CN105366792B - The preparation method of high-oxygen water, biocompatibility constituent and high-oxygen water containing high-oxygen water - Google Patents
The preparation method of high-oxygen water, biocompatibility constituent and high-oxygen water containing high-oxygen water Download PDFInfo
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Abstract
The present invention provides a kind of high-oxygen water, including water and oxygen, wherein：The oxygen content of the high-oxygen water is no less than 20ppm；And by the initial oxygen content of the high-oxygen water be 100% in terms of, by the high-oxygen water stand 30 minutes after oxygen content percentage (A) and by the high-oxygen water stand 180 minutes after oxygen content percentage (B) the two between difference (A B) be less than 24%.In addition, the present invention also provides the preparation method of biocompatibility constituent and high-oxygen water containing high-oxygen water.
Description
Technical field
The present invention relates to a kind of high-oxygen waters, more particularly to a kind of metastable high-oxygen water of oxygen content.In addition, of the invention
The preparation method of a kind of biocompatibility constituent containing aforementioned high-oxygen water and aforementioned high-oxygen water is also provided.
Background technology
High-oxygen water refers to a kind of drinking water that active oxygen is added on the basis of pure water, and industry is not to high-oxygen water at present
Oxygen content have a unified definition, but in general, often the water by oxygen content more than or equal to 20ppm is known as high-oxygen water.
According to statistics, hundreds of manufacturer's manufactures are had more than at present or sale high-oxygen water, target focus principally on health,
It is expected that user is by the way that long-term drinking high-oxygen water reaches health care the effect of.
However, the high-oxygen water of market today haves the shortcomings that stability is bad, causes often to there is public opinion to criticize and negate height
The effect of oxygen water.One of which comment thinks that high-oxygen water can not remain high under the conditions of body temperature and contain oxygen condition, so that high
Dissolved oxygen in oxygen water can be fast released and be unable to reach the effect of declared in gaseous form in vivo.
In this regard, Yin Zhaoxue et al. exists《Capital University of Medical Sciences's journal》The paper that the 6th phase of volume 28 in December, 2007 is delivered
In " preparation, stability and its influence to mouse blood toxicity of heavy-oxygen-enriched water ", has studied the volume of water body, whether leads in advance
Influence caused by gas, the oxygen content of the factors for obtained heavy-oxygen-enriched water such as whether pressurize, this research is thought, is passed through oxygen in advance
Heavy-oxygen-enriched water oxygen content obtained of pressurizeing after gas is relatively high, and points out under different condition reduction of speed under the oxygen content of heavy-oxygen-enriched water obtained
It is little to spend difference.
However, do not suggest that how to be made further improvements in technique in this document, with produce can be for a long time
And/or the high-oxygen water with high stability under relatively-high temperature (such as higher than 30 DEG C).
Invention content
In view of it is met in prior art the problem of, the present invention discloses a kind of high-oxygen water, the bio-compatible containing high-oxygen water
The preparation method of property constituent and high-oxygen water, wherein the oxygen content of the high-oxygen water is as the variable quantity of time is smaller and stability
It is higher.In addition, even if by the high-oxygen water of the present invention be placed in it is more harsh under conditions of (such as high temperature), can still have higher molten
Oxygen value (such as higher than 20ppm or higher than 25ppm) is solved, and by can still maintain relatively high oxygen content after a certain period of time.
In one embodiment, the present invention provides a kind of high-oxygen water, including water and oxygen, wherein：The high-oxygen water it is oxygen-containing
Amount is no less than 20ppm；And by the initial oxygen content of the high-oxygen water be 100% in terms of, by the high-oxygen water stand 30 minutes after
Oxygen content percentage (A) and by the high-oxygen water stand 180 minutes after oxygen content percentage (B) the two between difference (A-
B) it is less than 24%.
In a preferred embodiment, aforementioned differences (A-B) are less than 20%, preferably smaller than 15%, for example, between 5% and
Between 20%.
In a preferred embodiment, the oxygen content of high-oxygen water is no less than 25ppm, for example, between 20ppm and 50ppm it
Between.In addition, in another preferred embodiment, for high-oxygen water after standing 180 minutes, oxygen content is still no less than 25ppm.
The present invention also provides a kind of high-oxygen water above-mentioned, wherein the oxygen content be the high-oxygen water at 0 DEG C to 40 DEG C
It is measured under state, such as oxygen content is that the high-oxygen water is measured from the state of 0 DEG C to 12 DEG C, it is preferably described oxygen-containing
Amount is that the high-oxygen water is measured from the state of 4 DEG C to 8 DEG C (such as 6 DEG C).
In a preferred embodiment, by the high-oxygen water from after 10 DEG C are heated to 40 DEG C, oxygen content variation is less than 20%,
Preferably smaller than 10%.
In a preferred embodiment, by the high-oxygen water from after 10 DEG C are heated to 40 DEG C, oxygen content is no less than 25ppm,
Preferably no less than 30ppm.
In a preferred embodiment, after high-oxygen water maintains 120 minutes under conditions of 30 DEG C to 40 DEG C, oxygen content variation
Less than 30%, preferably smaller than 25%.
In a preferred embodiment, after high-oxygen water maintains 120 minutes under conditions of 30 DEG C to 40 DEG C, oxygen content is many
In 20ppm, preferably no less than 25ppm.
In a preferred embodiment, aforementioned high-oxygen water can be maintained under conditions of 30 DEG C to 40 DEG C rich oxygen content (such as
No less than 20ppm, no less than 25ppm or no less than 30ppm) it is at least up to 60 minutes.
In a preferred embodiment, aforementioned high-oxygen water under conditions of about 37 DEG C (such as 35 DEG C to 39 DEG C) can remain high
Oxygen content (such as no less than 20ppm, no less than 25ppm or no less than 30ppm) is at least up to 60 minutes, 90 minutes or 120 minutes.
In a preferred embodiment, aforementioned high-oxygen water can keep oxygen content to be no less than under conditions of higher than 40 DEG C
25ppm。
In a preferred embodiment, the initial temperature by the high-oxygen water from 5 DEG C to 10 DEG C is heated to 40 DEG C to 50 DEG C
Temperature after, oxygen content variation be less than 20%, be, for example, less than 15%.
In a preferred embodiment, during the high-oxygen water being heated to 50 DEG C from 5 DEG C to 10 DEG C of initial temperature,
Oxygen content keeps no less than 30ppm.
In one embodiment, high-oxygen water of the invention only contains water, oxygen and non-artificial adding ingredient.
The present invention also provides a kind of biocompatibility constituent, and it includes aforementioned high-oxygen water and at least one bio-compatibles
Property ingredient.
For example, aforementioned biological compatibility constituent can be medical component, cosmetic composition or beverage composition,
And the biocompatible component can be intravenous nutrition element, drug, cosmetic additive agent or food additives etc. respectively.
The present invention also provides a kind of preparation method of high-oxygen water, includes the steps that being supplied oxygen to a water body, feature exists
In：During oxygen supply, under conditions of the water body is maintained 0 DEG C to 12 DEG C, with the flow of 50cc/min to 1000cc/min
To the water body, oxygen supply time is no less than 30 minutes oxygen without interruption.
In one embodiment, during oxygen supply, under conditions of the water body is maintained 4 DEG C to 8 DEG C, such as 6 DEG C.
In one embodiment, the volume of aforementioned water body is between 1 liter and 15 liters and/or oxygen supply time is many
In 180 minutes, for example, about 210 minutes.
In one embodiment, it during oxygen supply, is first supplied oxygen with first flow, until the oxygen content of water body reaches
20ppm is between 25ppm, then, then is supplied oxygen with second flow, wherein second flow is less than or equal to first flow.It lifts
For example, first flow is not less than 50cc/min, and second flow is not more than 1000cc/min.
The present invention also provides a kind of high-oxygen water that preceding method is prepared.
Specific implementation mode
To make those skilled in the art can be appreciated that the features of the present invention and effect, below only with regard to specification and claims
In the term that refers to and term carry out general explanation and definition.Unless otherwise specified, otherwise all technologies used herein
And scientific words, the ordinary meaning all understood for the present invention with those skilled in the art, when there is collision scenario,
It should be subject to the definition of this specification.
First, herein certain parts be utilize " one ", "an", "one" or it is of the present invention to describe similar to term
Ingredient and technical characteristic, such description is intended merely to facilitate expression, and provides general meaning to the technical characteristic of the present invention.
Therefore, unless otherwise specified, otherwise such description is understood to include one or at least one, and odd number is also simultaneously including multiple
Number.
Herein, term "comprising", " comprising ", " having ", " containing " or other any similar terms belong to open
Property conjunction (open-ended transitional phrase), be intended to cover nonexcludability include object.For example,
A constituent or product containing plural element are not limited in these elements listed herein, but may also include not
Be expressly recited but the usually intrinsic other element of the constituent or product.In addition to this, it says unless the contrary is explicitly
Bright, otherwise term "or" refers to the "or" of including property, without referring to exclusive "or".For example, following any type situation is equal
Meet condition " A or B "：A is true (or presence) and B be pseudo- (or being not present), A be pseudo- (or being not present) and B be very (or presence),
A and B is true (or presence).In addition, herein, the deciphering of term "comprising", " comprising ", " having ", " containing " should be regarded as
It is specifically open and cover simultaneously " by ... formed " and closed or semi-enclosed conjunction such as " substantially by ... formed ".
Herein, the parameters such as the concentration of temperature, flow, numerical value, quantity or various composition, content are usually with numberical range
Or the form of percentage range indicates, but should give special heed to, it is all to be defined in the form of numberical range or percentage range
Feature or condition are merely to succinctly and conveniently.Accordingly, the description of numberical range or percentage range should be regarded as having covered and have
Body discloses the individual number in all possible underrange and range, especially integer numerical value.For example, the range of " 1 to 8 "
Description should be regarded as specifically disclosing such as 1 to 7,2 to 8,2 to 6,3 to 6,4 to 8,3 to 8 all underranges, especially by whole
The underrange that is defined of number numerical value, and should be regarded as such as 1 in specific the open scope, 2,3,4,5,6,7,8 individual numbers.It removes
Non- otherwise indicated, otherwise foregoing explanation method is suitable for all the elements of full text of the present invention, no matter whether in extensive range.
If quantity, concentration or other numerical value or parameter are indicated with range, preferred scope or a series of upper limits and lower limit,
Its should be understood as specifically disclosed herein by the lower limit of any upper limit to the range or preferred value and the range or
All ranges that preferred value is constituted, disclose respectively no matter whether these ranges have.If in addition, mentioning the range of numerical value herein
When, unless otherwise stated, the range should include its endpoint and all integers in range and score.
Herein, under the premise of may achieve goal of the invention, numerical value should be understood to have the numerical value number of significant digit
Accuracy.For example, number 40.0 then should be understood to cover the range from 39.50 to 40.49.
Herein, for using Ma Kushi group (Markush group) or option formula term to describe spy of the invention
Sign or example situation, it will be understood by a person skilled in the art that in Ma Kushi group or option list secondary group of all members or times
What individual member also can be used for describing the present invention.For example, if X is described as " selected from by X1、X2And X3The group formed ",
Also indicate that it is X that X, which is fully described out,1Opinion and X be X1And/or X2Opinion.Furthermore for use Ma Kushi group or
Option formula term is to describe feature or the example person of the present invention, it will be understood by a person skilled in the art that Ma Kushi group or option list
The secondary group of interior all members or any combinations of individual member also can be used for describing the present invention.Accordingly, for example, if X is retouched
It states into " selected from by X1、X2And X3The group formed ", and Y is described as " selected from by Y1、Y2And Y3The group formed ", then it represents that
It is X that X, which is fully described out,1Or X2Or X3And Y is Y1Or Y2Or Y3Opinion.
Herein, unless otherwise specified, " water " refers to H2O mainly exists in liquid form, but also may include other
Physical state, such as solid ice.In addition, herein, " water " refers at normal temperatures and pressures mainly by H2O molecules are constituted
Substance usually as liquid medium, and may include other compositions or Component units, for example, oxygen, trace element (such as calcium from
Son, magnesium ion, potassium ion, sodium ion, chlorion etc.) and/or impurity etc., but not limited to this, aforementioned other compositions or composition are single
Member is and the non-artificial addition because natural cause exists wherein during water generates mostly.Therefore, herein, " water " not only wraps
It includes purely by H2The pure material that O molecules are constituted is further included with plural H2O molecules are as carrier or medium and contain other compositions
Constituent or mixture.
Herein, refer to by a kind of or logical unless otherwise specified, term " constituent " is used interchangeably with " composition "
The substance that normal a variety of Component units, ingredient, compound or substance are formed." constituent " is artificially prepared product or product,
Component units, ingredient, the type of compound or substance, quantity, physical form included in constituent are it is usually because artificial
It intervenes and is limited, selects or controls.
Herein, unless otherwise specified, " hyperoxia (oxygen-enriched or oxygenated) " is described as one
Word, the noun (such as water) for representing its modification is so that its oxygen content, oxygen concentration or dissolved oxygen value is higher than by artificial intervention
Nature or without the state before artificial intervention.Unless otherwise specified, term " high-oxygen water " is used interchangeably with " heavy-oxygen-enriched water ".
In addition, oxygen content, oxygen concentration and dissolved oxygen value are referred to as " oxygen saturation (oxygen saturation) ", to describe oxygen
Quantity number or relative amount present in a medium (such as water), calculation are the oxygen-containing of the lower medium of the same terms
Amount, oxygen concentration or dissolved oxygen value divided by the medium may achieve highest oxygen content, oxygen concentration or dissolved oxygen value.
Herein, " dissolved oxygen ", " dissolved oxygen value ", " dissolving oxygen ", " dissolved oxygen content ", " oxygen content " and similar term
It is used interchangeably, refers to the oxygen-containing degree of every liter of medium (such as water), unit is mg/L or ppm.The measurement side of dissolved oxygen value
Formula includes electrochemical process, optical method, colorimetric method, titration etc., due to that can carry out dissolved oxygen value there are many instrument on the market
Measurement, therefore do not repeat especially herein.
Herein, term " biocompatibility " refers to that can be used for organism (such as people) and will not be generated to organism tight
The harmful effect person of weight, term " biocompatibility constituent " refer to the constituent of the high-oxygen water comprising the present invention, wherein hyperoxia
Medium or carrier of the water mainly as at least one biocompatible component.
Herein, term " medical component " refers to the constituent comprising high-oxygen water of the present invention and for medical usage,
It generally includes another biocompatible component to provide or enhance medical benefit, such as intravenous nutrition element (parenteral
) or drug nutrition.
Herein, term " cosmetic composition " refers to the composition comprising high-oxygen water of the present invention and for cosmetic use
Object generally includes another biocompatible component to provide or enhance beauty or modification effect, such as surfactant, powder
End, colorant, alcohols, tackifier, chelating agent, poly- silicon oxide compound, antioxidant, ultra-violet absorber, ultraviolet reflection agent, U.S.
White agent, moisturizer, fragrance, preservative, neutralizer and pH adjusting agent at least one, but not limited to this.
Herein, term " beverage composition " refers to comprising high-oxygen water of the present invention and edible or drinkable composition
Object generally includes another biocompatible component (it can be served ingredient, such as food additives) in favor of sale, such as anti-
Rotten agent, fungicide, antioxidant, nourishing additive agent, flavoring agent, acid, colorant, fragrance, sweetener, thickener and emulsification
At least one of agent, but not limited to this.
Herein, unless otherwise specified, physicochemical characteristic is measured under normal pressure (about 1 atmospheric pressure).
Herein, unless otherwise specified, physicochemical characteristic is surveyed under room temperature or room temperature (about 25 DEG C to about 27 DEG C)
It measures and obtains.
Herein, unless otherwise specified, " standing " refer to by high-oxygen water there is no artificial intervention (as disturbance, vibration
Or rock) under conditions of place a period of time, such as 5 minutes, 10 minutes, 30 minutes, 45 minutes, 60 minutes, 90 minutes, 120
Minute, 6 hours, 1 day, a couple of days, 1 week or several weeks.High-oxygen water can be rested under the temperature condition of a constant to remain high
The temperature of oxygen water is approximately fixed, such as stands under adiabatic conditions, such as rests in vacuum flask or cold insulation bottle, or by high-oxygen water
It rests in the open environment of temperature constant, is controlled by artificial heat to maintain environment temperature.In addition, also can be by hyperoxia
Water rests under the uncontrolled environment of temperature, as make under the conditions of room temperature its from initial temperature (such as 0 DEG C, 2 DEG C, 4 DEG C, 6 DEG C, 8
DEG C, 10 DEG C, 12 DEG C, 15 DEG C, 20 DEG C, 30 DEG C, 40 DEG C etc.) be gradually increasing or drop to room temperature.
Detailed description below is only substantially exemplary, is not intended to limitation present invention and application thereof.In addition, herein simultaneously
It is not limited by any theory described in the aforementioned prior art or invention content or detailed description below or embodiment.
Embodiment：The preparation of high-oxygen water
It is intended to prepare the high-oxygen water of the present invention, any type water body can be supplied oxygen under certain condition (or " to add
Oxygen ") it handles and obtains, actual conditions are as described below.
In the present invention, suitable for carry out oxygen supply processing water body can be through processing or untreated water body, including
But it is not limited to commercially available various bottled waters, tap water, mineral water, pure water, distilled water, magnetized water, electrolysis water, ionized water, life
The potable water body of any types such as state water, reverse osmosis water.Unless otherwise specified, then the range of aforementioned water body include mainly by
The water body that water is formed also includes that there are the water bodys of other compositions, such as using water as the water body of main medium, such as various types of beverages.
As the oxygen supply means in oxygen supply source, such as it may include the TaiWan, China new patent that applicant has authorized
No. M439652 " oxygen producing machine " a case disclosure of that (separately can be found in Chinese utility model patent CN202705029
Number), it is incorporated by herein incorporated by reference.In short, air compression is carried out using existing air compressor, by compressed sky
Gas is by molecular sieve, nitrogen in adsorption compression air and the oxygen for exporting high-purity.
High-oxygen water preparation method for the cooperation present invention uses, and oxygen supply means are preferably continous way apparatus of oxygen supply, such as aforementioned
" oxygen producing machine " patent, with continuously run and continue carry out oxygen supply.In addition, oxygen supply means can also be quantitative storage
Oxygen device, such as existing high pressure oxygen steel cylinder, flow that can be required persistently export oxygen at least a period of time, such as 30 points
Clock, 60 minutes, 120 minutes, 180 minutes, 210 minutes etc., wherein it is as described below to be suitable for the invention specific flow.
Specifically, the oxygen that oxygen supply means are exported can be pure oxygen, can also be the oxygen of high concentration, such as concentration
Higher than 80%, 85%, 90% or 95%, but it is not limited to this.
During oxygenated treatment carries out, aforementioned water body is located in a storage container, is continued by water body by apparatus of oxygen supply
The water body in oxygen to storage container is supplied in lower section, in addition, water body can be also placed in one larger storage container, by larger
Storage container supply water body to coupled logical smaller storage container, and oxygen is persistently supplied by apparatus of oxygen supply to compared with little Chu
Deposit the water body in container.During oxygenation, the storage container for putting water body can be open state, substantially air-tight state or complete
Air-tight state.
As a kind of specific embodiment, the TaiWan, China new patent M438316 that applicant has authorized can refer to
Number " high dissolved oxygen water dispenser " and No. M446884 " segmenting sub- high-oxygen water boiled water dispenser " two case disclosure of that are (another to can be found in
State's utility model patent No. 202820947 and No. 202932748), it is incorporated by herein incorporated by reference.
High-oxygen water after processing is taken for the convenience of the users, apparatus of oxygen supply and water body storage container can be fabricated to drink
The form of water dispenser or boiled water dispenser can supply water wherein the first water body storage container can be a kind of water supply installation to the second water body
Storage container, for example, water dispenser cold water container, the water body in oxygen to cold water container is persistently supplied by apparatus of oxygen supply.It utilizes as a result,
High-oxygen water made from the preparation method of high-oxygen water of the present invention can conveniently be taken by user.
In one embodiment, aforementioned boiled water dispenser includes pedestal and the water supply installation being set in pedestal and oxygen manufacture
Device, wherein accommodating space is formed in pedestal, pedestal bottom is installed with supporting rack, and the center of top of pedestal is then recessed downward
Have and is inverted the opening being inserted into for water butt.
Water supply installation has the pedestal for being located in accommodating space and being positioned at pedestal, and aqua storage tank, storage are equipped with above pedestal
Space above installing footstock center be equipped with to just and connection opening enter aquaporin, enter aquaporin center then be equipped with prolong upward
Stretch the ejection head for being inserted into and storage space being flowed into for its inside drinking water in water butt, footstock is passed through then at entering to be equipped on the outside of aquaporin
Perforation under putting on, pedestal front are equipped with more than one connection aqua storage tank to send out the Water outlet of drinking water.
Oxygen manufacturing device is set in the accommodating space of pedestal, and oxygen manufacturing device is provided with air above supporting rack
Compressor, solenoid valve, at least an oxygen-making trough and an accumulator tank, solenoid valve are connected to air compressor and oxygen-making trough, and oxygen-making trough with
Accumulator tank is connected to, and accumulator tank, which is connected with, to be extended upward by stretching into internal transfer tube above aqua storage tank, and transfer tube passes through footstock
Perforation stretch into storage space, then at transmission pipe end group be equipped with aeration tube.
In one embodiment, aforementioned boiled water dispenser further includes a sterilization or chlorination equipment, such as UV lamp pipe, can be installed in aqua storage tank
Inner wall or boiled water dispenser water outlet near, it is advantageously ensured that user can take sterile and safe high-oxygen water.Depending on high-oxygen water
Purposes depending on, sterilization or the type and quantity of chlorination equipment can be different.For example, it is used for the hyperoxia of medical usage
The water usually sterilizing demand with higher level.
Although prior art has disclosed all kinds of high-oxygen waters and preparation method thereof, inventor it was unexpectedly observed that
In the case of the certain Parameter Conditions of suitable control, the splendid high-oxygen water of stability can be made.Accordingly, the present invention discloses a kind of hyperoxia
The preparation method of water includes the steps that being supplied oxygen to a water body, it is characterised in that：During oxygen supply, the water body is maintained
Under conditions of 0 DEG C to 12 DEG C, oxygen is supplied to the water body with the flow of 50cc/min to 1000cc/min, and oxygen supply time
No less than 30 minutes.
Specifically, if inventor is surprised to find that water temperature, flow and time in suitable control technique, incite somebody to action
Be conducive to improve the stability of high-oxygen water.Thus obtained high-oxygen water, oxygen content can remain relatively small under given conditions
Variable quantity.
In general, in aforementioned preparation process, the volume of water body is not particularly limited.Under conditions of a large amount of manufactures,
The volume of water body can be hundreds of litres, thousands of litres or higher volume.In household, if being grasped in the form of boiled water dispenser
Make or implement aforementioned preparation process, it is contemplated that the volume of the volume size of boiled water dispenser device, usual water body can be tens of milliliters
To several liters, for example, 100 milliliters, 200 milliliters, 500 milliliters, 1 liter, 2 liters, 3 liters, 5 liters, 8 liters, 10 liters, 15
Litre etc., depending on the aqua storage tank of all kinds of boiled water dispensers or cold water container capacity.In one embodiment, the volume of water body is between 1 public affairs
Between liter and 15 liters.
In aforementioned preparation process, for treatment temperature, if the water body is maintained 0 DEG C to 12 DEG C during oxygen supply
Under conditions of, higher maximum dissolved oxygen value will be can get.In particular, inventor by temperature it was unexpectedly observed that maintain 4 DEG C extremely
Best dissolved oxygen effect can be obtained under conditions of 8 DEG C, such as highest dissolved oxygen value can be about 60ppm, 55ppm or 50ppm.One
In preferred embodiment, the water body is maintained under conditions of about 6 DEG C during oxygen supply.
In aforementioned preparation process, for oxygen flow, inventor is it was unexpectedly observed that excessively high oxygen flow and helpless
In the stability of final high-oxygen water, or even the stability of high-oxygen water may be unfavorable under certain conditions.On the contrary, aforementioned preparation
Method supplies oxygen to water body, to obtain the high-oxygen water of higher stability using the flow of 50cc/min to 1000cc/min.
By taking the oxygen content of general water body is about 3ppm to 5ppm as an example, found after inventor's observation, using aforementioned preparation side
Method is during supplying oxygen, and the oxygen content of water body is to before of about 20ppm to 25ppm, increased oxygen content (ppm/ per minute
Min it) can increase with the flow of supply oxygen and improve, however, after the oxygen content of water body is to of about 20ppm to 25ppm, often
Minute, increased oxygen content then will not obviously be influenced by oxygen supply flow, if or even being continuing under certain conditions
High flow is supplied oxygen (as being higher than 1500cc/min), and is unprofitable to improve the stability of high-oxygen water.Accordingly, system of the invention
Preparation Method be supply oxygen to water body using the flow of 50cc/min to 1000cc/min, such as it is permanent when or all the period of time be all made of it is solid
Fixed low discharge is supplied oxygen, such as 50cc/min, 100cc/min, 150cc/min, 200cc/min, 250cc/min, 300cc/
Min, 400cc/min, 500cc/min or 1000cc/min, but not limited to this.
In one embodiment, also sectional is supplied oxygen using different flow, for example, during oxygen supply, first with the
One flow is supplied oxygen, until the oxygen content of water body reaches 20ppm between 25ppm, then, then is supplied with second flow
Oxygen, wherein second flow are less than or equal to first flow.For example, first flow is not less than 50cc/min, and second flow is not
More than 1000cc/min.
In aforementioned preparation process, for oxygen supply time, inventor is it was unexpectedly observed that be different from the prior art using short
Time, high flow capacity, high pressure mode prepare high-oxygen water, the present invention, which is utilized, to be beneficial to improve high-oxygen water long lasting for oxygen supply
Stability.Therefore, in one embodiment, oxygen supply time is no less than 30 minutes, for example, oxygen supply time can be 45 minutes, 60 minutes,
90 minutes, 120 minutes, 150 minutes, 180 minutes, 210 minutes or 240 minutes.In one embodiment, oxygen supply time is 60 minutes
To 240 minutes.In one embodiment, when water body increased oxygen content per minute has been less than such as 0.01ppm/min, display water body
Oxygen content approached to saturation, the high-oxygen water completed at this time is capable of direct drinking or envelope bottle is for subsequently drinking.
Accordingly, preparation method of the invention, can be to each by controlling the parameters such as water temperature, oxygen flow, oxygen supply time
The water body of kind volume carries out oxygen supply processing, to prepare the high-oxygen water with excellent stability.
Embodiment：The highest measure of oxygen content of high-oxygen water
Take commercially available Yue Shi bottled mineral waters and very good bottled mineral water respectively as staying water one and accessing pending water
Body two, the original oxygen content before oxygenated treatment is respectively 3.7ppm and 3.5ppm.By the aforementioned water of certain volume (about 1 gallon)
Body is poured into respectively in the cold water container of boiled water dispenser described in previous embodiment, and (about 4 DEG C to 8 of the temperature of water body is maintained with cooling line
DEG C), and oxygenated treatment is carried out with certain flow (about 200cc/min), about 200 milliliters of water body is periodically exported during processing and with molten
Solution oxygen tester WTWOxi3210 collocation 325 electrodes of CellOx measure its oxygen content at room temperature.Experiment display, accessing pending water
Body one reaches highest oxygen content, about 38.5ppm after about 208 minutes in oxygenated treatment, staying water two oxygenated treatment about
Reach highest oxygen content, about 37.8ppm after 220 minutes.
Embodiment：The stability analysis (I) of high-oxygen water
Oxygenated treatment is carried out to obtain for staying water one and staying water two in a manner of described in the previous embodiment
High-oxygen water one and high-oxygen water two, and export about 200 milliliters respectively and be statically placed in open environment at room temperature, periodic measurement high-oxygen water
One and high-oxygen water two oxygen content with the time variable condition, as a result as shown in following table one.
Table one
By upper table numerical value it can be found that high-oxygen water prepare after the completion of place 30 minutes in, oxygen content reduce amplitude compared with
Greatly, thus it is speculated that should be caused by this section of time dissolved oxygen state not yet reaches and stablize, but it is then relatively stable later, and oxygen content reduce amplitude with
It the time and declines.In addition, it is possible to find even in open environment and at room temperature, if by the initial oxygen content of high-oxygen water one
The initial oxygen content (38.6ppm) of (37.9ppm) and high-oxygen water two is respectively seen as 100% meter, after high-oxygen water is stood 30 minutes
Oxygen content percentage (be respectively 79.95% and 80.31%) subtract the oxygen content percentage after high-oxygen water is stood 180 minutes
Difference obtained by (be respectively 67.81% and 64.77%) is respectively 12.14% and 15.54%, and containing after standing 180 minutes
Oxygen amount still greater than or be equal to 25ppm, show the present invention high-oxygen water have height stability.
Embodiment：The stability analysis (II) of high-oxygen water
High-oxygen water one and high-oxygen water two are prepared in a manner of previous embodiment, and be separately heated to 10 DEG C, 15 DEG C, 20 DEG C,
25 DEG C and 30 DEG C to 40 DEG C and its oxygen content is measured, as a result as shown in following table two.
Table two
| Temperature (DEG C) | One oxygen content of high-oxygen water (ppm) | Opposite oxygen content percentage (%) | Two oxygen content of high-oxygen water (ppm) | Opposite oxygen content percentage (%) |
| 10 | 34.9 | 100 | 37.0 | 100 |
| 15 | 35.9 | 102.87 | 37.0 | 100 |
| 20 | 37.0 | 106.02 | 38.5 | 104.05 |
| 25 | 36.3 | 104.01 | 40.6 | 109.73 |
| 30 | 33.7 | 96.56 | 30.9 | 83.51 |
| 31 | 33.7 | 96.56 | 29.8 | 80.54 |
| 32 | 33.4 | 95.70 | 29.8 | 80.54 |
| 33 | 33.2 | 95.13 | 29.8 | 80.54 |
| 34 | 33.5 | 95.99 | 29.8 | 80.54 |
| 35 | 33.3 | 95.42 | 29.9 | 80.81 |
| 36 | 33.1 | 94.84 | 29.9 | 80.81 |
| 37 | 32.7 | 93.70 | 29.9 | 80.81 |
| 38 | 32.6 | 93.41 | 29.9 | 80.81 |
| 39 | 32.4 | 92.84 | 29.8 | 80.54 |
| 40 | 32.4 | 92.84 | 29.9 | 80.81 |
In table two, it can be observed to have in high-oxygen water preparation completion initial stage to initial warm-up period (15 DEG C to 25 DEG C) oxygen-containing
Measure increased situation, thus it is speculated that should be since high-oxygen water has just just been prepared caused by stable state has not yet been reached in completion.It waits entering and stablizes shape
After state, it is possible to find the oxygen content variation of high-oxygen water then tends towards stability.For high-oxygen water one, it is possible to find heat it from 10 DEG C
To after 40 DEG C, oxygen content variation is less than 10%, and oxygen content is held in 30ppm or more during heating；For high-oxygen water two
For, it is possible to find by it from after 10 DEG C are heated to 40 DEG C, oxygen content variation is less than 20%, and oxygen content is held in the left sides 30ppm
It is right.
Embodiment：The stability analysis (III) of high-oxygen water
High-oxygen water one and high-oxygen water two are prepared in a manner of previous embodiment, from initial temperature be separately heated to 37 DEG C, 35
DEG C, 30 DEG C and substantially maintain at said temperatures, measure its oxygen content after 30,60,90,120 minutes respectively, as a result respectively such as
Shown in following table three (37 DEG C), table four (35 DEG C) and table five (30 DEG C).
Table three
Table four
Table five
It can be observed by the data of table three to table five, high-oxygen water of the present invention maintains under conditions of 30 DEG C to 40 DEG C
After 120 minutes, oxygen content variation smaller than 30%, preferably smaller than 25%, more preferably less than 20%.In addition, of the present invention
High-oxygen water maintained 120 minutes under conditions of 30 DEG C to 40 DEG C during, oxygen content be not less than 20ppm, preferably not less than
25ppm.On the other hand, high-oxygen water of the present invention can maintain oxygen content to be no less than 20ppm under conditions of 30 DEG C to 40 DEG C
At least up to 60 minutes, and preferably oxygen content can be maintained to be no less than 25ppm under conditions of about 37 DEG C and be at least up to 120 minutes.
Since the temperature of general human body is about 37 DEG C, from the above data, high-oxygen water of the invention is in normal person's body temperature
Under the conditions of still keep relatively high oxygen content, oxygen content can be kept to be no less than 25ppm under conditions of 37 DEG C and be at least up to 120 points
Clock, this time can be enough that high-oxygen water is allowed to recycle in vivo for a long time and still have rich oxygen content, be conducive to improve parts of body
Oxygen content.
In addition, by commercially available natural beauty health care high-oxygen water and hundred HOPPER O living2High-oxygen water respectively as comparative example one and
Comparative example two is separately heated to 37 DEG C, 35 DEG C, 30 DEG C from initial temperature and substantially maintains at said temperatures, respectively 30,
60, its oxygen content is measured after 90,120 minutes, as a result respectively such as following table six (37 DEG C), table seven (35 DEG C) and table eight (30 DEG C) institute
Show.
Table six
Table seven
Table eight
Comparison sheet three to table five the embodiment of the present invention and table six to table eight comparative example, can find easily the present invention height
Oxygen water after 120 minutes, still has higher oxygen content, oxygen content under the conditions of being placed on relatively-high temperature (being higher than 30 DEG C)
Variation preferably smaller than 25%, more preferably less than 20%, and oxygen content remains above 20ppm after 120 minutes, preferably higher than
25ppm.On the other hand, the high-oxygen water of comparative example is under the conditions of being placed on relatively-high temperature (being higher than 30 DEG C), after 120 minutes,
And can not have higher oxygen content, and oxygen content reduces about 35% to 43%, and oxygen content is below 15ppm.
Embodiment：The stability analysis (IV) of high-oxygen water
High-oxygen water one and high-oxygen water two are prepared in a manner of previous embodiment, are separately heated to from about 8 DEG C of initial temperatures
About 50 DEG C, during which simultaneously its oxygen content of continuous observation variation, as a result as shown in Table 9.
Table nine
It can be observed by the data of table nine, by high-oxygen water produced by the present invention from after initial temperature is heated to high temperature, still
There can be relatively high oxygen content.For example, the initial temperature by high-oxygen water from 5 DEG C to 10 DEG C is heated to 40 DEG C to 50 DEG C
After temperature, oxygen content variation is less than 20%, and its oxygen content keeps no less than 25ppm during heating.In addition, by high-oxygen water
From after the temperature that 5 DEG C to 10 DEG C of initial temperatures are heated to 40 DEG C to 50 DEG C, oxygen content variation preferably smaller than 15%, and heat
Its oxygen content of period keeps preferably no less than 30ppm.
As seen from the above embodiment, high-oxygen water of the invention has preferable stability really, has after the completion of preparing
Relatively high dissolved oxygen value, and its oxygen content changes as time goes by and/or under the conditions of relatively-high temperature (such as 37 DEG C of body temperature)
Amplitude is small, and oxygen-containing numerical quantity preferably may remain in 25ppm or more, is not only suitable for directly drinking, and is suitble to further processing
All kinds of constituents are made, are provided to human body in the form of all kinds of, such as with intravenous injection (intravenous injection), quiet
Arteries and veins is transfused the approach such as (intravenous infusion), oral, coating, and without being limited thereto.
In one embodiment, the high-oxygen water that the preceding method of the present invention is prepared can be prepared into a kind of biocompatibility
Constituent, it includes the high-oxygen water of the present invention and at least one biocompatible components.
Embodiment：Medical component
In this embodiment, it is that the high-oxygen water for being prepared the preceding method of the present invention is prepared into a kind of medicine composition
Object, and the biocompatible component is intravenous nutrition element and/or drug.
For example, all kinds of known intravenous nutrition elements can be added to the high-oxygen water that preceding method is prepared, it is such
Intravenous nutrition element can be at least one of amino acid, fat, carbohydrate, electrolyte, vitamin and minerals or its arbitrary two kinds
Or a variety of combination.For example, intravenous nutrition element can be dextrose (such as glucose) solution or concentration of concentration 5%
Thus 0.9% sodium chloride solution provides a kind of medical component suitable for venoclysis.
In addition, for example, can all kinds of known small molecules or macromolecular drug be added to preceding method and are prepared
High-oxygen water, thus obtain a kind of medical component with disease treatment purposes.Foregoing pharmaceutical is not specially limited, as long as its
It is suitble to exist as an aqueous solution.
Embodiment：Cosmetic composition
In this embodiment, it is that the high-oxygen water for being prepared the preceding method of the present invention is prepared into a kind of cosmetics composition
Object, and the biocompatible component is any common cosmetic additive agent, for example, such cosmetic additive agent can
To be surfactant, powder, colorant, alcohols, tackifier, chelating agent, poly- silicon oxide compound, antioxidant, ultraviolet radiation absorption
Agent, ultraviolet reflection agent, whitening agent, moisturizer, fragrance, preservative, neutralizer and pH adjusting agent at least one or its
It anticipates two or more of combinations, and without being limited thereto.
Aforesaid cosmetic product constituent generally is suitable for being provided to human body in the form of external application, such as the cosmetic composition is applied
It applies to human body in need.
Embodiment：Beverage composition
In this embodiment, it is that the high-oxygen water for being prepared the preceding method of the present invention is prepared into a kind of beverage composition
Object, and the biocompatible component is any common food additives, for example, such food additives can be
Preservative, fungicide, antioxidant, nourishing additive agent, flavoring agent, acid, colorant, fragrance, sweetener, thickener and breast
At least one of agent or its arbitrary two or more of combination, and it is without being limited thereto.
Accordingly, can bottled or canned form be made in the said beverage constituent containing high-oxygen water of the present invention to sell.
Embodiment of above be substantially only aid in illustrating, and be not intended to limit application object embodiment or these
The application of embodiment or purposes.Herein, term " illustrative " representative " as an example, example or explanation ".Unless otherwise
Indicate, otherwise herein any illustrative embodiment can not necessarily be read as other embodiment be
It is preferred that or advantageously.
In addition, although an at least exemplary embodiments have been proposed in the foregoing embodiment, it will be appreciated that the present invention still may be used
In the presence of a large amount of variation.It is asked it is equally understood that embodiment as described herein is not intended to limit in any manner
Range, purposes or the configuration for the application object asked.Opposite, aforementioned embodiments can provide a kind of letter of those skilled in the art
Just guide is to implement one or more described embodiments.Furthermore the range of this patent is special comprising known equipollent and at this
It is all it is contemplated that equipollent when sharp application case is filed an application.
Claims (33)
1. a kind of high-oxygen water, including water and oxygen, it is characterised in that：
The oxygen content of the high-oxygen water is no less than 20ppm；
It is the oxygen content percentage after standing the high-oxygen water 30 minutes in terms of 100% by the initial oxygen content of the high-oxygen water
(A) difference (A-B) between oxygen content percentage (B) the two after and standing the high-oxygen water 180 minutes is less than 24%；And
After the high-oxygen water maintains 120 minutes under conditions of 30 DEG C to 40 DEG C, oxygen content variation is less than 30%.
2. high-oxygen water as described in claim 1, wherein the difference is less than 20%.
3. high-oxygen water as described in claim 1, wherein the difference is less than 15%.
4. high-oxygen water as described in claim 1, wherein the difference is between 5% and 20%.
5. high-oxygen water as described in claim 1, wherein the oxygen content of the high-oxygen water is no less than 25ppm.
6. high-oxygen water as described in claim 1, wherein the oxygen content of the high-oxygen water is between 20ppm and 50ppm.
7. high-oxygen water as described in claim 1, after standing 180 minutes, oxygen content is no less than 25ppm.
8. the high-oxygen water as described in any one of claim 1 to 7, wherein the oxygen content is the high-oxygen water at 0 DEG C to 40
It is measured from the state of DEG C.
9. high-oxygen water as claimed in claim 8, wherein the oxygen content is the high-oxygen water in the state of 0 DEG C to 12 DEG C
It is measured from.
10. the high-oxygen water as described in any one of claim 1 to 7, wherein the high-oxygen water is heated to 40 DEG C from 10 DEG C
Afterwards, oxygen content variation is less than 20%.
11. high-oxygen water as claimed in claim 10, wherein by the high-oxygen water from after 10 DEG C are heated to 40 DEG C, oxygen-containing quantitative change
Change and is less than 10%.
12. the high-oxygen water as described in any one of claim 1 to 7, wherein the high-oxygen water is heated to 40 DEG C from 10 DEG C
Afterwards, oxygen content is no less than 25ppm.
13. high-oxygen water as described in claim 1, after being maintained 120 minutes under conditions of 37 DEG C, oxygen content variation is less than
25%.
14. the high-oxygen water as described in any one of claim 1 to 7 maintains 120 minutes under conditions of 30 DEG C to 40 DEG C
Afterwards, oxygen content is no less than 20ppm.
15. high-oxygen water as claimed in claim 14, after being maintained 120 minutes under conditions of 37 DEG C, oxygen content is no less than
25ppm。
16. the high-oxygen water as described in any one of claim 1 to 7 can maintain oxygen content under conditions of 30 DEG C to 40 DEG C
No less than 20ppm is at least up to 60 minutes.
17. high-oxygen water as claimed in claim 16, oxygen content can be maintained to be no less than 25ppm under conditions of 37 DEG C and be at least up to
120 minutes.
18. the high-oxygen water as described in any one of claim 1 to 7, oxygen content is no less than under conditions of higher than 40 DEG C
25ppm。
19. the high-oxygen water as described in any one of claim 1 to 7, wherein the high-oxygen water is initial from 5 DEG C to 10 DEG C
After temperature is heated to 40 DEG C to 50 DEG C of temperature, oxygen content variation is less than 20%.
20. the high-oxygen water as described in any one of claim 1 to 7, wherein the high-oxygen water is initial from 5 DEG C to 10 DEG C
During temperature is heated to 50 DEG C, oxygen content keeps no less than 30ppm.
21. the high-oxygen water as described in any one of claim 1 to 7 is made of water, oxygen and non-artificial adding ingredient.
22. a kind of biocompatibility constituent, it is characterised in that include the high-oxygen water described in any one of claim 1 to 21,
And at least one biocompatible component.
23. it is medical component biocompatibility constituent as claimed in claim 22, and the biocompatible component
For intravenous nutrition element or drug.
24. biocompatibility constituent as claimed in claim 23, wherein the intravenous nutrition element is selected from amino acid, fat
At least one of fat, carbohydrate, electrolyte, vitamin and minerals.
Be cosmetic composition 25. biocompatibility constituent as claimed in claim 22, and the biocompatibility at
Divide is selected from interfacial agent, powder, colorant, alcohols, tackifier, chelating agent, poly- silicon oxide compound, antioxidant, ultraviolet light
Absorbent, ultraviolet reflection agent, whitening agent, moisturizer, fragrance, preservative and pH adjusting agent at least one.
26. it is beverage composition biocompatibility constituent as claimed in claim 22, and the biocompatible component
It is to be selected from preservative, fungicide, antioxidant, nourishing additive agent, flavoring agent, colorant, fragrance, thickener and emulsifier extremely
Few one kind.
27. a kind of preparation method of high-oxygen water as described in claim 1, includes the steps that being supplied oxygen to a water body, special
Sign is：During oxygen supply, under conditions of the water body is maintained 0 DEG C to 12 DEG C, with 50cc/min to 1000cc/min's
Flow supplies oxygen to the water body, and oxygen supply time is no less than 30 minutes.
28. method as claimed in claim 27, wherein during oxygen supply, the water body is maintained to 4 DEG C to 8 DEG C of condition
Under.
29. method as claimed in claim 28, wherein the volume of the water body is between 1 liter and 15 liters.
30. method as claimed in claim 29, wherein the oxygen supply time is no less than 180 minutes.
31. method as claimed in claim 27, wherein during oxygen supply, first supplied oxygen with first flow, until water body
Oxygen content reaches 20ppm between 25ppm, then, then is supplied oxygen with second flow, and wherein second flow is less than or equal to the
One flow.
32. method as claimed in claim 31, wherein the first flow is not less than 50cc/min, and the second flow is not
More than 1000cc/min.
33. the high-oxygen water that a kind of method by described in any one of claim 27 to 32 is prepared.
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| HK16107922.0A HK1219940A1 (en) | 2015-09-07 | 2016-07-07 | Oxygen-enriched water, biocompatible composition containing oxygen- enriched water and method of preparing oxygen- enriched water |
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| CN201510562685.3A CN105366792B (en) | 2015-09-07 | 2015-09-07 | The preparation method of high-oxygen water, biocompatibility constituent and high-oxygen water containing high-oxygen water |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103408121A (en) * | 2013-07-26 | 2013-11-27 | 徐礼鲜 | Device for preparing water with dissolved hydrogen and dissolved oxygen through microbubble, replacement, baffle and mixing |
| CN103408122A (en) * | 2013-07-26 | 2013-11-27 | 徐礼鲜 | High-oxygen rich-hydrogen water and preparation method and application thereof |
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2015
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103408121A (en) * | 2013-07-26 | 2013-11-27 | 徐礼鲜 | Device for preparing water with dissolved hydrogen and dissolved oxygen through microbubble, replacement, baffle and mixing |
| CN103408122A (en) * | 2013-07-26 | 2013-11-27 | 徐礼鲜 | High-oxygen rich-hydrogen water and preparation method and application thereof |
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