CN105372382A - High temperature crucible single-mode static cooling parallel device - Google Patents
High temperature crucible single-mode static cooling parallel device Download PDFInfo
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- CN105372382A CN105372382A CN201510677487.1A CN201510677487A CN105372382A CN 105372382 A CN105372382 A CN 105372382A CN 201510677487 A CN201510677487 A CN 201510677487A CN 105372382 A CN105372382 A CN 105372382A
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- high temperature
- containers
- temperature crucibles
- cooled containers
- cooling
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Abstract
The invention discloses a high temperature crucible single-mode static cooling parallel device, which belongs to the field of sulphur content analytical equipment in bituminous coal combustible materials, and comprises a composite pallet, four cooling containers with same structures and block-structured solid ices, wherein composite pallet comprises support columns, four positioning holes and an overflow port, the four container positioning holes are respectively axially symmetrically arranged, the diameter of the overflow port is 5mm, the cooling containers are cylindrical containers, the wall thicknesses of the cylindrical containers are 2mm, the heights of the cylindrical containers are slightly higher than two third heights of high temperature crucibles, the inner diameters of the cylindrical containers are bigger than the outer diameter of the high temperature crucibles 5mm, the cooling containers are arranged in the container positioning holes of the composite pallet, the high temperature crucibles are arranged in the cooling containers, and a large number of block-structured solid ices are arranged in gaps which are arranged between the outer wall of the high temperature crucible and the inner walls of the cooling containers. The high temperature crucible single-mode static cooling parallel device is simple in structure, and uses the block-structured solid ices to cool and cools the high temperature crucibles at the same time.
Description
Technical field
The present invention is mainly concerned with the analytical equipment field of sulfur content in bituminous coal combustible, refers in particular to the static cooling LPT device of a kind of high-temperature crucibles single-mode.
Background technology
Element sulphur is topmost oxious component in coal sample, and it not only brings injurious effects to the coking of coal, gasification, burning, also can cause atmospheric pollution after burning.Therefore, the content measuring element sulphur in coal is a very important job.Emhorn surveys sulphur method, as one of the standard method of the general mensuration full content of Sulphur in coal content in current various countries, has that accuracy is high, the advantage such as mensuration in batch.But it is complicated that Emhorn surveys sulphur process, is difficult to realize whole-course automation, therefore it is lower to measure efficiency.Survey in sulphur at Emhorn, a critical step cools the high-temperature crucibles of taking out in comburant, blends the calcination thing in crucible after cooling with glass bar, makes solution.In prior art, be nearly all self-heating cooling to the cooling of high-temperature crucibles.The cooling of prior art has certain defect: cool time is longer, and cooling effectiveness is lower, thus causes the experimental period measuring sulphur very long.Therefore, design and a kind ofly the equipment of cooling down high-temperature crucible fast can have important value.
Summary of the invention
The technical matters that the present invention need solve is: the technical matterss such as cool time is longer existed for prior art, the invention provides a kind of structure simple, adopt solid ice cooling, the static cooling LPT device of high-temperature crucibles single-mode of simultaneously multiple high-temperature crucibles being implemented to cooling.
In order to solve the problem, the solution that the present invention proposes is: the static cooling LPT device of a kind of high-temperature crucibles single-mode, and it comprises the solid ice of the identical cooled containers of combination pallet, four structures and block structure; Described combination pallet comprises pillar, four rotational symmetry are divided other container pilot hole, are arranged at the diameter of described container pilot hole base plate center up/down perforation is the gap of 5mm; Described container pilot hole is diameter equals described cooled containers external diameter, the degree of depth is cooled containers height described in 1/10th circular hole; Described cooled containers is wall thickness is 2mm, highly a little more than high-temperature crucibles 2/3rds height, and the cylindrical container of internal diameter 5mm larger than the external diameter of described high-temperature crucibles.
Described cooled containers is positioned in the container pilot hole of described combination pallet, and described high-temperature crucibles is positioned in described cooled containers; A large amount of, block solid ice is equiped with in gap between the outer wall of described high-temperature crucibles and the inwall of described cooled containers; In described high-temperature crucibles, comburant is housed; The place of bottom centre of described cooled containers is provided with the circular outlets that a diameter is 4mm up/down perforation.
Compared with prior art, tool has the following advantages and beneficial effect in the present invention:
(1) the static cooling LPT device of a kind of high-temperature crucibles single-mode of the present invention is provided with 4 cooled containers, be equiped with the solid ice of a large amount of bulks between the inwall of cooled containers and the outer wall of high-temperature crucibles, implement the fast cooling to high-temperature crucibles by the contact of solid ice and high-temperature crucibles.
(2) structure of the present invention simple, adopt solid ice pattern to implement cooling to high-temperature crucibles, shorten cool time, improve cooling effectiveness.
Accompanying drawing explanation
Fig. 1 is the structural front view of the static cooling LPT device of a kind of high-temperature crucibles single-mode of the present invention.
Fig. 2 is plane figure's schematic diagram of container pilot hole on combination pallet of the present invention and gap.
In figure, 1-high-temperature crucibles; 10-comburant; 2-solid ice; 3-cooled containers; 31-water delivering orifice; 4-combination pallet; 41-container pilot hole; 42-gap; 43-pillar.
Embodiment
Below with reference to the drawings and specific embodiments, the present invention is described in further detail.
Shown in Fig. 1 and Fig. 2, the static cooling LPT device of a kind of high-temperature crucibles single-mode of the present invention, comprises the solid ice 2 of combination pallet 4, four cooled containers that structure is identical 3 and block structure; Combination pallet 4 comprises pillar 43, four rotational symmetry and divides other container pilot hole 41, is arranged at the gap 42 that the diameter of container pilot hole 41 base plate center up/down perforation is 5mm; Container pilot hole 41 for diameter equal cooled containers 3 external diameter, the degree of depth be 1/10th cooled containers 3 height circular holes.
Shown in Fig. 1 and Fig. 2, cooled containers 3 for wall thickness be 2mm, height a little more than high-temperature crucibles 2/1sts three height, the cylindrical container of internal diameter 5mm larger than the external diameter of high-temperature crucibles 1; Cooled containers 3 is positioned in the container pilot hole 41 of combination pallet 4, and high-temperature crucibles 1 is positioned in cooled containers 3; A large amount of, block solid ice 2 is equiped with in gap between the outer wall of high-temperature crucibles 1 and the inwall of cooled containers 3; Comburant 10 is housed in high-temperature crucibles 1; The place of bottom centre of cooled containers 3 is provided with the circular outlets 31 that a diameter is 4mm up/down perforation.
Cooling principle: high-temperature crucibles 1 is installed in cooled containers 3; The solid ice 2 of a large amount of bulks is filled with in gap between the inwall of cooled containers 3 and the outer wall of high-temperature crucibles 1; Solid ice 2, by the contact with high-temperature crucibles 1, absorbs a large amount of heats, and the water of generating portion, flowed out by water delivering orifice 31 and gap 42; After the heat of high-temperature crucibles 1 is absorbed by solid ice 2, its temperature declines rapidly, thus completes the cooling to high-temperature crucibles 1.
Claims (1)
1. the static cooling LPT device of high-temperature crucibles single-mode, is characterized in that: the solid ice (2) comprising the identical cooled containers (3) of combination pallet (4), four structures and block structure; Described combination pallet (4) comprises pillar (43), four rotational symmetry are divided other container pilot hole (41), are arranged at the gap (42) that the diameter of described container pilot hole (41) base plate center up/down perforation is 5mm; Described container pilot hole (41) for diameter equal described cooled containers (3) external diameter, the degree of depth be cooled containers described in 1/10th (3) height circular hole; Described cooled containers (3) for wall thickness be 2mm, height a little more than high-temperature crucibles (1) 2/3rds height, the cylindrical container of internal diameter 5mm larger than the external diameter of described high-temperature crucibles (1); Described cooled containers (3) is positioned in the container pilot hole (41) of described combination pallet (4), and described high-temperature crucibles (1) is positioned in described cooled containers (3); A large amount of, block solid ice (2) is equiped with in gap between the outer wall of described high-temperature crucibles (1) and the inwall of described cooled containers (3); Comburant (10) is housed in described high-temperature crucibles (1); The place of bottom centre of described cooled containers (3) is provided with the circular outlets (31) that a diameter is 4mm up/down perforation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510677487.1A CN105372382A (en) | 2015-10-19 | 2015-10-19 | High temperature crucible single-mode static cooling parallel device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510677487.1A CN105372382A (en) | 2015-10-19 | 2015-10-19 | High temperature crucible single-mode static cooling parallel device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105372382A true CN105372382A (en) | 2016-03-02 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201510677487.1A Pending CN105372382A (en) | 2015-10-19 | 2015-10-19 | High temperature crucible single-mode static cooling parallel device |
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2853046B2 (en) * | 1989-06-21 | 1999-02-03 | 日新製鋼株式会社 | Ultra fine powder production equipment |
| CN201440034U (en) * | 2009-07-09 | 2010-04-21 | 北京合非大道科技有限公司 | Fountain type cooling water circulation cold crucible |
| WO2011054086A1 (en) * | 2009-11-03 | 2011-05-12 | 7685297 Canada Inc. | Systems and methods for preparing samples for chemical analysis |
| CN204111568U (en) * | 2014-08-11 | 2015-01-21 | 南通晶鑫光学玻璃有限公司 | A kind of opticglass smelting pot device |
| CN204294252U (en) * | 2014-10-23 | 2015-04-29 | 齐齐哈尔大学 | A kind of use for laboratory is in the ice bath device of low-temp reaction |
| CN204323882U (en) * | 2014-12-10 | 2015-05-13 | 南京信息工程大学 | A kind of Muffle furnace dedicated ceramic pallet |
| CN204550691U (en) * | 2015-04-20 | 2015-08-12 | 山东海源光电科技有限公司 | Cooling crucible device |
-
2015
- 2015-10-19 CN CN201510677487.1A patent/CN105372382A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2853046B2 (en) * | 1989-06-21 | 1999-02-03 | 日新製鋼株式会社 | Ultra fine powder production equipment |
| CN201440034U (en) * | 2009-07-09 | 2010-04-21 | 北京合非大道科技有限公司 | Fountain type cooling water circulation cold crucible |
| WO2011054086A1 (en) * | 2009-11-03 | 2011-05-12 | 7685297 Canada Inc. | Systems and methods for preparing samples for chemical analysis |
| CN204111568U (en) * | 2014-08-11 | 2015-01-21 | 南通晶鑫光学玻璃有限公司 | A kind of opticglass smelting pot device |
| CN204294252U (en) * | 2014-10-23 | 2015-04-29 | 齐齐哈尔大学 | A kind of use for laboratory is in the ice bath device of low-temp reaction |
| CN204323882U (en) * | 2014-12-10 | 2015-05-13 | 南京信息工程大学 | A kind of Muffle furnace dedicated ceramic pallet |
| CN204550691U (en) * | 2015-04-20 | 2015-08-12 | 山东海源光电科技有限公司 | Cooling crucible device |
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Application publication date: 20160302 |