CN105399294B - Oil sludge and sand recycling, harmless treatment process - Google Patents
Oil sludge and sand recycling, harmless treatment process Download PDFInfo
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- CN105399294B CN105399294B CN201610000094.1A CN201610000094A CN105399294B CN 105399294 B CN105399294 B CN 105399294B CN 201610000094 A CN201610000094 A CN 201610000094A CN 105399294 B CN105399294 B CN 105399294B
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- oil
- sand
- pipeline
- gas
- oil sludge
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/10—Treatment of sludge; Devices therefor by pyrolysis
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/12—Treatment of sludge; Devices therefor by de-watering, drying or thickening
- C02F11/16—Treatment of sludge; Devices therefor by de-watering, drying or thickening using drying or composting beds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/10—Nature of the water, waste water, sewage or sludge to be treated from quarries or from mining activities
Abstract
The present invention provides oil sludge and sand recycling, harmless treatment process, its technical solution is：Mainly by the first screw conveyor（1）, pulverizer（2）, rinse bath（3）, slush pump（4）, efficient solid-liquid separator（5）, the first gas bag（6）, the first Residual Oil Tank（7）, the first cooler（8）, air-introduced machine（9）, purifying column（10）, circulating pump（11）, cold water system（12）, water pump（13）, the second gas bag（14）, the second Residual Oil Tank（15）, the second cooler（16）, grease storage tank（17）, light oil tank（18）, the 3rd screw conveyor（19）, the second slag remover（20）, the second main transmission equipment（21）, pyrolysis oven（22）, charger（23）, the second screw conveyor（24）, the first slag remover（25）, the first main transmission equipment（26）, drying equipment（27）, Safety water seal（28）And combustion furnace（29）Form；Beneficial effects of the present invention：Oil sludge and sand process resource, innoxious processing requirement are reached, oil recovery rate is high, realizes serialization, quality stability.
Description
Technical field
The present invention relates to oil sludge and sand technical field, especially oil sludge and sand recycling, harmless treatment process.
Background technology
At present, oil sludge and sand processing solves also without a kind of good method, have can only harmless treatment, what is had can only provide
Sourceization recycle, the former the shortcomings that be that processing time is longer, occupied space is big, it is impossible to recycles the crude oil in sludge, be easy to cause two
Secondary pollution, is not suitable for handling on a large scale；The shortcomings that the latter is that processing cost is higher, and technological process is grown, there are secondary pollution,
Energy consumption is higher, and due to the easy coking of product in processing procedure, more demanding to equipment and materials, treating capacity is limited, process cycle
It is long, be not suitable for extensive processing.
The content of the invention
The purpose of the invention is to overcome the deficiencies of the prior art and provide can harmless treatment have can recycling recycling
The oil sludge and sand recycling that utilizes, harmless treatment process, its technical solution are：First screw conveyor connects pulverizer, rubs
Machine connects rinse bath, and road pipeline connects the first cooler and connects the second cooler by water pump on rinse bath, and Road pipeline leads to
Slush pump connection efficient solid-liquid separator, bottom line connection drying equipment are crossed, efficient solid-liquid separator connects grease storage tank, the
Road pipeline connects purifying column and cold water system respectively on one cooler, and the lower left pipeline of road direction connects combustion furnace by Safety water seal,
Pipeline connects the second cooler, bottom line connection light oil tank to the right, and overhead line connects the first gas bag, and the first gas bag is to the right
Pipeline connects the first Residual Oil Tank, and the drying equipment of pipeline connection to the left, purifying column pipeloop is equipped with circulating pump, cold water system top
Portion pipeline connects the second cooler, and lower road pipeline connects the second cooler by water pump, the second cooler pipeline connection to the left the
One cooler simultaneously connects combustion furnace, lower road pipeline connection light oil tank by Safety water seal, and overhead line connects the second gas bag, the
Pipeline connects the second Residual Oil Tank to two gas bags to the right, and the pyrolysis oven of pipeline connection to the left, pyrolysis oven one end is equipped with the second main transmission equipment,
The other end is equipped with charger, and lower section connects the second slag remover, and one side-lower of the second main transmission equipment is equipped with the 3rd screw conveyor,
Pipeline connection combustion furnace, two road pipeline connection drying equipments, drying equipment side are equipped with the first main transmission equipment to pyrolysis oven all the way,
Lower section connects the first slag remover, and one side-lower of slag remover is equipped with the second screw conveyor, and pipeline passes through all the way on drying equipment top
Air-introduced machine connects purifying column, and two road pipelines connect the first gas bag, and three-way connection (pipe) line connects efficient solid-liquid separator and rinse bath respectively.
The technique includes the following steps：
（One）, oil sludge and sand hot wash-separating treatment：Oil sludge and sand enters pulverizer by screw conveyor, and crushing large particle is solid
Body, subsequently into hot wash groove, adds basic agent, demulsifier, stirs 30min under mechanical action, make grease and solid particle
Separation, bulky grain gravel using gravitational settling remove, distributed slurry by slush pump pressurization enter efficiently separates equipment, make grease with
The isolated grease of solid phase, oil sludge and sand, grease further separate and recover oil, the oil recycling of wherein 30%-80%, oil sludge and sand after separation
Oil-containing 2-8%, aqueous 50%-70%；
（Two）, oil sludge and sand drying and processing：Oil-containing 2-8%, aqueous 50%-70% oil sludge and sands, are sent to drying by screw conveyor and set
The flue gas indirect heat exchange that standby and pyrolysis oven comes out, temperature be -150 DEG C of room temperature, after drying the moisture content of oil sludge and sand less than 30% into
Enter pyrolysis oven, the boil-off gas of drying equipment is by condensate recovery liquid phase oil, water, the oil recovery after water-oil separating, fixed gas
Body enters hot-blast stove by two-stage water seal and is utilized as fuel recovery, and flue gas removes pollutant SO2、NO2Qualified discharge；
（Three）, the oil sludge and sand after drying add pyrolysis catalysts, mass ratio 5%, enters heat by screw conveyor is closed
Stove, and 600-800 DEG C of the high-temperature gas indirect heat exchange that hot-blast stove comes are solved, pyrolysis temperature is 170 DEG C -600 DEG C, in oil sludge and sand
Organic matter, the distillation of petroleum-type light component enter gas phase, heavy constituent, asphalitine, wax are pyrolyzed as light component and high temperature carbonization,
Residue oil content is less than 0.3%, reaches agricultural sludge and uses standard, pyrolysis oven exhaust pass pneumatic transmission to drying equipment comprehensively utilizes；
（Four）, hot-blast stove fuel be diesel oil, one kind and process of oil recovery for being produced in natural gas, pyrolysis drying course
The on-condensible gas of middle recycling, produces high temperature hot gas by dedicated combustion apparatus and is used for pyrolysis, drying.
Brief description of the drawings
Fig. 1 is the structure diagram of present invention process.
Embodiment
As shown in Figure 1, oil sludge and sand recycling, harmless treatment process, mainly by the first screw conveyor 1, pulverizer 2,
It is rinse bath 3, slush pump 4, efficient solid-liquid separator 5, the first gas bag 6, the first Residual Oil Tank 7, the first cooler 8, air-introduced machine 9, net
Change tower 10, circulating pump 11, cold water system 12, water pump 13, the second gas bag 14, the second Residual Oil Tank 15, the second cooler 16, grease storage
Tank 17, light oil tank 18, the 3rd screw conveyor 19, the second slag remover 20, the second main transmission equipment 21, pyrolysis oven 22, charging
Machine 23, the second screw conveyor 24, the first slag remover 25, the first main transmission equipment 26, drying equipment 27, Safety water seal 28 and combustion
Stove 29 is burnt to form；First screw conveyor 1 connects pulverizer 2, and pulverizer 2 connects rinse bath 3, and road pipeline connects on rinse bath 3
First cooler 8 simultaneously connects the second cooler 16 by water pump 13, and Road pipeline connects efficient solid-liquid separator by slush pump 4
5, bottom line 27 efficient solid-liquid separator 5 of connection drying equipment connects grease storage tank 17, and road pipeline is distinguished on the first cooler 8
Purifying column 10 and cold water system 12 are connected, the lower left pipeline of road direction connects combustion furnace 29 by Safety water seal 28, and pipeline connects to the right
Second cooler 16, bottom line connection light oil tank 18, overhead line connect the first gas bag 6, and pipeline connects the first gas bag 6 to the right
The first Residual Oil Tank 7 is connect, the drying equipment 27 of pipeline connection to the left, 10 pipeloop of purifying column is equipped with circulating pump 11, cold water system
12 overhead lines connect the second cooler 16, lower road pipeline by water pump 13 connect the second cooler 16, the second cooler 16 to
Left pipeline connects the first cooler 8 and connects combustion furnace 29, lower road pipeline connection light oil tank 18, top by Safety water seal 28
Pipeline connects the second gas bag 14, and pipeline connects the second Residual Oil Tank 15 to the second gas bag 14 to the right, the pyrolysis oven 22 of pipeline connection to the left, heat
22 one end of solution stove is equipped with the second main transmission equipment 21, and the other end is equipped with charger 23, and lower section connects the second slag remover 20, the second master
21 1 side-lower of drive apparatus is equipped with the 3rd screw conveyor 19,22 1 road pipeline connection combustion furnace 29 of pyrolysis oven, two road pipelines
Drying equipment 27 is connected, 27 side of drying equipment is equipped with the first main transmission equipment 26, and lower section connects the first slag remover 25, slag remover
25 1 side-lowers are equipped with the second screw conveyor 24, and pipeline connects purifying column 10 by air-introduced machine 9 all the way on drying equipment 27 top,
Two road pipelines connect the first gas bag 6, and three-way connection (pipe) line connects efficient solid-liquid separator 5 and rinse bath 3 respectively.
The application method of the present invention
（One）, oil sludge and sand hot wash-separating treatment：Oil sludge and sand enters pulverizer by screw conveyor, and crushing large particle is solid
Body, subsequently into hot wash groove, adds basic agent, demulsifier, stirs 30min under mechanical action, make grease and solid particle
Separation, bulky grain gravel using gravitational settling remove, distributed slurry by slush pump pressurization enter efficiently separates equipment, make grease with
The isolated grease of solid phase, oil sludge and sand, grease further separate and recover oil, the oil recycling of wherein 30%-80%, oil sludge and sand after separation
Oil-containing 2-8%, aqueous 50%-70%；
（Two）, oil sludge and sand drying and processing：Oil-containing 2-8%, aqueous 50%-70% oil sludge and sands, are sent to drying by screw conveyor and set
The flue gas indirect heat exchange that standby and pyrolysis oven comes out, temperature be -150 DEG C of room temperature, after drying the moisture content of oil sludge and sand less than 30% into
Enter pyrolysis oven, the boil-off gas of drying equipment is by condensate recovery liquid phase oil, water, the oil recovery after water-oil separating, fixed gas
Body enters hot-blast stove by two-stage water seal and is utilized as fuel recovery, and flue gas removes pollutant SO2、NO2Qualified discharge；
（Three）, the oil sludge and sand after drying add pyrolysis catalysts, mass ratio 5%, enters heat by screw conveyor is closed
Stove, and 600-800 DEG C of the high-temperature gas indirect heat exchange that hot-blast stove comes are solved, pyrolysis temperature is 170 DEG C -600 DEG C, in oil sludge and sand
Organic matter, the distillation of petroleum-type light component enter gas phase, heavy constituent, asphalitine, wax are pyrolyzed as light component and high temperature carbonization,
Residue oil content is less than 0.3%, reaches agricultural sludge and uses standard, pyrolysis oven exhaust pass pneumatic transmission to drying equipment comprehensively utilizes；
（Four）, hot-blast stove fuel be diesel oil, one kind and process of oil recovery for being produced in natural gas, pyrolysis drying course
The on-condensible gas of middle recycling, produces high temperature hot gas by dedicated combustion apparatus and is used for pyrolysis, drying.
According to above-mentioned technique, complete to produce daily 1 ton of oil sludge and sand and handle, before processing oil sludge and sand oil content 26%, moisture content 47%,
Solid contents 27%.∕ tons of sodium oxide molybdena 17kg, ∕ tons of polyacrylamide 0.5kg are hydrogenated with processing procedure.It is residual through over cleaning, pyrolysis
Slag oil content 0.12%, detects Waste gas outlet in processing procedure, and pollutant is not exceeded, and waste water recycles, without outer row.
Claims (2)
1. oil sludge and sand recycling, harmless treatment process, it is characterised in that：First screw conveyor（1）Connect pulverizer（2）,
Pulverizer（2）Connect rinse bath（3）, rinse bath（3）Upper road pipeline connects the first cooler（8）And pass through water pump（13）Connection the
Two coolers（16）, Road pipeline passes through slush pump（4）Connect efficient solid-liquid separator（5）, bottom line connection charger
（23）, efficient solid-liquid separator（5）Connect grease storage tank（17）, the first cooler（8）Upper road pipeline connects purifying column respectively
（10）With cold water system（12）, the lower left pipeline of road direction passes through Safety water seal（28）Connect combustion furnace（29）, pipeline connection to the right the
Two coolers（16）, bottom line connection light oil tank（18）, overhead line the first gas bag of connection（6）, the first gas bag（6）To the right
Pipeline connects the first Residual Oil Tank（7）, the drying equipment of pipeline connection to the left（27）, purifying column（10）Pipeloop is equipped with circulating pump
（11）, cold water system（12）Overhead line connects the second cooler（16）, lower road pipeline passes through water pump（13）The cooling of connection second
Device（16）, the second cooler（16）Pipeline connects the first cooler to the left（8）And pass through Safety water seal（28）Connect combustion furnace
（29）, lower road pipeline connection light oil tank（18）, overhead line the second gas bag of connection（14）, the second gas bag（14）Pipeline connects to the right
Connect the second Residual Oil Tank（15）, the pyrolysis oven of pipeline connection to the left（22）, pyrolysis oven（22）One end is equipped with the second main transmission equipment（21）,
The other end is equipped with charger（23）, lower section connects the second slag remover（20）, the second main transmission equipment（21）One side-lower is equipped with the
Three screw conveyors（19）, pyrolysis oven（22）Pipeline connection combustion furnace all the way（29）, two road pipeline connection drying equipments（27）, dry
Dry equipment（27）Side is equipped with the first main transmission equipment（26）, lower section connects the first slag remover（25）, slag remover（25）Under side
Side is equipped with the second screw conveyor（24）, drying equipment（27）Pipeline passes through air-introduced machine all the way on top（9）Connect purifying column（10）,
Two road pipelines connect the first gas bag（6）, three-way connection (pipe) line connects efficient solid-liquid separator respectively（5）And rinse bath（3）.
2. oil sludge and sand recycling according to claim 1, harmless treatment process, it is characterised in that：The technique is included such as
Lower step：
（One）, oil sludge and sand hot wash-separating treatment：Oil sludge and sand enters pulverizer by screw conveyor, crushing large particle solid, so
Enter hot wash groove afterwards, add basic agent, demulsifier, stir 30min under mechanical action, separate grease and solid particle,
Bulky grain gravel is removed using gravitational settling, and distributed slurry is entered by slush pump pressurization efficiently separates equipment, makes grease and solid phase
Isolated grease, oil sludge and sand, grease further separate and recover oil, the oil recycling of wherein 30%-80%, oil sludge and sand oil-containing after separation
2-8%, aqueous 50%-70%；
（Two）, oil sludge and sand drying and processing：Oil-containing 2-8%, aqueous 50%-70% oil sludge and sands, sent by screw conveyor to drying equipment and
The flue gas indirect heat exchange that pyrolysis oven comes out, temperature is -150 DEG C of room temperature, and the moisture content of oil sludge and sand is less than 30% and enters heat after drying
Stove is solved, mutually oil, water, the oil recovery after water-oil separating, on-condensible gas pass through the boil-off gas of drying equipment by condensate recovery liquid
Cross two-stage water seal to utilize as fuel recovery into hot-blast stove, flue gas removes pollutant SO2、NO2Qualified discharge；
（Three）, the oil sludge and sand after drying add pyrolysis catalysts, ratio 5%, enters pyrolysis oven by screw conveyor is closed,
The high-temperature gas indirect heat exchange of 600-800 DEG C to come with hot-blast stove, pyrolysis temperature are 170 DEG C -600 DEG C, having in oil sludge and sand
Machine matter, the distillation of petroleum-type light component enter gas phase, and heavy constituent, asphalitine, wax are pyrolyzed as light component and high temperature carbonization, residue
Oil content is less than 0.3%, reaches agricultural sludge and uses standard, pyrolysis oven exhaust pass pneumatic transmission to drying equipment comprehensively utilizes；
（Four）, hot-blast stove fuel be diesel oil, one kind of oil recovery for being produced in natural gas, pyrolysis drying course and during return
The on-condensible gas of receipts, produces high temperature hot gas by dedicated combustion apparatus and is used for pyrolysis, drying.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610000094.1A CN105399294B (en) | 2016-01-01 | 2016-01-01 | Oil sludge and sand recycling, harmless treatment process |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610000094.1A CN105399294B (en) | 2016-01-01 | 2016-01-01 | Oil sludge and sand recycling, harmless treatment process |
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| CN105399294A CN105399294A (en) | 2016-03-16 |
| CN105399294B true CN105399294B (en) | 2018-05-01 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107098559A (en) * | 2017-06-16 | 2017-08-29 | 南京塔川化工设备有限公司 | A kind of oily sludge is from heat supply Non-oxygen pyrolytic equipment and its method for pyrolysis |
| CN108383350A (en) * | 2018-04-02 | 2018-08-10 | 大庆高新区百世环保科技开发有限公司 | A kind of ultra-clean treatment process of oily sludge object and equipment |
| CN108531207A (en) * | 2018-06-19 | 2018-09-14 | 大庆高新区百世环保科技开发有限公司 | A kind of oily sludge substance treating method and its device using conduction oil indirectly heat |
| CN108795464B (en) * | 2018-06-19 | 2024-03-19 | 大庆高新区百世环保科技开发有限公司 | Desorption treatment method and device using flue gas indirect heating |
| CN108467742B (en) * | 2018-06-19 | 2024-03-15 | 大庆高新区百世环保科技开发有限公司 | Sand desorption treatment method and device by utilizing flue gas indirect heating |
| CN109095743A (en) * | 2018-08-24 | 2018-12-28 | 郑州高路亚环保科技有限公司 | The overcritical organic stripping system of one kind and its technique |
| CN110482836A (en) * | 2019-04-27 | 2019-11-22 | 南京河海环境研究院有限公司 | A kind of oily sludge recycling and method for innocent treatment based on anaerobism thermal desorption |
| CN110054388A (en) * | 2019-05-24 | 2019-07-26 | 河南省四达仙龙实业有限公司 | A kind of device that greasy filth harmless treatment utilizes |
| CN110550846A (en) * | 2019-09-18 | 2019-12-10 | 纪禹操 | Oily sludge harmless treatment process and equipment |
| CN114933400B (en) * | 2022-05-11 | 2023-05-05 | 国家石油天然气管网集团有限公司 | Harmless treatment device for oil sludge |
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| JP3646925B2 (en) * | 2000-07-31 | 2005-05-11 | 株式会社荏原製作所 | Organic wastewater treatment method and treatment apparatus |
| CN104341081B (en) * | 2013-07-30 | 2016-08-17 | 麦王环境技术股份有限公司 | Greasy filth separates and the method for innocent treatment reclaimed |
| CN104261649B (en) * | 2014-09-28 | 2016-04-27 | 东南大学 | A kind of high-efficiency oil sludge pyrolysis oil preparation method and system |
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Address after: 257061, No. two, 271 North Road, Shandong, Dongying (inner exploration Hall of Petroleum University) Applicant after: Shandong top Environment Technology Co., Ltd. Address before: 257061, No. two, 271 North Road, Shandong, Dongying (inner exploration Hall of Petroleum University) Applicant before: Shandong Top Petroleum Equipment Co., Ltd. |
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Inventor after: Li Jianhua Inventor after: Shen Fei Inventor after: Wu Baohua Inventor after: Wang Xihui Inventor before: Li Jianhua Inventor before: Shen Fei Inventor before: Chen Shujun Inventor before: Wu Baohua Inventor before: Jin Zhanxin Inventor before: Wang Xihui |
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