy stearate 8 parts
Two alkylphosphonic acid carboxylic acid 5 parts
Antioxidant 2 parts
Dispersion agent 10 parts
Sanitising agent 5 parts
Ignition dope 15 parts
Taking quality proportioning is isopropylcarbinol: acetone: normal hexane=5:3:2 solubility promoter 40 parts, oleic acid 15 parts, butyl epoxy stearate 8 parts, two alkylphosphonic acid carboxylic acid 5 parts, by N, N'-bis-salicylidene propylene diamine: 2, 6-di-t-butyl-4-cresols=2:1 quality proportioning composition antioxidant 2 parts, glyceryl monostearate 10 parts, by barium mahogany sulfonate: ethylene glycol alkyl phenylate=1:1 quality proportioning forms sanitising agent 5 parts, by polyethylene polyamine hydramine: Di Iso Propyl Ether: mix light aromatic hydrocarbons=2:3:5 quality proportioning and form ignition dope 15 parts, , raw material is added in reactor successively, heat, when component is heated to 30 DEG C, stir 30 minutes, after stirring and get final product.
With above-mentioned according to desirable embodiment of the present invention for enlightenment, by above-mentioned description, relevant staff in the scope not departing from this invention technological thought, can carry out various change and amendment completely.The technical scope of this invention is not limited to the content on specification sheets, must determine its technical scope according to right.

Claims (6)

1. a biofuel composite additive for efficient stable, is characterized in that, is made up of the raw material of following parts by weight:
Solubility promoter 40-60 parts
Oleic acid 10-20 parts
Butyl epoxy stearate 5-8 parts
Two alkylphosphonic acid carboxylic acid 5-15 parts
Antioxidant 1-5 parts
Dispersion agent 5-15 parts
Sanitising agent 5-15 parts
Ignition dope 10-15 parts.
2. the biofuel composite additive of a kind of efficient stable according to claim 1, is characterized in that described solubility promoter is by isopropylcarbinol: acetone: normal hexane=5:3:2 quality proportioning forms.
3. the biofuel composite additive of a kind of efficient stable according to claim 1, is characterized in that described oxidation inhibitor is by N, N'-bis-salicylidene propylene diamine: BHT=2:1 quality proportioning forms.
4. the biofuel composite additive of a kind of efficient stable according to claim 1, is characterized in that described dispersion agent is one or more in vinyl bis-stearamides, glyceryl monostearate, Tristearoylglycerol.
5. the biofuel composite additive of a kind of efficient stable according to claim 1, is characterized in that described sanitising agent is by barium mahogany sulfonate: ethylene glycol alkyl phenylate=1:1 quality proportioning forms.
6. the biofuel composite additive of a kind of efficient stable according to claim 1, is characterized in that described ignition dope is by polyethylene polyamine hydramine: Di Iso Propyl Ether: mix light aromatic hydrocarbons=2:3:5 quality proportioning and form.
CN201610002732.3A 2016-01-06 2016-01-06 A kind of biodiesel compound additive of efficient stable Active CN105505492B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109294688A (en) * 2018-10-24 2019-02-01 定远县碧蓝山新能源有限公司 A kind of environment-friendly biomass fuel additive

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6767374B1 (en) * 1995-03-14 2004-07-27 Exxon Chemical Patents Inc. Fuel oil additives and compositions
CN103509615A (en) * 2012-06-14 2014-01-15 刘粤荣 Fuel oil blending additive and preparation method thereof
CN104357101A (en) * 2014-11-06 2015-02-18 金景达(北京)环保动力科技有限公司 High-efficiency stable composite biodiesel fuel

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6767374B1 (en) * 1995-03-14 2004-07-27 Exxon Chemical Patents Inc. Fuel oil additives and compositions
CN103509615A (en) * 2012-06-14 2014-01-15 刘粤荣 Fuel oil blending additive and preparation method thereof
CN104357101A (en) * 2014-11-06 2015-02-18 金景达(北京)环保动力科技有限公司 High-efficiency stable composite biodiesel fuel

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109294688A (en) * 2018-10-24 2019-02-01 定远县碧蓝山新能源有限公司 A kind of environment-friendly biomass fuel additive

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