CN105330913B - A kind of rubber compound - Google Patents
A kind of rubber compound Download PDFInfo
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- CN105330913B CN105330913B CN201510834018.6A CN201510834018A CN105330913B CN 105330913 B CN105330913 B CN 105330913B CN 201510834018 A CN201510834018 A CN 201510834018A CN 105330913 B CN105330913 B CN 105330913B
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- butyronitrile
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Abstract
The invention discloses a kind of rubber compound.The rubber compound includes:Auspicious father-in-law's butyronitrile DN4050 of 100 parts by weight;The vulcanizing agent of 3.5 parts by weight;The accelerating agent of 3.5 parts by weight;The activating agent of 6 parts by weight;The antioxidant of 3 parts by weight;The spraying carbon black of 70 parts by weight;The fine particle calcium carbonate of 25 parts by weight;The plasticizer of 20 parts by weight;The mould inhibitor of 5 parts by weight.The rubber compound of the present invention is using soft butyronitrile raw rubber as raw material, the hard butyronitrile raw rubber used in analysis original formulation and difference of the soft butyronitrile raw rubber in the properties such as molecular structure, composition distribution, molecular weight, molecular weight distribution, the degree of branching, gel content, the microstructure of butadiene short chain, segment distribution and rubber compound aspect of performance for intending use, best substitute kind is theoretically found out on the basis of comparative analysis, then by being formulated design, actual cooperation, being kneaded, vulcanization, the nitrile rubber performance finally prepared reaches original index request.
Description
Technical field
The present invention relates to aeronautical material manufacturing technology field, and in particular to a kind of rubber compound.
Background technology
Raw rubber is the main and key raw material of elastomeric material, and the performance of elastomeric material depends primarily upon raw rubber class used
Type.It can be divided to two kinds of high temperature polymerization and low temperature polymerization by polymerization technique, this depends primarily upon the initiator of selection reaction.High temperature gathers
The hard butyronitrile raw rubber closed generally forms distribution width, includes gel component height, and side chain is more, and Mooney viscosity is big, is needed when producing rubber compound
Repeatedly plasticated, poor in processability, machining energy consumption is huge, and foreign countries seldom apply in rubber.
Soft the butyronitrile raw rubber gel component and Mooney viscosity of low temperature polymerization are low, and microstructure regularity is high, average molecular matter
Measure narrowly distributing, it is not necessary to which plasticating can mixed refining process.
Domestic civilian nitrile rubber is from the 1980s substantially based on the soft butyronitrile of low temperature polymerization, but aviation is used
Nitrile rubber is since various aspects of performance problem, civilian nitrile rubber are unable to reach, and therefore, still mainly uses high temperature polymerization work
The hard butyronitrile raw rubber of skill production, hard butyronitrile raw rubber production technology seriously pollute environment, and hidden danger is continuous in terms of Environmental Safety.
Thus, it is desirable to have a kind of technical solution is come at least one above problem for overcoming or at least mitigating the prior art.
The content of the invention
It is an object of the invention to provide a kind of rubber compound come overcome or at least mitigate it is of the prior art it is at least one on
State problem.
To achieve the above object, the present invention provides a kind of rubber compound, the rubber compound to include:The auspicious father-in-law of 100 parts by weight
Butyronitrile DN4050;The vulcanizing agent of 3.5 parts by weight, the vulcanizing agent are peroxide and sulphur;The accelerating agent of 3.5 parts by weight;6 weight
The activating agent of part;The antioxidant of 3 parts by weight;The spraying carbon black of 70 parts by weight;The fine particle calcium carbonate of 25 parts by weight;The plasticising of 20 parts by weight
Agent, the plasticizer are dibutyl sebacate or di-n-octyl sebacate;The mould inhibitor of 5 parts by weight.
The rubber compound of the present invention is using soft butyronitrile raw rubber as raw material, and according to the purposes of aviation nitrile rubber, work bar
Part and index request, analyze the hard butyronitrile raw rubber used in original formulation with intending the soft butyronitrile raw rubber of use in molecular structure, composition
The raw rubbers such as distribution, molecular weight, molecular weight distribution, the degree of branching, gel content, the microstructure of butadiene short chain, segment distribution
Can and rubber compound aspect of performance difference, best substitute kind is theoretically found out on the basis of comparative analysis, then by with
Side's design, actual cooperation, be kneaded, vulcanization, and the nitrile rubber performance finally prepared reaches original index request.
Brief description of the drawings
Fig. 1 is the performance test figure of rubber compound according to a first embodiment of the present invention.
Fig. 2 is the heat aging performance Test Drawing of the rubber compound shown in Fig. 1.
Fig. 3 is the oil resistivity performance test figure of the rubber compound shown in Fig. 1.
Fig. 4 is the compression set performance test figure shown in Fig. 1.
Embodiment
To make the purpose, technical scheme and advantage that the present invention is implemented clearer, below in conjunction with the embodiment of the present invention
Attached drawing, the technical solution in the embodiment of the present invention is further described in more detail.In the accompanying drawings, identical from beginning to end or class
As label represent same or similar element or there is same or like element.Described embodiment is the present invention
Part of the embodiment, instead of all the embodiments.The embodiments described below with reference to the accompanying drawings are exemplary, it is intended to uses
It is of the invention in explaining, and be not considered as limiting the invention.Based on the embodiments of the present invention, ordinary skill people
Member's all other embodiments obtained without creative efforts, belong to the scope of protection of the invention.Under
Face is described in detail the embodiment of the present invention with reference to attached drawing.
In the description of the present invention, it is to be understood that term " " center ", " longitudinal direction ", " transverse direction ", "front", "rear",
The orientation or position relationship of the instruction such as "left", "right", " vertical ", " level ", " top ", " bottom " " interior ", " outer " is based on attached drawing institutes
The orientation or position relationship shown, is for only for ease of the description present invention and simplifies description, rather than instruction or the dress for implying meaning
Put or element there must be specific orientation, with specific azimuth configuration and operation, therefore it is not intended that the present invention is protected
The limitation of scope.
Fig. 1 is the performance test design sketch of rubber compound according to a first embodiment of the present invention.Fig. 2 is the mixing shown in Fig. 1
The heat aging performance test effect figure of glue.Fig. 3 is the oil resistivity performance test design sketch of the rubber compound shown in Fig. 1.Fig. 4 is Fig. 1
Shown compression set performance test design sketch.
The rubber compound of the present invention includes:Auspicious father-in-law's butyronitrile DN4050 of 100 parts by weight;The vulcanizing agent of 3.5 parts by weight;3.5 weight
Measure the accelerating agent of part;The activating agent of 6 parts by weight;The antioxidant of 3 parts by weight;The spraying carbon black of 70 parts by weight;25 parts by weight it is light
Calcium;The plasticizer of 20 parts by weight;The mould inhibitor of 5 parts by weight.
In the present embodiment, the vulcanizing agent is peroxide and sulphur.
In the present embodiment, the plasticizer is dibutyl sebacate or di-n-octyl sebacate.
The rubber compound of the present invention uses the more advanced soft butyronitrile raw rubber of environmental friendly, technology as raw material, according to boat
The purposes of empty nitrile rubber, operating condition and index request, it is soft with intending using to analyze the hard butyronitrile raw rubber used in original formulation
Butyronitrile raw rubber molecular structure, composition distribution, molecular weight, molecular weight distribution, the degree of branching, gel content, butadiene short chain it is micro-
The difference of the properties such as structure, segment distribution and rubber compound aspect of performance is seen, is theoretically found out on the basis of comparative analysis
Best substitute kind, then by being formulated design, actual cooperation, being kneaded, vulcanization, the nitrile rubber performance finally prepared reaches former
There is index request.
In Fig. 1 to Fig. 4, hard butyronitrile is the contrast butyronitrile of contrast.
It is last it is to be noted that:The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations.To the greatest extent
Pipe is with reference to the foregoing embodiments described in detail the present invention, it will be understood by those of ordinary skill in the art that:It is still
It can modify to the technical solution described in foregoing embodiments, or which part technical characteristic is equally replaced
Change;And these modifications or replacement, the essence of appropriate technical solution is departed from the essence of various embodiments of the present invention technical solution
God and scope.
Claims (1)
1. a kind of rubber compound, it is characterised in that the rubber compound includes:
Auspicious father-in-law's butyronitrile DN4050 of 100 parts by weight;
The vulcanizing agent of 3.5 parts by weight, the vulcanizing agent are peroxide and sulphur;
The accelerating agent of 3.5 parts by weight;
The activating agent of 6 parts by weight;
The antioxidant of 3 parts by weight;
The spraying carbon black of 70 parts by weight;
The fine particle calcium carbonate of 25 parts by weight;
The plasticizer of 20 parts by weight, the plasticizer are dibutyl sebacate or di-n-octyl sebacate;
The mould inhibitor of 5 parts by weight.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201510834018.6A CN105330913B (en) | 2015-11-24 | 2015-11-24 | A kind of rubber compound |
Applications Claiming Priority (1)
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CN201510834018.6A CN105330913B (en) | 2015-11-24 | 2015-11-24 | A kind of rubber compound |
Publications (2)
Publication Number | Publication Date |
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CN105330913A CN105330913A (en) | 2016-02-17 |
CN105330913B true CN105330913B (en) | 2018-04-13 |
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CN201510834018.6A Active CN105330913B (en) | 2015-11-24 | 2015-11-24 | A kind of rubber compound |
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Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
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JPWO2007026707A1 (en) * | 2005-08-31 | 2009-03-12 | 日本ゼオン株式会社 | Nitrile copolymer rubber cross-linked product, nitrile copolymer rubber composition, and method for producing the composition |
CN103012880A (en) * | 2012-11-30 | 2013-04-03 | 西安致泰橡塑工业有限公司 | High-strength oil-resistant rubber part for machinery |
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2015
- 2015-11-24 CN CN201510834018.6A patent/CN105330913B/en active Active
Non-Patent Citations (1)
Title |
---|
软丁腈橡胶的性能及其配合加工技术;李晓强;《第二届全国橡胶制品技术研讨会论文集》;20040810;第209-214页 * |
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CN105330913A (en) | 2016-02-17 |
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Effective date of registration: 20201030 Address after: Building B, building 28, Jiangsu information service industry base, Guangling New Town, Yangzhou City, Jiangsu Province, 225002 Patentee after: Shenyang Aircraft Design Institute Yangzhou Collaborative Innovation Research Institute Co., Ltd Address before: Thavorn street in Huanggu District of Shenyang city of Liaoning Province, No. 40 110035 Patentee before: SHENYANG AIRCRAFT DESIGN INSTITUTE, AVIATION INDUSTRY CORPORATION OF CHINA |
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