CN105327520B - Feeding and heating system of alcohol recovery tower - Google Patents

Feeding and heating system of alcohol recovery tower Download PDF

Info

Publication number
CN105327520B
CN105327520B CN201510701968.1A CN201510701968A CN105327520B CN 105327520 B CN105327520 B CN 105327520B CN 201510701968 A CN201510701968 A CN 201510701968A CN 105327520 B CN105327520 B CN 105327520B
Authority
CN
China
Prior art keywords
feeding
channel
spiral
heat exchanger
passage
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201510701968.1A
Other languages
Chinese (zh)
Other versions
CN105327520A (en
Inventor
吕西军
陈超
纵鑫
姚东烨
党钰
王洪新
陈刚
马鹏举
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SUZHOU WANSHENMIAN PRODUCT Co Ltd
Original Assignee
SUZHOU WANSHENMIAN PRODUCT Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SUZHOU WANSHENMIAN PRODUCT Co Ltd filed Critical SUZHOU WANSHENMIAN PRODUCT Co Ltd
Priority to CN201510701968.1A priority Critical patent/CN105327520B/en
Publication of CN105327520A publication Critical patent/CN105327520A/en
Application granted granted Critical
Publication of CN105327520B publication Critical patent/CN105327520B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/02Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The invention provides a feeding and heating system of an alcohol recovery tower. The feeding and heating system comprises a first spiral plate heat exchanger, a feeding channel and a distillation still. The first spiral plate heat exchanger is arranged in the top layer of the recovery tower and comprises a first channel and a second channel. An inlet of the first channel penetrates through the tower wall and is connected with an outside low-concentration alcohol source. An outlet of the first channel is connected with an inlet of the feeding channel. An outlet of the feeding channel is connected with a feeding port of the distillation still. An inlet of the second channel is connected with a tower tray in the top layer of the recovery tower. An outlet of the second channel is located in the top layer. Compared with the prior art, the heat of alcohol steam in the top layer of the recover tower is used for heat exchange with low-concentration alcohol, waste heat of condensate discharged out of the distillation still is used for heating the low-concentration alcohol, and alcohol vapor can be liquidized; the waste heat of the condensate can be recycled, the temperature of the low-concentration alcohol can also be increased, and the steam using amount of the distillation still can be reduced.

Description

A kind of charging heating system of alcohol distillation column
Technical field
The present invention relates to ethanol processing technique field, a kind of specifically light wine recovery system.
Background technology
The alcohol distillation column for using in industries such as pharmacy, food, light industry, chemical industry at present is typically mainly stored up by tower body, a high position Tank, condenser, cooler composition.The light wine for needing to reclaim is prevented the heating volatilization in distillating still by which, after tower body rectification, The alcohol gas of high concentration are separated out, in gas uphill process, temperature is gradually reduced makes part ethanol produce backflow.Finally enter The alcohol gas of tower top generally require introducing low-temperature receiver lowers the temperature to which condenses which.Process is loaded down with trivial details, and consumes energy.
Distillating still can produce a large amount of vapor condensed waters when distilling to light wine, and vapor condensed water temperature is higher, such as not secondary profit With, it will very big energy loss is caused, certain pollution also can be caused to environment.
The content of the invention
The invention aims to solve the big defect that consumes energy in thin alcohol recovery tower in prior art, there is provided a kind of The charging heating system of alcohol distillation column is solving the above problems.
Invention is to be achieved through the following technical solutions above-mentioned technical purpose:
A kind of charging heating system of alcohol distillation column, including the first spiral-plate heat exchanger, feeding-passage, distillating still;Institute State the first spiral-plate heat exchanger to be arranged in recovery tower top layer;First spiral-plate heat exchanger includes that first passage, second are led to Road;The import of the first passage is connected through tower wall with extraneous light wine source;The outlet of the first passage and feeding-passage Import connects;The outlet of the feeding-passage is connected with the charging aperture of the distillating still;The import of the second channel with it is described The column plate alcohol steam import connection of recovery tower top layer;The outlet of the second channel is in top layer.
Preferably, the system also includes secondary spiral lamina heat exchanger;Secondary spiral lamina heat exchanger include third channel, Four-way;The import of the third channel is connected with the outlet of the feeding-passage;The outlet of the third channel and the steaming Evaporate the charging aperture connection of kettle;The distillating still includes that vapor condensed water is exported;The vapour of the import of the fourth lane and the distillating still Solidifying water out connection.
Preferably, the recovery tower top layer is divided into the first chamber and the second chamber by dividing plate;The ethanol of the recovery tower top layer steams Vapor inlet is in the second intracavity;First spiral-plate heat exchanger is in the first intracavity;The of first spiral-plate heat exchanger Two imports are connected through dividing plate with the alcohol steam import of the second intracavity;The second outlet of first spiral-plate heat exchanger is passed through Dividing plate is in the second intracavity.
Further, the feeding-passage part is connected through recovery tower top layer tower wall with first spiral-plate heat exchanger Connect;Another is connected with secondary spiral lamina heat exchanger outside recovery tower.
Preferably, the feed pipe is externally provided with heat-insulation layer.
Preferably, the feeding-passage is provided with sealing member through at the tower wall.
The present invention compared with prior art, with advantages below:
1., using the heat of recovery tower top layer alcohol steam, heat exchange is carried out with light wine, and using distillating still discharge The waste heat of vapor condensed water is heated to light wine, can be alcohol steam liquefaction;Vapor condensed water waste heat can recycle again, moreover it is possible to improve The temperature of light wine, reduces the steam consumption of distillating still;
2. the first spiral-plate heat exchanger and alcohol steam are separated by the design of two cavitys of recovery tower top layer, it is ensured that ethanol The cleaning of steam.
3. feeding-passage is arranged on outside recovery tower, without the need for every layer of tray revamping of recovery tower, simple to operation.
Description of the drawings
Fig. 1 is a kind of structural representation of the charging heating system of alcohol distillation column of the invention;
Fig. 2 is the axial section of feeding-passage in Fig. 1;
Fig. 3 is feeding-passage in Fig. 1 through the profile reclaimed at tower wall.
Specific embodiment
To make architectural feature and the effect reached to the present invention have a better understanding and awareness, to preferably Embodiment and accompanying drawing coordinate detailed description, are described as follows:
As shown in figure 1, a kind of charging heating system of alcohol distillation column, including the first spiral-plate heat exchanger 1, the second spiral Sheet heat exchanger 2, feeding-passage 3, distillating still 4.
First spiral-plate heat exchanger 1 is arranged in recovery tower top layer;First spiral-plate heat exchanger 1 include first passage, Two passages.The import of first passage is connected through tower wall with extraneous light wine source.The outlet of first passage and the import of feeding-passage 3 Connection.The outlet of feeding-passage 3 is connected with the charging aperture of distillating still 4.The import of second channel and the column plate wine of recovery tower top layer Smart steam inlet connection;The outlet of second channel is inside top layer.
Secondary spiral lamina heat exchanger 2 includes third channel, fourth lane.The import of third channel is gone out with feeding-passage 3 Mouth connection.The outlet of third channel is connected with the charging aperture of distillating still 4.Distillating still 4 includes that vapor condensed water is exported, and fourth lane is entered Mouth is connected with the vapor condensed water outlet of distillating still 4.
In order that alcohol steam cleaning is not contaminated, recovery tower top layer is the by 5 points of dividing plate by the system that the present invention is provided One chamber and the second chamber.The alcohol steam import of recovery tower top layer is in the second intracavity;First spiral-plate heat exchanger 1 is in the first chamber It is interior.Second import of the first spiral-plate heat exchanger 1 is connected through dividing plate 5 with the alcohol steam import of the second intracavity.First spiral The second outlet of sheet heat exchanger 1 is in the second intracavity through dividing plate 5.
In order to not change the structure of original recovery tower column plate, 3 part of feeding-passage is passed through by the system that the present invention is provided Recovery tower top layer tower wall is connected with the first spiral-plate heat exchanger 1;Another is connected with secondary spiral lamina heat exchanger 2 outside recovery tower Connect.
As shown in Figure 2 and Figure 3, heat-insulation layer 8 can be externally provided with feed pipe, and is set through at tower wall in feeding-passage 3 There is sealing member 6.So that light wine heat in the feeding-passage 3 does not lose, sealing member 6 can by inside recovery tower top layer with it is outside very Good isolation, to ensure the cleaning of ethanol.
In specific works, light wine source 7 is input into weak liquor to the first spiral-plate heat exchanger 1, while the second chamber is to the first spiral Sheet heat exchanger 1 is input into alcohol steam, and the two completes heat exchange in the first spiral-plate heat exchanger 1, and alcohol steam liquefaction flows into the Two intracavity, weak liquor flow to secondary spiral lamina heat exchanger 2 by feeding-passage 3 after heating up.Distillating still 4 exchanges heat to secondary spiral lamina Device 2 supplies vapor condensed water.In secondary spiral lamina heat exchanger 2, post bake is completed with vapor condensed water through the weak liquor of first preheating. After heat exchange is completed in secondary spiral lamina heat exchanger 2, arrange outside vapor condensed water or recycle, weak liquor flow in distillating still 4 after It is continuous to carry out heat exchange to design temperature with steam.The vaporized alcohol reached in the weak liquor after design temperature is input into recovery tower. So far, complete the whole circulation of light wine charging heating.
Ultimate principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry The simply present invention of the personnel it should be appreciated that the present invention is not restricted to the described embodiments, described in above-described embodiment and description Principle, without departing from the spirit and scope of the present invention the present invention also have various changes and modifications, these change and Improvement is both fallen within the range of claimed invention.The protection domain of application claims by appending claims and its Equivalent is defined.

Claims (6)

1. the charging heating system of a kind of alcohol distillation column, it is characterised in that:The feed system includes that the first spiral lamina exchanges heat Device, feeding-passage, distillating still;First spiral-plate heat exchanger is arranged in recovery tower top layer;The first spiral lamina heat exchange Device includes first passage, second channel;The import of the first passage is connected through tower wall with extraneous light wine source;Described first leads to The outlet in road is connected with the import of feeding-passage;The outlet of the feeding-passage is connected with the charging aperture of the distillating still;It is described The import of second channel is connected with the column plate alcohol steam import of the recovery tower top layer;The outlet of the second channel is in top In layer.
2. the charging heating system of a kind of alcohol distillation column according to claim 1, it is characterised in that:The system is also wrapped Include secondary spiral lamina heat exchanger;Secondary spiral lamina heat exchanger includes third channel, fourth lane;The import of the third channel with The outlet connection of the feeding-passage;The outlet of the third channel is connected with the charging aperture of the distillating still;The distillating still Export including vapor condensed water;The import of the fourth lane is connected with the vapor condensed water outlet of the distillating still.
3. the charging heating system of a kind of alcohol distillation column according to claim 2, it is characterised in that:The recovery tower top Layer is divided into the first chamber and the second chamber by dividing plate;The alcohol steam import of the recovery tower top layer is in the second intracavity;Described first Spiral-plate heat exchanger is in the first intracavity;Second import of first spiral-plate heat exchanger passes through the wine of dividing plate and the second intracavity Smart steam inlet connection;The second outlet of first spiral-plate heat exchanger is in the second intracavity through dividing plate.
4. the charging heating system of a kind of alcohol distillation column according to claim 2, it is characterised in that:The feeding-passage A part is connected through recovery tower top layer tower wall with first spiral-plate heat exchanger;Another is in outside recovery tower and the second spiral shell Spiral plate exchanger connects.
5. the charging heating system of a kind of alcohol distillation column according to claim 1, it is characterised in that:The feed pipe It is externally provided with heat-insulation layer.
6. the charging heating system of a kind of alcohol distillation column according to claim 4, it is characterised in that:The feeding-passage Sealing member is provided with through at the tower wall.
CN201510701968.1A 2015-10-23 2015-10-23 Feeding and heating system of alcohol recovery tower Active CN105327520B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510701968.1A CN105327520B (en) 2015-10-23 2015-10-23 Feeding and heating system of alcohol recovery tower

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510701968.1A CN105327520B (en) 2015-10-23 2015-10-23 Feeding and heating system of alcohol recovery tower

Publications (2)

Publication Number Publication Date
CN105327520A CN105327520A (en) 2016-02-17
CN105327520B true CN105327520B (en) 2017-05-03

Family

ID=55278408

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510701968.1A Active CN105327520B (en) 2015-10-23 2015-10-23 Feeding and heating system of alcohol recovery tower

Country Status (1)

Country Link
CN (1) CN105327520B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112741217B (en) * 2019-10-30 2022-12-20 国投生物科技投资有限公司 Fuel ethanol distillation dehydration device and preparation method of distiller's dried grain protein feed

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3481835A (en) * 1967-10-05 1969-12-02 Gen Electric Multiple effect distillation apparatus
CN101857202B (en) * 2010-06-04 2012-01-25 黎明化工研究院 Purification method of sulfur hexafluoride and equipment thereof
CN102059042B (en) * 2010-10-30 2012-10-24 陈群 Combination unit for multilevel heat exchange and gas liquid separation
CN205084434U (en) * 2015-10-23 2016-03-16 宿州市皖神面制品有限公司 Feeding heating system of alcohol recovery tower

Also Published As

Publication number Publication date
CN105327520A (en) 2016-02-17

Similar Documents

Publication Publication Date Title
CN105000612B (en) Mechanical vapor recompression system of concentrated organic waste water and method
CN204034294U (en) The board-like forced-circulation evaporator of novel triple effect
CN104922974B (en) A kind of concentration device for material liquid
CN104986910A (en) Mechanical steam recompression falling film evaporation process method and system
CN207187150U (en) A kind of energy-saving distillation recovery device
CN107812393A (en) A kind of methanol three-effect rectification system and technique
CN102602960B (en) Method for stilling ammonia by aid of waste heat of flue gas of coke oven and equipment
CN102249203A (en) Phosphoric acid evaporation process and device thereof
CN205730432U (en) A kind of mechanical steam recompression Distallation systm
CN105327520B (en) Feeding and heating system of alcohol recovery tower
CN106512458A (en) Distillation system for sugar industry factory
CN204824504U (en) Machinery vapor recompression falling film evaporation process systems
CN105669380B (en) The ethylene glycol recyclable device and ethylene glycol recovery method of polyester waste water recovery system
CN106809896B (en) A kind of organic wastewater treating system and method
CN205084434U (en) Feeding heating system of alcohol recovery tower
CN204176663U (en) A kind of process waste reclaims energy conserving system
CN207031178U (en) Sewage recorery treatment system
CN209383437U (en) A kind of ammonia-containing water exhaust gas treating tower
CN104892358A (en) Ethanol recovery tower heat exchange technology
CN203017795U (en) Efficient distillation reboiler
CN108854456B (en) System and method for recycling heat energy of desorption tower
CN104524789A (en) Single-effect concentrated alcohol recovering apparatus
CN106186132A (en) Low cost power plant zeroth order value waste water evaporation and concentration processing system and method
CN205730418U (en) A kind of economic benefits and social benefits external-circulation concentrating device of efficient recovery organic solvent
CN105817046A (en) Reduced pressure multi-effect glass evaporator system

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: Feeding and heating system of alcohol recovery tower

Effective date of registration: 20181129

Granted publication date: 20170503

Pledgee: Suzhou Longqiao Branch of Huizhou Commercial Bank Co.,Ltd.

Pledgor: SUZHOU WANSHEN FLOUR PRODUCT CO.,LTD.

Registration number: 2018340000687

PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20191209

Granted publication date: 20170503

Pledgee: Suzhou Longqiao Branch of Huizhou Commercial Bank Co.,Ltd.

Pledgor: SUZHOU WANSHEN FLOUR PRODUCT CO.,LTD.

Registration number: 2018340000687

PC01 Cancellation of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: Feeding and heating system of alcohol recovery tower

Effective date of registration: 20191224

Granted publication date: 20170503

Pledgee: Suzhou Longqiao Branch of Huizhou Commercial Bank Co.,Ltd.

Pledgor: SUZHOU WANSHEN FLOUR PRODUCT CO.,LTD.

Registration number: Y2019980001248

PC01 Cancellation of the registration of the contract for pledge of patent right
PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20210707

Granted publication date: 20170503

Pledgee: Suzhou Longqiao Branch of Huizhou Commercial Bank Co.,Ltd.

Pledgor: SUZHOU WANSHEN FLOUR PRODUCT Co.,Ltd.

Registration number: Y2019980001248

PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: A feed heating system for alcohol recovery tower

Effective date of registration: 20220214

Granted publication date: 20170503

Pledgee: China Construction Bank Corporation Suzhou Branch

Pledgor: SUZHOU WANSHEN FLOUR PRODUCT CO.,LTD.

Registration number: Y2022980001489

PC01 Cancellation of the registration of the contract for pledge of patent right
PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20230915

Granted publication date: 20170503

Pledgee: China Construction Bank Corporation Suzhou Branch

Pledgor: SUZHOU WANSHEN FLOUR PRODUCT CO.,LTD.

Registration number: Y2022980001489