CN105334169A - Spectrometric multi-component gas analyzer for transformer oil gas - Google Patents

Spectrometric multi-component gas analyzer for transformer oil gas Download PDF

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Publication number
CN105334169A
CN105334169A CN201510878655.3A CN201510878655A CN105334169A CN 105334169 A CN105334169 A CN 105334169A CN 201510878655 A CN201510878655 A CN 201510878655A CN 105334169 A CN105334169 A CN 105334169A
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China
Prior art keywords
bottle
transformer oil
volume measuring
initial
filtrator
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Granted
Application number
CN201510878655.3A
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Chinese (zh)
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CN105334169B (en
Inventor
菅有为
段建军
庄燕飞
曲文韬
冯迎春
任庆帅
冯玉柱
吕学宾
卢志鹏
袁森
孙兆国
惠杰
杨逸晴
陈仁刚
杨晓滨
陈培峰
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State Grid Corp of China SGCC
Maintenance Branch of State Grid Shandong Electric Power Co Ltd
Original Assignee
State Grid Corp of China SGCC
Maintenance Branch of State Grid Shandong Electric Power Co Ltd
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Priority to CN201510878655.3A priority Critical patent/CN105334169B/en
Publication of CN105334169A publication Critical patent/CN105334169A/en
Application granted granted Critical
Publication of CN105334169B publication Critical patent/CN105334169B/en
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Abstract

A spectrometric multi-component gas analyzer for transformer oil gas comprises a spectrograph host machine and an impurity filtration device, wherein the impurity filtration device comprises a support, two volume measuring instruments and a filter are installed on the support, the two volume measuring instruments are respectively installed at the upper portion and the lower portion of the filter, and the volume measuring instruments are in serial connection with the filter. A second communication pipe is arranged between the impurity filtration device and the spectrograph host machine, and a delivery pump is arranged on the second communication pipe. A supporting seat is installed at the upper portion of the support, a plurality of initial bottles are arranged on the supporting seat, an outlet of each initial bottle is connected with a flow divider valve through management, the flow divider valve is connected with an inlet, a fixing rack is installed on the side of each initial bottle, an electric pushing rod is arranged on each fixing rack, a masking agent tube is arranged on the side of each initial bottle, and the ends of the piston rods of the electric pushing rods are matched with the inner walls of the masking agent tubes. By the adoption of the spectrometric multi-component gas analyzer, a transformer oil sample is added into the initial bottles first, a corresponding masking agent is filled into the initial bottles according to the measurement demands, and accordingly the influence of heavy metal ions is reduced.

Description

A kind of transformer oil gas multicomponent gas spectroanalysis instrument
Technical field
The present invention relates to and belongs to transformer oil checkout equipment field, is exactly a kind of transformer oil gas multicomponent gas spectroanalysis instrument.
Background technology
Transformer oil is a kind of fraction products of oil, has the effects such as insulation, thermolysis, extinguishing arc in transformer application.Transformer oil after Long-Time Service needs periodic detection, avoids deterioration of oil product to cause effect to decline.At present, employing spectrometer is detected for transformer oil to carry out.There are insoluble greasy filth, fiber and foul etc. in the transformer oil of Long-Time Service, these materials may cause spectrometer to block, and cause fault together.During for multicomponent determination` in transformer oil, be easily subject to the impact of part heavy metal ion, cause measurement result accuracy to reduce.
Summary of the invention
For solving the problem, the object of this invention is to provide a kind of transformer oil gas multicomponent gas spectroanalysis instrument.
The present invention for achieving the above object, is achieved through the following technical solutions:
A kind of transformer oil gas multicomponent gas spectroanalysis instrument, comprise spectrometer unit and device for filtering impurities, device for filtering impurities comprises support, support installs two volume measuring instruments and filtrator, two volume measuring instruments are arranged on the upper and lower of filtrator respectively, volume measuring instrument and positioned inline; Volume measuring instrument is made up of bottle, separation net, Infrared survey instrument and floater shot, bottle upper and lower arranges import and outlet respectively, and arrange vertical separation net in bottle, floater shot is positioned at bottle, bottle upper side installation infrared measuring instrument, Infrared survey instrument is positioned at floater shot side; Filtrator is made up of filtration barrel body, several screen pack and upper cover, and filtration barrel body inwall arranges fixture block, and several screen pack is distributed up and down and coordinated by support bar each other, and support bar card is placed on fixture block, and upper cover coordinates with filtration barrel body; Upper cover is connected by flexible pipe with the volume measuring instrument on filtrator top; Arranged for the second communicating pipe between device for filtering impurities and spectrometer unit, the second communicating pipe was provided with discharge pump; Supporting seat is installed on the top of support, supporting seat is arranged several initial bottle, the outlet of each initial bottle each connects diverting valve by management, the connection import of diverting valve, the sidepiece of each initial bottle all installs a fixed mount, fixed mount is arranged electric push rod, the sidepiece of each initial bottle arranges screening agent pipe, and the piston rod end of electric push rod coordinates with screening agent inside pipe wall.
For realizing object of the present invention further, can also by the following technical solutions: between described spectrometer unit and device for filtering impurities, de-watering apparatus is set, third connecting pipe is set between de-watering apparatus and spectrometer unit, second communicating pipe arranged T-valve, T-valve connects one end of the first communicating pipe, and the other end of the first communicating pipe connects de-watering apparatus; De-watering apparatus comprises base, and base installs two weighers and vacuum drainage cylinder, and two weighers lay respectively at vacuum drainage cylinder two ends, and weigher is connected with vacuum drainage cylinder; Weigher is made up of weighing cup and electronic scale, and weighing cup is fixedly mounted on the top of electronic scale; Vacuum drainage cylinder comprises cylindrical shell, arranges heating rod in cylindrical shell, and the top of cylindrical shell arranges gas-liquid separator, and gas-liquid separator connects vacuum pump.Described spectrometer unit is arranged input keyboard, overturning seat and display screen, display screen is connected with spectrometer unit by overturning seat.
The invention has the advantages that: first transformer oil sample joins in initial bottle by the present invention, according to measurement needs, in initial bottle, inject corresponding screening agent, thus reduce the impact of heavy metal ion, improve the accuracy of measurement result, realize measurement of multi-components.Tested transformer oil can be filtered before detection, by insoluble greasy filth, fiber and dirt filtration out, avoid spectrometer to block.After being filtered by device for filtering impurities, can calculate and obtain volume number shared by impurity, determine tested transformer oil reuses after whether can carrying out filtration treatment, thus determine the transformer oil that whether is necessary again to renew, avoid waste.Clear up after filtration conveniently.Transformer oil after filtration, after kaleidophon detects, can reduce the impact of solid matter, discharges physical factor, obtains experimental result and more press close to production and application.The present invention also has advantage compact, cheap for manufacturing cost and easy to use simple for structure.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention; Fig. 2 is the I partial enlargement structural representation of Fig. 1; Fig. 3 is the II partial enlargement structural representation of Fig. 1; Fig. 4 is that the A of Fig. 1 is to looking structure for amplifying schematic diagram.
Reference numeral: 1 spectrometer unit 2 input keyboard 3 overturning seat 4 display screen 5 weighing cup 6 electronic scale 7 vacuum drainage cylinder 8 base 9 heating rod 10 weigher 11 T-valve 12 discharge pump 13 support 14 volume measuring instrument 15 filtrator 16 first communicating pipe 17 second communicating pipe 18 vacuum pump 19 gas-liquid separator 20 third connecting pipe 21 bottle 22 separation net 23 Infrared survey instrument 24 floater shot 25 import 26 exports the electric push rod of the 27 filtration barrel body 28 fixture block 29 screen pack 30 support bar 31 upper cover 32 initial bottle 34 diverting valve 35 fixed mount 36 screening agent pipe 37 of supporting seat 33.
Embodiment
A kind of transformer oil gas multicomponent gas spectroanalysis instrument, as shown in Figure 1, Figure 2 and Figure 3, comprise spectrometer unit 1 and device for filtering impurities, device for filtering impurities comprises support 13, support 13 installs two volume measuring instruments 14 and filtrator 15, two volume measuring instruments 14 are arranged on the upper and lower of filtrator 15 respectively, and volume measuring instrument 14 and filtrator 15 are connected; Volume measuring instrument 14 is made up of bottle 21, separation net 22, Infrared survey instrument 23 and floater shot 24, bottle 21 upper and lower arranges import 25 and outlet 26 respectively, vertical separation net 22 is set in bottle 21, floater shot 24 is positioned at bottle 21, bottle 21 upper side installation infrared measuring instrument 23, Infrared survey instrument 23 is positioned at floater shot 24 side; Filtrator 15 is made up of filtration barrel body 27, several screen pack 29 and upper cover 31, filtration barrel body 27 inwall arranges fixture block 28, several screen pack about 29 is distributed and is coordinated by support bar 30 each other, and support bar 30 card is placed on fixture block 28, and upper cover 31 coordinates with filtration barrel body 27; Upper cover 31 is connected by flexible pipe with the volume measuring instrument 14 on filtrator 15 top; Arrange between device for filtering impurities and spectrometer unit 1 and be provided with discharge pump 12 second communicating pipe 17 communicating pipe 17, second; Supporting seat 32 is installed on the top of support 13, supporting seat 32 is arranged several initial bottle 33, the outlet of each initial bottle 33 each connects diverting valve 34 by management, the connection import 25 of diverting valve 34, the sidepiece of each initial bottle 33 all installs a fixed mount 35, fixed mount 35 is arranged electric push rod 37, the sidepiece of each initial bottle 33 arranges screening agent pipe 36, and the piston rod end of electric push rod 37 coordinates with screening agent pipe 36 inwall.
Use procedure of the present invention is: be added in the volume measuring instrument 14 on top by checked transformer oil sample, before adding, closes the valve of volume measuring instrument 14 upper outlet.Along with adding of transformer oil, floater shot 24 upwards floats, and avoids floater shot 24 to move left and right under the restriction of separation net 22, after adding stopping, being measured the position of floater shot 24 by Infrared survey instrument 23, thus determines the volume of the transformer oil added.Transformer oil in the volume measuring instrument 14 on top is entered after filtrator 15 filters the volume measuring instrument 14 of bottom.In like manner, the volume of the transformer oil after filtration can be measured, thus obtain the amount filtering out impurity.If the amount of filtered impurities is fewer, illustrate that this transformer oil reuses after can filtering.For filtrator 15, upper cover 31 can be opened during cleaning, screen pack 29 is taken out cleaning.
Owing to also there is a lot of moisture in transformer oil, moisture also can affect testing result, and detecting the water cut of the transformer oil of Long-Time Service is also an important indicator.In order to realize lab scale test, between described spectrometer unit 1 and device for filtering impurities, de-watering apparatus is set, third connecting pipe 20 is set between de-watering apparatus and spectrometer unit 1, second communicating pipe 17 arranged T-valve 11, T-valve 11 connects one end of the first communicating pipe 16, and the other end of the first communicating pipe 16 connects de-watering apparatus; De-watering apparatus comprises base 8, and on base 8, installation two weighers 10 and vacuum drainage cylinder 7, two weighers 10 lay respectively at vacuum drainage cylinder 7 two ends, and weigher 10 is connected with vacuum drainage cylinder; Weigher 10 is made up of weighing cup 5 and electronic scale 6, and weighing cup 5 is fixedly mounted on the top of electronic scale 6; Vacuum drainage cylinder 10 comprises cylindrical shell, arranges heating rod 9 in cylindrical shell, and the top of cylindrical shell arranges gas-liquid separator 19, and gas-liquid separator 19 connects vacuum pump 18.Transformer oil after filtration is added in weigher 10 and weighs, enter in vacuum drainage cylinder 7 after weighing, improving temperature by heating rod 9 is moisture evaporation, reduces pressure by vacuum pump 18, extruded by moisture in transformer oil, moisture is separated through gas-liquid separator 19.Transformer oil after draining weighs entering another weigher 10, thus determines the water cut in transformer oil.Can judge whether transformer oil can be recycled according to water cut.
Described spectrometer unit 1 is arranged input keyboard 2, overturning seat 3 and display screen 4, display screen 4 is connected with spectrometer unit 1 by overturning seat 3.Display screen 4 and input keyboard 2 are structure as a whole with spectrometer main frame 1, easy to use, and without the need to other connection device, when not using, display screen 4 turnover can be protected display screen 4, display screen 4 can cover on input keyboard 2, also can protect input keyboard.
Technical scheme of the present invention is not restricted in the scope of embodiment of the present invention.The technology contents of the not detailed description of the present invention is known technology.

Claims (3)

1. a transformer oil gas multicomponent gas spectroanalysis instrument, it is characterized in that: comprise spectrometer unit (1) and device for filtering impurities, device for filtering impurities comprises support (13), upper installation two volume measuring instruments (14) of support (13) and filtrator (15), two volume measuring instruments (14) are arranged on the upper and lower of filtrator (15) respectively, volume measuring instrument (14) and filtrator (15) series connection; Volume measuring instrument (14) is made up of bottle (21), separation net (22), Infrared survey instrument (23) and floater shot (24), bottle (21) upper and lower arranges import (25) and outlet (26) respectively, vertical separation net (22) is set in bottle (21), floater shot (24) is positioned at bottle (21), bottle (21) upper side installation infrared measuring instrument (23), Infrared survey instrument (23) is positioned at floater shot (24) side; Filtrator (15) is made up of filtration barrel body (27), several screen pack (29) and upper cover (31), filtration barrel body (27) inwall arranges fixture block (28), several screen pack (29) is distributed up and down and is coordinated by support bar (30) each other, support bar (30) card is placed on fixture block (28), and upper cover (31) coordinates with filtration barrel body (27); Upper cover (31) is connected by flexible pipe with the volume measuring instrument (14) on filtrator (15) top; Arrange the second communicating pipe (17) between device for filtering impurities and spectrometer unit (1), the second communicating pipe (17) is provided with discharge pump (12); Supporting seat (32) is installed on the top of support (13), supporting seat (32) is arranged several initial bottle (33), the outlet of each initial bottle (33) each connects diverting valve (34) by management, the connection import (25) of diverting valve (34), the sidepiece of each initial bottle (33) all installs a fixed mount (35), fixed mount (35) is arranged electric push rod (37), the sidepiece of each initial bottle (33) arranges screening agent pipe (36), and the piston rod end of electric push rod (37) coordinates with screening agent pipe (36) inwall.
2. a kind of transformer oil gas multicomponent gas spectroanalysis instrument according to claim 1, it is characterized in that: between described spectrometer unit (1) and device for filtering impurities, de-watering apparatus is set, third connecting pipe (20) is set between de-watering apparatus and spectrometer unit (1), arranged T-valve (11) second communicating pipe (17), T-valve (11) connects one end of the first communicating pipe (16), and the other end of the first communicating pipe (16) connects de-watering apparatus; De-watering apparatus comprises base (8), upper installation two weighers (10) of base (8) and vacuum drainage cylinder (7), and two weighers (10) lay respectively at vacuum drainage cylinder (7) two ends, and weigher (10) is connected with vacuum drainage cylinder; Weigher (10) is made up of weighing cup (5) and electronic scale (6), and weighing cup (5) is fixedly mounted on the top of electronic scale (6); Vacuum drainage cylinder (10) comprises cylindrical shell, arranges heating rod (9) in cylindrical shell, and the top of cylindrical shell arranges gas-liquid separator (19), and gas-liquid separator (19) connects vacuum pump (18).
3. a kind of transformer oil gas multicomponent gas spectroanalysis instrument according to claim 1, it is characterized in that: described spectrometer unit (1) is arranged input keyboard (2), overturning seat (3) and display screen (4), display screen (4) is connected with spectrometer unit (1) by overturning seat (3).
CN201510878655.3A 2015-12-04 2015-12-04 A kind of transformer oil gas multicomponent gas spectroanalysis instrument Active CN105334169B (en)

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CN105334169B CN105334169B (en) 2018-02-06

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101281129B (en) * 2005-09-15 2011-06-15 聚光科技(杭州)股份有限公司 On-position type gas analysis system with on-position calibration function
WO2012032124A1 (en) * 2010-09-08 2012-03-15 Tecan Trading Ag Microplate-reader with a controlled gas atmosphere, corresponding method and use of same
CN102495006A (en) * 2011-11-22 2012-06-13 中国铝业股份有限公司 Method for detecting non-anode effect CF4
CN102585991A (en) * 2011-12-22 2012-07-18 北京盈胜泰科技术有限公司 Method and system for removing and supplying antioxidant from/to transformer insulating oil impurities
CN205139000U (en) * 2015-12-04 2016-04-06 国家电网公司 Transformer oil gas multicomponent gas spectral analysis appearance

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101281129B (en) * 2005-09-15 2011-06-15 聚光科技(杭州)股份有限公司 On-position type gas analysis system with on-position calibration function
WO2012032124A1 (en) * 2010-09-08 2012-03-15 Tecan Trading Ag Microplate-reader with a controlled gas atmosphere, corresponding method and use of same
CN102495006A (en) * 2011-11-22 2012-06-13 中国铝业股份有限公司 Method for detecting non-anode effect CF4
CN102585991A (en) * 2011-12-22 2012-07-18 北京盈胜泰科技术有限公司 Method and system for removing and supplying antioxidant from/to transformer insulating oil impurities
CN205139000U (en) * 2015-12-04 2016-04-06 国家电网公司 Transformer oil gas multicomponent gas spectral analysis appearance

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