CN105419956A - Production method and equipment of MES-containing powdery composition with good liquidity - Google Patents
Production method and equipment of MES-containing powdery composition with good liquidity Download PDFInfo
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- CN105419956A CN105419956A CN201510710728.8A CN201510710728A CN105419956A CN 105419956 A CN105419956 A CN 105419956A CN 201510710728 A CN201510710728 A CN 201510710728A CN 105419956 A CN105419956 A CN 105419956A
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Abstract
The present invention discloses a production method and equipment of an MES-containing powdery composition with good liquidity. The MES-containing powdery composition comprises 70-95 weight parts of fatty acid methyl ester sulfonate sodium (MES), 10-30 weight parts of mirabilite and 0-30 weight parts of zeolite. The fatty acid methyl ester sulfonate sodium (MES) is ground and weighted and is mixed with the raw materials of powdery mirabilite and zeolite to prepare an MES raw material composition containing a certain ratio of mirabilite. The mirabilite is added into the MES raw material, so that the lumping problem of the MES raw material can be solved, and the liquidity of the raw material is improved.
Description
Technical field
The present invention relates to a kind of tensio-active agent, belong to daily chemical products technical field, the powdery particularly relating to a kind of good fluidity contains production method and the equipment of MES composition.
Background technology
Methyl sodiosul foaliphatate (MES), as a kind of daily use chemicals cleaning product raw material, is a kind of tensio-active agent of very excellent anti-performance of hard water.In powder-like product, methyl sodiosul foaliphatate (MES) generally directly mixes interpolation with the form of powdery with other compositions of product.
Because raw material itself has viscosity, meeting conglomeration quickly in process deposited by the MES raw material of powdery.Impact accurately and easily adds the application that have impact on MES raw material when subsequent product is produced, hinder this raw material applying quickly in powdery cleaning product.
For addressing this problem, many measures are taken in industry, in powdery MES raw material, be wherein mixed into zeolite (addition is about 15%) have certain help to the mobility of MES raw material and the improvement of anti-caking effect, but in the application process of reality, luming and the normal phenomenon used of impact still appears in raw material.
Therefore, how seeking a kind of expense cost low and can reduce powdery MES raw material caking further and can improve the production technology of mobility, is the technical barrier that MES raw material production field and powdery cleaning product production field are paid close attention to for a long time.
Summary of the invention
For the problem that MES powder raw material easily lumps, the object of the present invention is to provide a kind of production method of powdery containing MES composition of good fluidity, its powdery MES raw material or containing the MES raw material of zeolite in add the agglomeration problems that saltcake can improve MES raw material, and improve the mobility of raw material.
Another object of the present invention is to the production unit providing a kind of powdery of above-mentioned good fluidity containing MES composition.
In order to achieve the above object, following technical scheme is adopted:
The powdery of good fluidity, containing a production method for MES composition, comprises the following steps:
1), after methyl sodiosul foaliphatate (MES) raw material or the MES raw material that is mixed with zeolite materials being ground, respectively by electronic scales metering, the saltcake raw material of powdery is also measured by electronic scales;
2) above-mentioned two or three raw material joins in impeller respectively continuously, in impeller, mix discharging continuously, is mixed with containing the powdery MES composition of certain proportion containing saltcake.
Production method of the present invention, step 1) in, the consumption of described methyl sodiosul foaliphatate (MES) raw material is 70-95 weight part; The consumption of described zeolite materials is 0-30 weight part; The consumption of powdery saltcake raw material is 10-30 weight part.
Production method of the present invention, step 1) in, the raw material dosage of described methyl sodiosul foaliphatate (MES) is 75-80 weight part; The consumption of described zeolite materials is 5-25 weight part; The consumption of described powdery saltcake is 10-15 weight part.
Production method of the present invention, grinds rear weighing by methyl sodiosul foaliphatate (MES), with zeolite materials and the mixing of saltcake raw material of powdery, is mixed with the MES raw material containing certain proportion saltcake.
Production method of the present invention, described MES raw material is powdery; Described sodium sulfate raw material is powdery; The ratio of saltcake raw material in MES mixing raw material is no more than 30%, is preferably 10%-20%.
In addition, the present invention also provides a kind of production unit of powdery containing MES composition of good fluidity, and it comprises:
The multiple raw material feed bins connected successively, the upper end of each raw material feed bin is connected with jumbo bag lifting gear; The lower end of each raw material feed bin is connected with measuring apparatus; Be arranged on the raw material travelling belt of multiple measuring apparatus lower end, for the multiple raw materials after conveying and metering; Impeller, the exit end of the corresponding above-mentioned raw materials travelling belt of its opening end, for carrying out rotation mixing by the multiple raw materials after metering; Compound travelling belt, the exit end of its entrance corresponding rotation mixing tank; Fly-ash separator, is connected to impeller, for the production of the automatic dust removing of equipment.
Production unit of the present invention, described raw material feed bin comprises: the first feed bin of splendid attire zeolite materials, and the second feed bin of splendid attire saltcake raw material and splendid attire newly grind the 3rd feed bin of MES raw material.
Production unit of the present invention, the lower end of described first feed bin is connected with the first weigher weighing zeolite materials; The lower end of described second feed bin is connected with the second weigher weighing saltcake raw material; The lower end of described 3rd feed bin is connected with the 3rd weigher that weighing newly grinds MES raw material.
Production unit of the present invention, the upper end of described first feed bin is connected with the first lifter promoting zeolite materials, the upper end of described second feed bin is connected with the second lifter promoting saltcake raw material, and the upper end of described 3rd feed bin is connected with the 3rd lifter that lifting newly grinds MES raw material.
Owing to have employed above technical scheme, the beneficial effect that the present invention has is:
1, adopt above technology, saltcake raw material can mix Homogeneous phase mixing by a certain percentage with powdery MES raw material; Or adopt saltcake raw material to mix Homogeneous phase mixing in proportion with zeolite materials and powdery MES raw material.
2, be mixed with the MES raw material of saltcake, compared with the MES raw material not adding saltcake, in the agglomeration resistance and mobility raising of raw material, have unusual effect.
3, when producing powdery cleaning product, the MES being mixed with saltcake in advance can more evenly, continuously add in production process.
4, raw material is in certain storage pilling up time, and still can avoid caking, what improve raw material deposits quality and safety and ease of use.
Accompanying drawing explanation
Fig. 1 newly grinds MES raw material and saltcake, zeolite hybrid technique schema material to feed intake schematic diagram.
First feed bin 11, second feed bin 12,
3rd feed bin 13; First weigher 21,
Second weigher the 22, three weigher 23;
First lifter 31, second lifter 32,
3rd lifter 33, raw material travelling belt 41,
Compound travelling belt 42, impeller 50,
Fly-ash separator 60.
Embodiment
Refer to shown in Fig. 1, the production unit of a kind of powdery fatty acids of the present invention methyl ester sulfonate (MES) composition comprises: the multiple raw material feed bins connected successively, first feed bin 11 of splendid attire zeolite materials, the second feed bin 12 of splendid attire saltcake raw material and splendid attire newly grind the 3rd feed bin 13 of MES raw material.
The lower end of each feed bin is connected to measuring apparatus, the lower end of this first feed bin 11 is connected with the first weigher 21 (electronics Weightlessness balance) weighing zeolite materials, the lower end of this second feed bin 12 is connected with the second weigher 22 (electronics Weightlessness balance) weighing saltcake raw material, and the lower end of the 3rd feed bin 13 is connected with the 3rd weigher 23 (electronics Weightlessness balance) that weighing newly grinds MES raw material.
The upper end of each feed bin is connected to jumbo bag lifting gear, the upper end of this first feed bin 11 is connected with the first lifter 31 promoting zeolite materials, the upper end that the upper end of this second feed bin 12 is connected with the second lifter the 32, three feed bin 13 promoting saltcake raw material is connected with the 3rd lifter 33 that lifting newly grinds MES raw material.
Respectively by zeolite materials, the saltcake raw material after the weighing of above-mentioned first weigher 21, second weigher 22 and the 3rd weigher 23 and newly grind MES raw material and drop on raw material travelling belt 41 by action of gravity, and drop in impeller 50 by this raw material travelling belt 41, be provided with an impeller 50 immediately below the other end of this raw material travelling belt 41.This impeller 50 is also connected with a fly-ash separator 60.After all raw materials mix continuously in this impeller 50, be made into the MES powder raw material containing saltcake of good fluidity.The other end outlet below of this impeller 50 is provided with compound travelling belt 42, stand-by after being packaged into product.
Below by way of concrete preferred embodiment, the present invention is expressed in further detail, but the present invention is not limited in following embodiment.Following per-cent is all weight percentage.
embodiment 1
Zeolite materials is put in the first feed bin 11; Saltcake raw material is put in the second feed bin 12; The MES raw material newly ground is put in the 3rd feed bin 13; The MES raw material of the continuous weighing material total amount 75% of MES first weigher 21 newly ground by metering outfit; Zeolite materials is by 15% of the continuous weighing material total amount of the second weigher 22; Saltcake is by 10% of the continuous weighing material total amount of the 3rd weigher 23.After impeller 3 continuously mixing, be made into the MES powder raw material containing saltcake 10%.
embodiment 2
The MES raw material newly ground is put in the first feed bin 11; Zeolite materials is put in the second feed bin 12; Saltcake raw material is put in the 3rd feed bin 13; The MES raw material of the continuous weighing material total amount 70% of MES first weigher 21 newly ground by metering outfit; Zeolite materials is by 15% of the continuous weighing material total amount of the second weigher 22; Saltcake is by 15% of the continuous weighing material total amount of the 3rd weigher 23.After impeller 50 continuously mixing, be made into the MES powder raw material composition containing saltcake 15%.
embodiment 3
Zeolite materials is put in the first feed bin 11; Saltcake raw material is put in the second feed bin 12; The MES raw material newly ground is put in the 3rd feed bin 13; The MES raw material of the continuous weighing material total amount 80% of MES first weigher 21 newly ground by metering outfit; Zeolite materials is by 10% of the continuous weighing material total amount of the second weigher 22; Saltcake is by 10% of the continuous weighing material total amount of the 3rd weigher 23.After impeller 50 continuously mixing, be made into the MES powder raw material composition containing saltcake 20%.
effect test example 1
The MES containing zeolite 15%, saltcake 10% of every jumbo bag 600Kg and the MES only containing 15% zeolite of every jumbo bag 600Kg, carry out liquidity costs contrast, related data is as shown in table 1 below.
Table 1 is containing the MES raw material charging time test of saltcake 10%, zeolite 15%
As can be seen from above-mentioned table 1, under the identical condition that feeds intake, the MES containing zeolite 15%, saltcake 10% of every jumbo bag 600Kg and the MES only containing 15% zeolite of every jumbo bag 600Kg, carries out liquidity costs contrast by the mode of Fig. 1.Charging time (mean value) is respectively 9.5 minutes and 17.8 minutes, illustrates that the MES mobility of the saltcake containing 10% is improved.
effect test example 2
The MES containing zeolite 15%, saltcake 15% of every jumbo bag 600Kg and the MES only containing 15% zeolite of every jumbo bag 600Kg, carry out liquidity costs contrast by the mode of Fig. 1, related data is as shown in table 2.
Table 2 is containing the MES raw material charging time test of saltcake 10%, zeolite 15%
As can be seen from Table 2, under the identical condition that feeds intake, the MES containing zeolite 15%, saltcake 15% of every jumbo bag 600Kg and the MES only containing 15% zeolite of every jumbo bag 600Kg, carries out liquidity costs contrast by the mode of Fig. 1.Charging time (mean value) is respectively 8.5 minutes and 17.7 minutes, illustrates that the MES mobility of the saltcake containing 15% is improved.
effect test example 3
The MES containing zeolite 10%, saltcake 12% of every jumbo bag 600Kg and the MES only containing 15% zeolite of every jumbo bag 600Kg, carry out liquidity costs contrast, related data is as shown in table 3.
Table 3 is containing the MES raw material charging time test of saltcake 12%, zeolite 10%
As can be seen from Table 3, under the identical condition that feeds intake, the MES containing zeolite 10%, saltcake 12% of every jumbo bag 600Kg and the MES only containing 15% zeolite of every jumbo bag 600Kg, carries out liquidity costs contrast by the mode of Fig. 1.Charging time (mean value) is respectively 9.2 minutes and 18 minutes, illustrates that the MES mobility of the saltcake containing 12% is improved.
The above, it is only preferred embodiment of the present invention, not any pro forma restriction is done to the present invention, therefore everyly do not depart from technical solution of the present invention content, the any simple modification done above embodiment according to technical spirit of the present invention, equivalent variations and modification, all still belong in the scope of technical solution of the present invention.
Claims (9)
1. the powdery of good fluidity is containing a production method for MES composition, it is characterized in that comprising the following steps:
1), after methyl sodiosul foaliphatate (MES) raw material or the MES raw material that is mixed with zeolite materials being ground, respectively by electronic scales metering, the saltcake raw material of powdery is also measured by electronic scales;
2) above-mentioned two or three raw material joins in impeller respectively continuously, in impeller, mix discharging continuously, is mixed with containing the powdery MES composition of certain proportion containing saltcake.
2. the powdery of good fluidity according to claim 1 is containing the production method of MES composition, it is characterized in that: step 1) in, the consumption of described methyl sodiosul foaliphatate (MES) raw material is 70-95 weight part; The consumption of described zeolite materials is 0-30 weight part; The consumption of powdery saltcake raw material is 10-30 weight part.
3. the powdery of good fluidity according to claim 2 is containing the production method of MES composition, it is characterized in that: step 1) in, the raw material dosage of described methyl sodiosul foaliphatate (MES) is 75-80 weight part; The consumption of described zeolite materials is 5-25 weight part; The consumption of described powdery saltcake is 10-15 weight part.
4. the powdery of good fluidity according to claim 1 contains the production method of MES composition, it is characterized in that: methyl sodiosul foaliphatate (MES) is ground rear weighing, with powdery zeolite materials and saltcake raw material mixing, be mixed with the MES feedstock composition containing certain proportion saltcake.
5. the powdery of good fluidity according to claim 4 is containing the production method of MES composition, it is characterized in that: described MES raw material is powdery; Described saltcake sodium sulfate raw material is powdery; The ratio of saltcake raw material in MES mixing raw material is no more than 30%, is preferably 10%-20%.
6. the powdery of good fluidity is containing a production unit for MES composition, it is characterized in that it comprises:
The multiple raw material feed bins connected successively, the upper end of each raw material feed bin is connected with jumbo bag lifting gear; The lower end of each raw material feed bin is connected with measuring apparatus;
Be arranged on the raw material travelling belt of multiple measuring apparatus lower end, for the multiple raw materials after conveying and metering;
Impeller, the exit end of the corresponding above-mentioned raw materials travelling belt of its opening end, for carrying out rotation mixing by the multiple raw materials after metering;
Compound travelling belt, the exit end of its entrance corresponding rotation mixing tank;
Fly-ash separator, is connected to impeller, for the production of the automatic dust removing of equipment.
7. the powdery of good fluidity according to claim 6 contains the production unit of MES composition, it is characterized in that: described raw material feed bin comprises: the first feed bin of splendid attire zeolite materials, the second feed bin of splendid attire saltcake raw material and splendid attire newly grind the 3rd feed bin of MES raw material.
8. the powdery of good fluidity according to claim 7 is containing the production unit of MES composition, it is characterized in that:
The lower end of described first feed bin is connected with the first weigher weighing zeolite materials; The lower end of described second feed bin is connected with the second weigher weighing saltcake raw material; The lower end of described 3rd feed bin is connected with the 3rd weigher that weighing newly grinds MES raw material.
9. the powdery of good fluidity according to claim 7 contains the production unit of MES composition, it is characterized in that: the upper end of described first feed bin is connected with the first lifter promoting zeolite materials, the upper end of described second feed bin is connected with the second lifter promoting saltcake raw material, and the upper end of described 3rd feed bin is connected with the 3rd lifter that lifting newly grinds MES raw material.
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| CN201510710728.8A CN105419956B (en) | 2015-10-27 | 2015-10-27 | A kind of production method and equipment of powdery composition containing MES of good fluidity |
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| CN201510710728.8A CN105419956B (en) | 2015-10-27 | 2015-10-27 | A kind of production method and equipment of powdery composition containing MES of good fluidity |
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| CN105419956A true CN105419956A (en) | 2016-03-23 |
| CN105419956B CN105419956B (en) | 2018-12-11 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107253924A (en) * | 2017-06-09 | 2017-10-17 | 常州大学 | A kind of preparation method of MES pulvis surfactant |
| CN107308882A (en) * | 2017-06-09 | 2017-11-03 | 常州大学 | A kind of preparation method of K12 pulvis surfactant |
| CN110668979A (en) * | 2019-10-15 | 2020-01-10 | 常州大学 | High-purification and powdering method for MES and K12 surfactants |
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| EP1043387A2 (en) * | 1999-03-27 | 2000-10-11 | Cognis Deutschland GmbH | Alkylbenzenesulfonate granulates |
| JP2008094942A (en) * | 2006-10-11 | 2008-04-24 | Lion Corp | Surface active agent composition |
| CN102051287A (en) * | 2010-12-31 | 2011-05-11 | 向红跃 | Method and equipment for preparing washing powder |
| CN102277238A (en) * | 2011-07-13 | 2011-12-14 | 杭州迪康生物技术有限公司 | Granular fatty acid methyl ester sulfonate (MES)-containing composite |
| CN102634425A (en) * | 2012-04-11 | 2012-08-15 | 广州立白企业集团有限公司 | Production technology and production equipment of concentrated detergent powder |
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2015
- 2015-10-27 CN CN201510710728.8A patent/CN105419956B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1043387A2 (en) * | 1999-03-27 | 2000-10-11 | Cognis Deutschland GmbH | Alkylbenzenesulfonate granulates |
| JP2008094942A (en) * | 2006-10-11 | 2008-04-24 | Lion Corp | Surface active agent composition |
| CN102051287A (en) * | 2010-12-31 | 2011-05-11 | 向红跃 | Method and equipment for preparing washing powder |
| CN102277238A (en) * | 2011-07-13 | 2011-12-14 | 杭州迪康生物技术有限公司 | Granular fatty acid methyl ester sulfonate (MES)-containing composite |
| CN102634425A (en) * | 2012-04-11 | 2012-08-15 | 广州立白企业集团有限公司 | Production technology and production equipment of concentrated detergent powder |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107253924A (en) * | 2017-06-09 | 2017-10-17 | 常州大学 | A kind of preparation method of MES pulvis surfactant |
| CN107308882A (en) * | 2017-06-09 | 2017-11-03 | 常州大学 | A kind of preparation method of K12 pulvis surfactant |
| CN107253924B (en) * | 2017-06-09 | 2019-11-12 | 常州大学 | A kind of preparation method of MES pulvis surfactant |
| CN110668979A (en) * | 2019-10-15 | 2020-01-10 | 常州大学 | High-purification and powdering method for MES and K12 surfactants |
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| CN105419956B (en) | 2018-12-11 |
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