CN105481046A - Efficient and environment-friendly wastewater treating agent and preparation method thereof - Google Patents
Efficient and environment-friendly wastewater treating agent and preparation method thereof Download PDFInfo
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- CN105481046A CN105481046A CN201610046626.5A CN201610046626A CN105481046A CN 105481046 A CN105481046 A CN 105481046A CN 201610046626 A CN201610046626 A CN 201610046626A CN 105481046 A CN105481046 A CN 105481046A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
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- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
- B01J20/0262—Compounds of O, S, Se, Te
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
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- B01J20/0288—Halides of compounds other than those provided for in B01J20/046
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
- B01J20/0274—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04 characterised by the type of anion
- B01J20/0296—Nitrates of compounds other than those provided for in B01J20/04
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
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- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/041—Oxides or hydroxides
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/045—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing sulfur, e.g. sulfates, thiosulfates, gypsum
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- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/12—Naturally occurring clays or bleaching earth
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- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/285—Treatment of water, waste water, or sewage by sorption using synthetic organic sorbents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/46—Materials comprising a mixture of inorganic and organic materials
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/48—Sorbents characterised by the starting material used for their preparation
- B01J2220/4806—Sorbents characterised by the starting material used for their preparation the starting material being of inorganic character
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- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/48—Sorbents characterised by the starting material used for their preparation
- B01J2220/4812—Sorbents characterised by the starting material used for their preparation the starting material being of organic character
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2305/00—Use of specific compounds during water treatment
- C02F2305/04—Surfactants, used as part of a formulation or alone
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Abstract
The invention discloses an efficient and environment-friendly wastewater treating agent and a preparation method thereof. The efficient and environment-friendly wastewater treating agent is prepared from raw materials as follows: soybean protein, ammonium persulfate, potassium nitrite, ethylene dichloride, hydrogen peroxide, potassium hydroxide, sodium hexameta-sulfate, bis-succinimide, vesuvianite, carboxymethyl chitosan, barium sulfide, ferric nitrate, seaweed soil, hypochlorous acid and dimethyl sulfate. The efficient and environment-friendly wastewater treating agent has a wide application range and is environment-friendly, non-toxic and high in purification efficiency.
Description
Technical field
The present invention relates to a kind of high-efficiency environment friendly waste water conditioner and preparation method thereof.
Background technology
Due to population growth and Economic development, the series of problems affecting resource quality produced the excessive exploitation of resource and unreasonable development, these problems have directly threatened the existence of we and descendants.
China is faced with these problems equally, and China is the country of a water resources shortage, how to alleviate the problem such as water resources shortage and pollution and has become an instant problem.
At present, process water resource pollution problem has physics, chemistry, biology, the multiple method such as comprehensive, but to there is treatment effect not good more for physical method, processing rate instability problem; Biological method processing cost is too high, is not suitable for promoting the use of; Many employings chemical process is disposed of sewage, but existing sewage-treating agent, and there is secondary pollution problem in its agent formulations, also can have a certain impact to environment.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of applied widely, environment-protecting asepsis and the high high-efficiency environment friendly waste water conditioner of purification efficiency and preparation method thereof.
For solving the problems of the technologies described above, the present invention adopts following technical scheme:
A kind of high-efficiency environment friendly waste water conditioner and preparation method thereof, is made up of following raw material: soybean protein, ammonium persulphate, potassium nitrite, ethylene dichloride, hydrogen peroxide, potassium hydroxide, six inclined sodium sulfate, two succimide, volcanized rock, cm-chitosan, barium sulphide, iron nitrate, marine alga soil, hypochlorous acid and methyl-sulfate, described raw material is by following parts by weight proportioning composition: soybean protein 20 ?22 parts, ammonium persulphate 16 ?18 parts, potassium nitrite 18 ?20 parts, ethylene dichloride 16 ?18 parts, hydrogen peroxide 12 ?16 parts, potassium hydroxide 10 ?12 parts, six inclined sodium sulfate 14 ?16 parts, two succimide 12 ?18 parts, volcanized rock 16 ?18 parts, cm-chitosan 10 ?12 parts, barium sulphide 12 ?16 parts, iron nitrate 16 ?20 parts, marine alga soil 20 ?22 parts, hypochlorous acid 16 ?20 parts and methyl-sulfate 10 ?16 parts.
Further, described raw material is by following parts by weight proportioning composition: soybean protein 20 parts, ammonium persulphate 18 parts, potassium nitrite 20 parts, ethylene dichloride 18 parts, 16 parts, hydrogen peroxide, 12 parts, potassium hydroxide, six inclined 16 parts, sodium sulfate, two succimide 18 parts, volcanized rock 18 parts, cm-chitosan 12 parts, barium sulphide 16 parts, iron nitrate 20 parts, 22 parts, marine alga soil, hypochlorous acid 20 parts and methyl-sulfate 16 parts.
Further, described raw material is by following parts by weight proportioning composition: soybean protein 21 parts, ammonium persulphate 17 parts, potassium nitrite 19 parts, ethylene dichloride 17 parts, 14 parts, hydrogen peroxide, 11 parts, potassium hydroxide, six inclined 15 parts, sodium sulfate, two succimide 15 parts, volcanized rock 17 parts, cm-chitosan 11 parts, barium sulphide 14 parts, iron nitrate 18 parts, 21 parts, marine alga soil, hypochlorous acid 18 parts and methyl-sulfate 13 parts.
Further, described raw material is by following parts by weight proportioning composition: soybean protein 22 parts, ammonium persulphate 16 parts, potassium nitrite 18 parts, ethylene dichloride 16 parts, 12 parts, hydrogen peroxide, 10 parts, potassium hydroxide, six inclined 14 parts, sodium sulfate, two succimide 12 parts, volcanized rock 16 parts, cm-chitosan 10 parts, barium sulphide 12 parts, iron nitrate 16 parts, 20 parts, marine alga soil, hypochlorous acid 16 parts and methyl-sulfate 10 parts.
Another technical problem that the present invention will solve is to provide a kind of preparation method of high-efficiency environment friendly waste water conditioner, includes following steps:
1) get soybean protein 20 ?22 parts, ammonium persulphate 16 ?18 parts, potassium nitrite 18 ?20 parts, ethylene dichloride 16 ?18 parts, hydrogen peroxide 12 ?16 parts and potassium hydroxide 10 ?12 parts, put into stirrer, stir;
2) material after above-mentioned stirring is put into well heater, temperature rise to 80 ?90 DEG C, heat 5 ?10min, for subsequent use;
3) get volcanized rock 16 ?18 parts and marine alga soil 20 ?22 parts, put into micronizer mill, be ground into 100 ?140 object powders, for subsequent use;
4) get six inclined sodium sulfate 14 ?16 parts, two succimide 12 ?18 parts, cm-chitosan 10 ?12 parts and barium sulphide 12 ?16 parts, put into a container, with vibration of ultrasonic wave 15 ?25min, hyperacoustic vibration frequency is 1000w, for subsequent use;
5) by step 2), step 3) and step 4) in obtained material put into stirrer, stir, leave standstill 10 ?15min;
6) by step 5) in obtained material put into well heater, temperature rise to 60 ?80 DEG C, heat 5 ?10min;
7) get iron nitrate 16 ?20 parts, hypochlorous acid 16 ?20 parts and methyl-sulfate 10 ?16 parts add step 6 to) in material after heating, the interpolation of often kind of material is spaced apart 5min, and interpolation limit, limit is stirred, and can obtain high-efficiency environment friendly waste water conditioner.
Beneficial effect of the present invention is: this high-efficiency environment friendly waste water conditioner is under the effect of cooperatively interacting of each raw material, it has applied widely, environment-protecting asepsis and the high advantage of purification efficiency, this effect Environment-friendlywastewater wastewater treatment agent has good adsorption, the pollutent be suspended in sewage can be adsorbed, secondary injury can not be caused to water quality simultaneously.
Embodiment
Embodiment 1:
A kind of high-efficiency environment friendly waste water conditioner, described raw material is by following parts by weight proportioning composition: soybean protein 20 parts, ammonium persulphate 18 parts, potassium nitrite 20 parts, ethylene dichloride 18 parts, 16 parts, hydrogen peroxide, 12 parts, potassium hydroxide, six inclined 16 parts, sodium sulfate, two succimide 18 parts, volcanized rock 18 parts, cm-chitosan 12 parts, barium sulphide 16 parts, iron nitrate 20 parts, 22 parts, marine alga soil, hypochlorous acid 20 parts and methyl-sulfate 16 parts.
A preparation method for high-efficiency environment friendly waste water conditioner, includes following steps:
1) get soybean protein 20 parts, ammonium persulphate 18 parts, potassium nitrite 20 parts, ethylene dichloride 18 parts, 16 parts, hydrogen peroxide and 12 parts, potassium hydroxide, put into stirrer, stir;
2) material after above-mentioned stirring is put into well heater, temperature rise to 80 ?90 DEG C, heat 5 ?10min, for subsequent use;
3) get volcanized rock 18 parts and 22 parts, marine alga soil, put into micronizer mill, be ground into 100 ?140 object powders, for subsequent use;
4) get six inclined 16 parts, sodium sulfate, two succimide 18 parts, cm-chitosan 12 parts and barium sulphide 16 parts, put into a container, with vibration of ultrasonic wave 15 ?25min, hyperacoustic vibration frequency is 1000w, for subsequent use;
5) by step 2), step 3) and step 4) in obtained material put into stirrer, stir, leave standstill 10 ?15min;
6) by step 5) in obtained material put into well heater, temperature rise to 60 ?80 DEG C, heat 5 ?10min;
7) get iron nitrate 20 parts, hypochlorous acid 20 parts and methyl-sulfate 16 parts and add step 6 to) heating after material in, the interpolation of often kind of material is spaced apart 5min, interpolation limit, limit stir, high-efficiency environment friendly waste water conditioner can be obtained.
Embodiment 2:
A kind of high-efficiency environment friendly waste water conditioner, described raw material is by following parts by weight proportioning composition: soybean protein 21 parts, ammonium persulphate 17 parts, potassium nitrite 19 parts, ethylene dichloride 17 parts, 14 parts, hydrogen peroxide, 11 parts, potassium hydroxide, six inclined 15 parts, sodium sulfate, two succimide 15 parts, volcanized rock 17 parts, cm-chitosan 11 parts, barium sulphide 14 parts, iron nitrate 18 parts, 21 parts, marine alga soil, hypochlorous acid 18 parts and methyl-sulfate 13 parts.
A preparation method for high-efficiency environment friendly waste water conditioner, includes following steps:
1) get soybean protein 21 parts, ammonium persulphate 17 parts, potassium nitrite 19 parts, ethylene dichloride 17 parts, 14 parts, hydrogen peroxide and 11 parts, potassium hydroxide, put into stirrer, stir;
2) material after above-mentioned stirring is put into well heater, temperature rise to 80 ?90 DEG C, heat 5 ?10min, for subsequent use;
3) get volcanized rock 17 parts and 21 parts, marine alga soil, put into micronizer mill, be ground into 100 ?140 object powders, for subsequent use;
4) get six inclined 15 parts, sodium sulfate, two succimide 15 parts, cm-chitosan 11 parts and barium sulphide 14 parts, put into a container, with vibration of ultrasonic wave 15 ?25min, hyperacoustic vibration frequency is 1000w, for subsequent use;
5) by step 2), step 3) and step 4) in obtained material put into stirrer, stir, leave standstill 10 ?15min;
6) by step 5) in obtained material put into well heater, temperature rise to 60 ?80 DEG C, heat 5 ?10min;
7) get iron nitrate 18 parts, hypochlorous acid 18 parts and methyl-sulfate 13 parts and add step 6 to) heating after material in, the interpolation of often kind of material is spaced apart 5min, interpolation limit, limit stir, high-efficiency environment friendly waste water conditioner can be obtained.
Embodiment 3:
A kind of high-efficiency environment friendly waste water conditioner, described raw material is by following parts by weight proportioning composition: soybean protein 22 parts, ammonium persulphate 16 parts, potassium nitrite 18 parts, ethylene dichloride 16 parts, 12 parts, hydrogen peroxide, 10 parts, potassium hydroxide, six inclined 14 parts, sodium sulfate, two succimide 12 parts, volcanized rock 16 parts, cm-chitosan 10 parts, barium sulphide 12 parts, iron nitrate 16 parts, 20 parts, marine alga soil, hypochlorous acid 16 parts and methyl-sulfate 10 parts.
A preparation method for high-efficiency environment friendly waste water conditioner, includes following steps:
1) get soybean protein 22 parts, ammonium persulphate 16 parts, potassium nitrite 18 parts, ethylene dichloride 16 parts, 12 parts, hydrogen peroxide and 10 parts, potassium hydroxide, put into stirrer, stir;
2) material after above-mentioned stirring is put into well heater, temperature rise to 80 ?90 DEG C, heat 5 ?10min, for subsequent use;
3) get volcanized rock 16 parts and 20 parts, marine alga soil, put into micronizer mill, be ground into 100 ?140 object powders, for subsequent use;
4) get six inclined 14 parts, sodium sulfate, two succimide 12 parts, cm-chitosan 10 parts and barium sulphide 12 parts, put into a container, with vibration of ultrasonic wave 15 ?25min, hyperacoustic vibration frequency is 1000w, for subsequent use;
5) by step 2), step 3) and step 4) in obtained material put into stirrer, stir, leave standstill 10 ?15min;
6) by step 5) in obtained material put into well heater, temperature rise to 60 ?80 DEG C, heat 5 ?10min;
7) get iron nitrate 16 parts, hypochlorous acid 16 parts and methyl-sulfate 10 parts and add step 6 to) heating after material in, the interpolation of often kind of material is spaced apart 5min, interpolation limit, limit stir, high-efficiency environment friendly waste water conditioner can be obtained.
Experimental example:
Experimental subjects: select high-efficiency environment friendly waste water conditioner of the present invention and two kinds of common waste water conditioners, be divided into experimental group, control group 1 and control group 2 respectively.
Experimental technique: the waste water the same to three groups of pollution levels respectively with the waste water conditioner of each group processes.
Experimental result:
As can be seen here, the action effect of high-efficiency environment friendly waste water conditioner of the present invention to waste water is best, compared with common waste water conditioner, has marked improvement.
Beneficial effect of the present invention is: this high-efficiency environment friendly waste water conditioner is under the effect of cooperatively interacting of each raw material, it has applied widely, environment-protecting asepsis and the high advantage of purification efficiency, this effect Environment-friendlywastewater wastewater treatment agent has good adsorption, the pollutent be suspended in sewage can be adsorbed, secondary injury can not be caused to water quality simultaneously.
Typical case:
Factory between Zhang and friend's cooperative construction one, have passed through 2 years, its Plant development is stablized, but Huang finds that the discharge of wastewater problem of its factory is very serious, neighbouring trees are caused to wither, Huang feels to regret, so bring into use the waste water of common waste water conditioner to factory to renovate, employ 1 year, little to the treatment effect of waste water, but also create secondary pollution, after Huang employs high-efficiency environment friendly waste water conditioner of the present invention afterwards, the discharge of waste water obtains effective regulation, environment near factory also starts to improve gradually, arboreal growth obtains more and more vigorous.
The above, be only the specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, and any change of expecting without creative work or replacement, all should be encompassed in protection scope of the present invention.
Claims (5)
1. high-efficiency environment friendly waste water conditioner and preparation method thereof, is characterized in that: be made up of following raw material: soybean protein, ammonium persulphate, potassium nitrite, ethylene dichloride, hydrogen peroxide, potassium hydroxide, six inclined sodium sulfate, two succimide, volcanized rock, cm-chitosan, barium sulphide, iron nitrate, marine alga soil, hypochlorous acid and methyl-sulfate, described raw material is by following parts by weight proportioning composition: soybean protein 20 ?22 parts, ammonium persulphate 16 ?18 parts, potassium nitrite 18 ?20 parts, ethylene dichloride 16 ?18 parts, hydrogen peroxide 12 ?16 parts, potassium hydroxide 10 ?12 parts, six inclined sodium sulfate 14 ?16 parts, two succimide 12 ?18 parts, volcanized rock 16 ?18 parts, cm-chitosan 10 ?12 parts, barium sulphide 12 ?16 parts, iron nitrate 16 ?20 parts, marine alga soil 20 ?22 parts, hypochlorous acid 16 ?20 parts and methyl-sulfate 10 ?16 parts.
2. high-efficiency environment friendly waste water conditioner as claimed in claim 2 and preparation method thereof, is characterized in that: described raw material forms by following parts by weight proportioning: soybean protein 20 parts, ammonium persulphate 18 parts, potassium nitrite 20 parts, ethylene dichloride 18 parts, 16 parts, hydrogen peroxide, 12 parts, potassium hydroxide, six inclined 16 parts, sodium sulfate, two succimide 18 parts, volcanized rock 18 parts, cm-chitosan 12 parts, barium sulphide 16 parts, iron nitrate 20 parts, 22 parts, marine alga soil, hypochlorous acid 20 parts and methyl-sulfate 16 parts.
3. high-efficiency environment friendly waste water conditioner as claimed in claim 3 and preparation method thereof, is characterized in that: described raw material forms by following parts by weight proportioning: soybean protein 21 parts, ammonium persulphate 17 parts, potassium nitrite 19 parts, ethylene dichloride 17 parts, 14 parts, hydrogen peroxide, 11 parts, potassium hydroxide, six inclined 15 parts, sodium sulfate, two succimide 15 parts, volcanized rock 17 parts, cm-chitosan 11 parts, barium sulphide 14 parts, iron nitrate 18 parts, 21 parts, marine alga soil, hypochlorous acid 18 parts and methyl-sulfate 13 parts.
4. high-efficiency environment friendly waste water conditioner as claimed in claim 4 and preparation method thereof, is characterized in that: described raw material forms by following parts by weight proportioning: soybean protein 22 parts, ammonium persulphate 16 parts, potassium nitrite 18 parts, ethylene dichloride 16 parts, 12 parts, hydrogen peroxide, 10 parts, potassium hydroxide, six inclined 14 parts, sodium sulfate, two succimide 12 parts, volcanized rock 16 parts, cm-chitosan 10 parts, barium sulphide 12 parts, iron nitrate 16 parts, 20 parts, marine alga soil, hypochlorous acid 16 parts and methyl-sulfate 10 parts.
5. a preparation method for high-efficiency environment friendly waste water conditioner, is characterized in that: include following steps:
1) get soybean protein 20 ?22 parts, ammonium persulphate 16 ?18 parts, potassium nitrite 18 ?20 parts, ethylene dichloride 16 ?18 parts, hydrogen peroxide 12 ?16 parts and potassium hydroxide 10 ?12 parts, put into stirrer, stir;
2) material after above-mentioned stirring is put into well heater, temperature rise to 80 ?90 DEG C, heat 5 ?10min, for subsequent use;
3) get volcanized rock 16 ?18 parts and marine alga soil 20 ?22 parts, put into micronizer mill, be ground into 100 ?140 object powders, for subsequent use;
4) get six inclined sodium sulfate 14 ?16 parts, two succimide 12 ?18 parts, cm-chitosan 10 ?12 parts and barium sulphide 12 ?16 parts, put into a container, with vibration of ultrasonic wave 15 ?25min, hyperacoustic vibration frequency is 1000w, for subsequent use;
5) by step 2), step 3) and step 4) in obtained material put into stirrer, stir, leave standstill 10 ?15min;
6) by step 5) in obtained material put into well heater, temperature rise to 60 ?80 DEG C, heat 5 ?10min;
7) get iron nitrate 16 ?20 parts, hypochlorous acid 16 ?20 parts and methyl-sulfate 10 ?16 parts add step 6 to) in material after heating, the interpolation of often kind of material is spaced apart 5min, and interpolation limit, limit is stirred, and can obtain high-efficiency environment friendly waste water conditioner.
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Publication number | Priority date | Publication date | Assignee | Title |
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CN110272111A (en) * | 2019-07-31 | 2019-09-24 | 郑州恒博环境科技股份有限公司 | A kind of oxidant and preparation method thereof removing high-salt wastewater COD organic matter |
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