CN105300845B - Bitumen regenerant diffusion test device and method of testing - Google Patents

Bitumen regenerant diffusion test device and method of testing Download PDF

Info

Publication number
CN105300845B
CN105300845B CN201510897570.XA CN201510897570A CN105300845B CN 105300845 B CN105300845 B CN 105300845B CN 201510897570 A CN201510897570 A CN 201510897570A CN 105300845 B CN105300845 B CN 105300845B
Authority
CN
China
Prior art keywords
pitch
bitumen
mrow
msub
regenerative agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201510897570.XA
Other languages
Chinese (zh)
Other versions
CN105300845A (en
Inventor
易军艳
许勐
冯德成
周长俊
王东升
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Harbin Institute of Technology
Original Assignee
Harbin Institute of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Harbin Institute of Technology filed Critical Harbin Institute of Technology
Priority to CN201510897570.XA priority Critical patent/CN105300845B/en
Publication of CN105300845A publication Critical patent/CN105300845A/en
Application granted granted Critical
Publication of CN105300845B publication Critical patent/CN105300845B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Abstract

Bitumen regenerant diffusion test device and method of testing, the present invention relates to bitumen regenerant diffusion evaluate experimental rig and its application process, it in order to solve at present not yet have bitumen regenerant spread related experiment device and evaluation method not enough efficiently accurately problem.The experimental rig includes dissolving bucket, holds sample ware, collection device, feed tube and drain pipe.Method of testing is first to carry out stewing process to the bitumen samples for adding regenerative agent, bitumen samples are weighed and measured with the height of sample, add trichloro ethylene and carry out pitch cleaning, then repeated washing process is multiple, measure four components of discharge liquor solid formation, regenerative agent relative amount is calculated, then regenerative agent diffusion rate is obtained by diffusion depth.Present invention utilizes the trichloro ethylene characteristic big to the dissolubility of pitch, the bitumen samples handled by regenerative agent are progressively dissolved using the method for layering dissolving, then the diffusion property of regenerative agent analyzed according to the composition analysis result of solution after dissolving.

Description

Bitumen regenerant diffusion test device and method of testing
Technical field
The present invention relates to the experimental rig and its application process that bitumen regenerant diffusion is evaluated.
Background technology
The Large scale construction of highway in China will trace back to eighties of last century the mid-80, by the construction in more than 30 years, arrive 2015, highway in China total kilometrage reached more than 450 ten thousand kilometers, and wherein highway reaches 10.8 ten thousand kilometers, wherein 80% is drip Blue or green concrete road surface.Till now, there are a considerable amount of bituminous pavings to reach service life, be faced with extensive maintenance dimension Repair or even rebuild.In addition, continuing to develop with China Transportation Industry, the volume of traffic and vehicular load increase rapidly make it is newly-built Highway has just had been subjected to a certain degree of damage in a short time, needs the necessary maintenance work of progress badly to extend making for road Use the life-span.In general, China's road life is not generally long, builds and completes to be accomplished by carrying out regular maintenance in the near future.But at present Highway in China build nutrient from general layout still have, and be still difficult to solve, how by the theory of life cycle management through highway Construction, maintenance and operation in, have become one urgent problem to be solved of highway industry.
For newly-built bituminous paving, in the presence of temperature and oxygen, asphalt material is in pressure of mixing and stirring, transport and pave A certain degree of short ageing can occur during reality, although this process duration is very short, the generation to asphalt performance Huge destruction, has research to think that the needle penetration after short ageing is only the 60%-75% of original value.And the newly-built drip after being compacted Blue or green road surface, surface void is not blocked also, therefore with certain permeability.Before being open to traffic, large quantity of air and water penetration are arrived Newly-built bituminous paving, can also accelerate the aging of new pavement.
For old asphalt pavement, in the influence of the extraneous factors such as ultraviolet radiation, high-temperature oxydation, water erosion, traffic wear Under, pitch is persistently aging, and then triggers the pavement diseases such as fatigue cracking, pit.This long-term ageing process can continue to weaken The performance of bituminous paving.
Bitumen regenerant mainly use petroleum refining material, its application purpose be mainly regulation and improve asphalt material due to The component that the newly-built short ageing of road or old road long-term ageing are caused is unbalance, the design performance of fast quick-recovery bituminous paving. So as to repair the asphalt pavement material of aging, improve road surface outward appearance and performance, delay bituminous paving ager process, prolonged with reaching Long service life of road surface, reduces the purpose of maintenance cost.
Because current regenerative agent product is by actual verification for many years, the ability of its " softening " aged asphalt will not be deposited substantially In problem, however, can regenerative agent diffusion but have emphatically into pitch to the recovery situation of bituminous pavement property well The influence wanted, it may be said that regenerative agent regeneration effect is heavily dependent on the height of diffusion degree.As regenerative agent is spilt The change of the factors such as cloth amount, time of penetration, asphalt mixture porosity, fracture spacing so that its penetration depth is differed. The road surface of China is mostly closely knit fluid-tight, and after the rolling repeatedly of vehicle surface become more closely knit, under ooze Effect is relatively weak.Thus regeneration mist sealing can play preferable palingenesis in a long time, main still by again The diffusion of raw agent.Therefore generally believe that can regenerative agent (including regeneration agent material for cold and hot regeneration) in the world at present Playing the influence depth of " regeneration " effect and regenerative agent well has important relation, therefore the research of regenerative agent diffusion problem is It is highly desirable to, and is significantly.
But not yet there is the experimental provision and means of correlation to analyze regenerative agent diffusion process and rule at present, it is basic herein It is upper to need to develop a set of experimental rig and its application method for diffusion test for correlative study.
The content of the invention
The invention aims to the related experiment device for solving not yet to have bitumen regenerant to spread at present and evaluation side Not efficiently accurate enough the problem of method, and bitumen regenerant diffusion test device and method of testing are provided.
Bitumen regenerant diffusion test device of the present invention includes dissolving cylinder, holds sample ware, collection device, feed tube and go out liquid Pipe, dissolving cylinder forms tubular by barrel and cylinder bottom, is provided with opening at the center at cylinder bottom, the thickness edge at cylinder bottom dissolve the radial direction of cylinder by Be as thin as it is thick form the gradient, drain pipe is communicated with opening, and collection device is located at the lower section of drain pipe, one end of " L " shape feed tube and Drain pipe is connected, and the other end opening of feed tube is provided with valve on feed tube and drain pipe, holds sample as inlet Ware is located at the bottom of dissolving cylinder in shallow disc shape.
The dissolving cylinder of bitumen regenerant diffusion test device of the present invention is used to hold to hold sample ware and trichloro ethylene solution, its bottom Portion slightly has the gradient, to facilitate the trichloro ethylene of inside all to discharge, prevents pitch from residuing in dissolving cylinder bottom to tie experiment Fruit impacts.The bottom center opening of cylinder, connection feed tube and drain pipe are dissolved, sample ware is held for shallow disc shape, for holding drip Blue or green sample.There is switch on feed tube and drain pipe, for controlling trichloro ethylene to pass in and out.Standard (acidity) drop is connect at the top of feed tube Fixed tube.In order to prevent asphalt sample from being washed away by the uneven of trichloro ethylene, feed tube is arranged on the bottom of dissolving cylinder, drain pipe Place solution collection device in bottom.
The method that present invention application bitumen regenerant diffusion test device is tested is realized according to the following steps:
First, pour into and held in sample ware after pitch is heated, be then placed in baking oven and be dried to pitch levelling, obtain filling pitch Hold sample ware;
2nd, to fill pitch hold in sample ware add regenerative agent or regeneration mist sealing material, make regenerative agent or regeneration mist envelope Layer material is uniformly covered with the surface of pitch, obtains testing bitumen samples;
3rd, the test bitumen samples for obtaining step 2 carry out stewing process TdiffHour, obtain filling bitumen samples Hold sample ware;
4th, the sample ware that holds for filling bitumen samples is weighed, is designated as G0, and the upper surfaces of bitumen samples is measured away from holding on sample ware The height at edge is H0, it is then placed into dissolving cylinder, the valve closed on drain pipe opens the valve on feed tube, Xiang Jin Trichloro ethylene is added in liquid pipe, trichloro ethylene was flooded the upper surface of bitumen samples, the volume of record trichloro ethylene is V ml, The valve closed after standing on feed tube, opens the valve on drain pipe, collects discharge liquor, is taken out from dissolving cylinder and holds sample ware, Weighed after drying, be designated as G1, now the upper surface of bitumen samples away from hold sample ware top edge height be H1, complete a pitch clear Wash;
5th, the pitch cleaning process of repeat step four repeatedly, weighed after the cleaning of each pitch fill bitumen samples hold sample The weight of ware is Gk, the weight for holding sample ware that bitumen samples are filled after preceding pitch cleaning is Gk-1, dripped after each pitch cleaning The upper surface of blue or green sample away from hold sample ware top edge height be Hk, the upper surface of bitumen samples is away from holding sample after the cleaning of a preceding pitch The height of ware top edge is Hk-1, so that obtaining kth time washes out the quality of pitch for mk=Gk-1-Gk, unit is g, and kth time is washed The thickness of the pitch gone out is hk=Hk-Hk-1, unit is mm, while making three chloroethenes under the discharge liquor normal temperature condition collected to kth time Alkene volatilizees completely, four component tests is then carried out to solid formation, i.e., the solid formation saturation point percentage of test kth time discharge contains respectively Measure Sk, fragrance point percentage composition Pk, colloid percentage composition Rk, asphalitine percentage composition Ak
6th, the regenerative agent relative amount F of kth time discharge is calculated as followsk
7th, as the regenerative agent relative amount F for occurring the m times discharge firstmWith the regenerative agent relative amount of the m+1 times discharge Fm+1Difference then reflects that regenerative agent diffuses to m-1 layers when being no more than 10%, then regenerative agent diffusion depth HdiffFor:
8th, regenerative agent diffusion rate D, unit are calculated as follows:Mm/h, calculation formula is:
Wherein TdiffFor diffusion time, the diffusion test test of completion bitumen regenerant.
, will be by again using the method for layering dissolving present invention utilizes the trichloro ethylene characteristic big to the dissolubility of pitch The bitumen samples of raw agent processing progressively dissolve, then according to diffusion property of the composition analysis result of solution after dissolving to regenerative agent Analyzed.This method tested using bitumen regenerant diffusion test device can accurately determine regenerative agent Diffusion rate, can be applied to the research field of regenerative agent regeneration effect.
Brief description of the drawings
Fig. 1 is the structural representation of bitumen regenerant diffusion test device of the present invention.
Embodiment
Embodiment one:Present embodiment bitumen regenerant diffusion test device includes dissolving cylinder 1, holds sample ware 2, receipts Acquisition means 8, feed tube 3 and drain pipe 4, dissolving cylinder 1 form tubular by barrel and cylinder bottom, and opening 9, cylinder are provided with the center at cylinder bottom Radial direction of the thickness at bottom along dissolving cylinder 1 forms the gradient by being as thin as thickness, and drain pipe 4 is communicated with opening 9, and collection device 8 is located at liquid The lower section of pipe 4, one end of " L " shape feed tube 3 is connected with drain pipe 4, and the other end of feed tube 3 is open as inlet, Valve 7 is provided with feed tube 3 and drain pipe 4, the bottom that sample ware 2 is located at dissolving cylinder 1 in shallow disc shape is held.
Embodiment two:Present embodiment and dissolving cylinder 1 described unlike embodiment one, hold sample ware 2nd, the material of collection device 8, feed tube 3 and drain pipe 4 is metal material.
Embodiment three:Present embodiment is stainless from metal material described unlike embodiment two Steel or aluminium alloy.
Embodiment four:The thickness edge at cylinder bottom unlike one of present embodiment and embodiment one to three The radial direction for dissolving cylinder forms the gradient by being as thin as thickness, and the slope angle of the gradient is 5 °~10 °.
Embodiment five:In feed tube 3 unlike one of present embodiment and embodiment one to four Acid burette is provided with above inlet.
Embodiment six:Unlike one of present embodiment and embodiment one to five in feed tube 3 Footpath is 3~5mm.
The feed tube of present embodiment should not be excessively thick, prevents too fast flow velocity from causing the turbulent flow of sample surfaces, so that sample Trichloro ethylene can not be uniformly dissolved in.Also it is unsuitable meticulous, otherwise influence test speed.
Embodiment seven:The method that present embodiment application bitumen regenerant diffusion test device is tested by with Lower step is realized:
First, pour into and held in sample ware after pitch is heated, be then placed in baking oven and be dried to pitch levelling, obtain filling pitch Hold sample ware;
2nd, to fill pitch hold in sample ware add regenerative agent or regeneration mist sealing material, make regenerative agent or regeneration mist envelope Layer material is uniformly covered with the surface of pitch, obtains testing bitumen samples;
3rd, the test bitumen samples for obtaining step 2 carry out stewing process TdiffHour, obtain filling bitumen samples Hold sample ware;
4th, the sample ware that holds for filling bitumen samples is weighed, is designated as G0, and the upper surfaces of bitumen samples is measured away from holding on sample ware The height at edge is H0, it is then placed into dissolving cylinder, the valve closed on drain pipe opens the valve on feed tube, Xiang Jin Trichloro ethylene is added in liquid pipe, trichloro ethylene was flooded the upper surface of bitumen samples, the volume of record trichloro ethylene is V ml, The valve closed after standing on feed tube, opens the valve on drain pipe, collects discharge liquor, is taken out from dissolving cylinder and holds sample ware, Weighed after drying, be designated as G1, now the upper surface of bitumen samples away from hold sample ware top edge height be H1, complete a pitch clear Wash;
5th, the pitch cleaning process of repeat step four repeatedly, weighed after the cleaning of each pitch fill bitumen samples hold sample The weight of ware is Gk, the weight for holding sample ware that bitumen samples are filled after preceding pitch cleaning is Gk-1, dripped after each pitch cleaning The upper surface of blue or green sample away from hold sample ware top edge height be Hk, the upper surface of bitumen samples is away from holding sample after the cleaning of a preceding pitch The height of ware top edge is Hk-1, so that obtaining kth time washes out the quality of pitch for mk=Gk-1-Gk, unit is g, and kth time is washed The thickness of the pitch gone out is hk=Hk-Hk-1, unit is mm, while making three chloroethenes under the discharge liquor normal temperature condition collected to kth time Alkene volatilizees completely, four component tests is then carried out to solid formation, i.e., the solid formation saturation point percentage of test kth time discharge contains respectively Measure Sk, fragrance point percentage composition Pk, colloid percentage composition Rk, asphalitine percentage composition Ak
6th, the regenerative agent relative amount F of kth time discharge is calculated as followsk
7th, as the regenerative agent relative amount F for occurring the m times discharge firstmWith the regenerative agent relative amount of the m+1 times discharge Fm+1Difference then reflects that regenerative agent diffuses to m-1 layers when being no more than 10%, then regenerative agent diffusion depth HdiffFor:
8th, regenerative agent diffusion rate D, unit are calculated as follows:Mm/h, calculation formula is:
Wherein TdiffFor diffusion time, the diffusion test test of completion bitumen regenerant.
Bitumen samples 5 are placed in by present embodiment holds sample ware 2, and trichloro ethylene 6 flooded the upper surface of bitumen samples 5.Step If rapid seven are not present such m values, illustrate that regenerative agent diffusion rate is too fast, test should be re-started, and shorten step 3 Processing time.
Present embodiment according to《Highway engineering pitch and Asphalt Mixture Experiment code》In (JTG E20-2011) The discharge liquor sample that the constituent test methods of T0618-1993 tetra- are obtained to step 5 carries out four constituent tests respectively.Add regeneration Before agent test pitch upper surface away from hold sample ware top edge height be 1~3mm.
Embodiment eight:Present embodiment from unlike embodiment seven when step 2 is to filling pitch When holding addition regenerative agent in sample ware, step 3 is that test bitumen samples are stood into T at room temperaturediffTime be 45~96h.Its Its step and parameter are identical with embodiment seven.
Embodiment nine:Present embodiment from unlike embodiment seven when step 2 is to filling pitch When holding addition regeneration mist sealing material in sample ware, step 3 is that test bitumen samples are stood into T in 120 DEG C of baking ovendifff's Time is 2~5 hours.Other steps and parameter are identical with embodiment seven.
Embodiment:The method that the present embodiment application bitumen regenerant diffusion test device is tested is real according to the following steps It is existing:
First, pour into and held in sample ware after Anda 90# pitches are heated, be then placed in baking oven and be dried to pitch levelling, contained Have pitch holds sample ware;
2nd, regenerative agent is added in sample ware to filling holding for pitch, sample ware is held in rotation makes regenerative agent uniformly be covered with pitch Surface, obtains testing bitumen samples;
3rd, the test bitumen samples for obtaining step 2 carry out stewing process Tdiff=48 hours, obtain filling pitch examination Sample holds sample ware;
4th, the sample ware that holds for filling bitumen samples is weighed, is designated as G0=26.32g, and measure the upper surfaces of bitumen samples away from The height for holding sample ware top edge is H0=0.86mm, is then placed into dissolving cylinder, and the valve closed on drain pipe opens feed liquor Valve on pipe, trichloro ethylene is added into feed tube, trichloro ethylene was flooded the upper surface of bitumen samples, records three chloroethenes The volume of alkene is V ml, the valve closed on feed tube after standing, opens the valve on drain pipe, discharge liquor is collected, from dissolving Taken out in cylinder and hold sample ware, weighed after drying, be designated as G1=25.74g, now the upper surface of bitumen samples is away from holding sample ware top edge Highly it is H1, complete a pitch cleaning;
5th, the pitch cleaning process of repeat step four repeatedly, weighed after the cleaning of each pitch fill bitumen samples hold sample The weight of ware is Gk, the weight for holding sample ware that bitumen samples are filled after preceding pitch cleaning is Gk-1, dripped after each pitch cleaning The upper surface of blue or green sample away from hold sample ware top edge height be Hk, the upper surface of bitumen samples is away from holding sample after the cleaning of a preceding pitch The height of ware top edge is Hk-1, so that obtaining kth time washes out the quality of pitch for mk=Gk-1-Gk, unit is g, and kth time is washed The thickness of the pitch gone out is hk=Hk-Hk-1, unit is mm, while making three chloroethenes under the discharge liquor normal temperature condition collected to kth time Alkene volatilizees completely, four component tests is then carried out to solid formation, i.e., the solid formation saturation point percentage of test kth time discharge contains respectively Measure Sk, fragrance point percentage composition Pk, colloid percentage composition Rk, asphalitine percentage composition Ak
6th, the regenerative agent relative amount F of kth time discharge is calculated as followsk
7th, as the regenerative agent relative amount F for occurring the m times discharge firstmWith the regenerative agent relative amount of the m+1 times discharge Fm+1Difference then reflects that regenerative agent diffuses to m-1 layers when being no more than 10%, then regenerative agent diffusion depth HdiffFor:
8th, regenerative agent diffusion rate D, unit are calculated as follows:Mm/h, calculation formula is:
Wherein TdiffFor diffusion time, the diffusion test test of completion bitumen regenerant.
The specific test data of the present embodiment step 5 to seven is shown in Table 1;
Table 1
k hk Fk
1 0.88 12.5
2 0.74 10
3 0.44 3.13
4 0.35 1.81
5 0.26 1.66
6 0.33 1.96
The 4th and the 5th difference are less than 10%, it is taken as that being diffused into the 4th layer, diffusion depth Hdiff=(0.88+0.64 + 0.44+0.35) mm=2.41mm, D=2.41mm/48h=0.05mm/h.

Claims (9)

1. bitumen regenerant diffusion test device, it is characterised in that the bitumen regenerant diffusion test device include dissolving cylinder (1), Sample ware (2), collection device (8), feed tube (3) and drain pipe (4) are held, dissolving cylinder (1) forms tubular by barrel and cylinder bottom, in cylinder The center at bottom is provided with opening (9), and the thickness at cylinder bottom radially forms slope along Tong Di centers to the edge for dissolving cylinder (1) by being as thin as thickness Degree, drain pipe (4) is communicated with opening (9), and collection device (8) is located at the lower section of drain pipe (4), one end of " L " shape feed tube (3) It is connected with drain pipe (4), the other end opening of feed tube (3) is as inlet, on feed tube (3) and drain pipe (4) Valve (7) is provided with, the bottom that sample ware (2) is located at dissolving cylinder (1) in shallow disc shape is held.
2. bitumen regenerant diffusion test device according to claim 1, it is characterised in that be described dissolving cylinder (1), The material for holding sample ware (2), collection device (8), feed tube (3) and drain pipe (4) is metal material.
3. bitumen regenerant diffusion test device according to claim 2, it is characterised in that described metal material is not Become rusty steel or aluminium alloy.
4. bitumen regenerant diffusion test device according to claim 1, it is characterised in that the thickness edge dissolving cylinder at cylinder bottom (1) Tong Di centers to edge radially forms the gradient by being as thin as thickness, and the slope angle of the gradient is 5 °~10 °.
5. bitumen regenerant diffusion test device according to claim 1, it is characterised in that on the inlet of feed tube 3 Side is provided with acid burette.
6. bitumen regenerant diffusion test device according to claim 1, it is characterised in that the internal diameter of feed tube 3 is 3~ 5mm。
7. the method tested using bitumen regenerant diffusion test device as claimed in claim 1, it is characterised in that be Follow these steps to realize:
First, pour into and held in sample ware after pitch is heated, be then placed in baking oven and be dried to pitch levelling, obtain filling pitch holds sample Ware;
2nd, to fill pitch hold in sample ware add regenerative agent or regeneration mist sealing material, make regenerative agent or regeneration mist sealing material Material is uniformly covered with the surface of pitch, obtains testing bitumen samples;
3rd, the test bitumen samples for obtaining step 2 carry out stewing process TdiffHour, obtain filling bitumen samples holds sample Ware;
4th, the sample ware that holds for filling bitumen samples is weighed, is designated as G0, and the upper surfaces of bitumen samples is measured away from holding sample ware top edge Height be H0, it is then placed into dissolving cylinder, the valve closed on drain pipe opens the valve on feed tube, to feed tube Middle addition trichloro ethylene, makes trichloro ethylene flood the upper surface of bitumen samples, the volume of record trichloro ethylene is V ml, is stood The valve closed afterwards on feed tube, opens the valve on drain pipe, collects discharge liquor, is taken out from dissolving cylinder and holds sample ware, dried After weigh, be designated as G1, now the upper surface of bitumen samples away from hold sample ware top edge height be H1, complete a pitch cleaning;
5th, the pitch cleaning process of repeat step four repeatedly, weigh after the cleaning of each pitch fill bitumen samples hold sample ware Weight is Gk, the weight for holding sample ware that bitumen samples are filled after preceding pitch cleaning is Gk-1, pitch is tried after each pitch cleaning The upper surface of sample away from hold sample ware top edge height be Hk, the upper surface of bitumen samples is away from holding on sample ware after the cleaning of a preceding pitch The height at edge is Hk-1, so that obtaining kth time washes out the quality of pitch for mk=Gk-1-Gk, unit is g, what kth time was washed out The thickness of pitch is hk=Hk-Hk-1, unit is mm, while making trichloro ethylene complete under the discharge liquor normal temperature condition collected to kth time Full volatilization, then carries out four component tests to solid formation, i.e., test the solid formation saturation point percentage composition of kth time discharge respectively Sk, fragrance point percentage composition Pk, colloid percentage composition Rk, asphalitine percentage composition Ak
6th, the regenerative agent relative amount F of kth time discharge is calculated as followsk
<mrow> <msub> <mi>F</mi> <mi>k</mi> </msub> <mo>=</mo> <mfrac> <mrow> <msub> <mi>S</mi> <mi>k</mi> </msub> <mo>+</mo> <msub> <mi>P</mi> <mi>k</mi> </msub> </mrow> <mrow> <msub> <mi>R</mi> <mi>k</mi> </msub> <mo>+</mo> <msub> <mi>A</mi> <mi>k</mi> </msub> </mrow> </mfrac> <mo>;</mo> </mrow> 1
7th, as the regenerative agent relative amount F for occurring the m times discharge firstmWith the regenerative agent relative amount F of the m+1 times dischargem+1Phase Difference then reflects that regenerative agent diffuses to m-1 layers when being no more than 10%, then regenerative agent diffusion depth HdiffFor:
<mrow> <msub> <mi>H</mi> <mrow> <mi>d</mi> <mi>i</mi> <mi>f</mi> <mi>f</mi> </mrow> </msub> <mo>=</mo> <munderover> <mo>&amp;Sigma;</mo> <mrow> <mi>i</mi> <mo>=</mo> <mn>1</mn> </mrow> <mrow> <mi>m</mi> <mo>-</mo> <mn>1</mn> </mrow> </munderover> <msub> <mi>h</mi> <mi>i</mi> </msub> <mo>;</mo> </mrow>
8th, regenerative agent diffusion rate D, unit are calculated as follows:Mm/h, calculation formula is:
<mrow> <mi>D</mi> <mo>=</mo> <mfrac> <msub> <mi>H</mi> <mrow> <mi>d</mi> <mi>i</mi> <mi>f</mi> <mi>f</mi> </mrow> </msub> <msub> <mi>T</mi> <mrow> <mi>d</mi> <mi>i</mi> <mi>f</mi> <mi>f</mi> </mrow> </msub> </mfrac> <mo>;</mo> </mrow>
Wherein TdiffFor diffusion time, the diffusion test test of completion bitumen regenerant.
8. the method for test according to claim 7, it is characterised in that when step 2 adds to holding in sample ware for pitch is filled When entering regenerative agent, step 3 is that test bitumen samples are stood into T at room temperaturediffTime be 45~96h.
9. the method for test according to claim 7, it is characterised in that when step 2 adds to holding in sample ware for pitch is filled When entering to regenerate mist sealing material, step 3 is that test bitumen samples are stood into T in 120 DEG C of baking ovendiffTime be 2~5 Hour.
CN201510897570.XA 2015-12-08 2015-12-08 Bitumen regenerant diffusion test device and method of testing Active CN105300845B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510897570.XA CN105300845B (en) 2015-12-08 2015-12-08 Bitumen regenerant diffusion test device and method of testing

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510897570.XA CN105300845B (en) 2015-12-08 2015-12-08 Bitumen regenerant diffusion test device and method of testing

Publications (2)

Publication Number Publication Date
CN105300845A CN105300845A (en) 2016-02-03
CN105300845B true CN105300845B (en) 2017-11-07

Family

ID=55198358

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510897570.XA Active CN105300845B (en) 2015-12-08 2015-12-08 Bitumen regenerant diffusion test device and method of testing

Country Status (1)

Country Link
CN (1) CN105300845B (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105716999B (en) * 2016-04-14 2018-04-03 河海大学 A kind of reclaimed asphalt mixture regenerative agent diffuser efficiency evaluation method
CN108195721B (en) * 2017-12-07 2020-12-29 同济大学 Method for testing diffusion coefficients among different asphalts
CN108333083A (en) * 2018-03-06 2018-07-27 长安大学 A kind of assessment method of emulsification pitch penetration oil penetration depth
CN108956433B (en) * 2018-05-25 2021-03-09 中交第二公路勘察设计研究院有限公司 Calculation method of ultraviolet aging vertical diffusion depth of asphalt mixture
CN109115672B (en) * 2018-11-06 2021-01-01 苏交科集团股份有限公司 Method for evaluating permeability of asphalt pavement regeneration seal material
CN111024556B (en) * 2019-12-13 2020-09-15 四川省公路规划勘察设计研究院有限公司 Device and method for evaluating diffusion capacity of regenerant in aged asphalt

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101788446A (en) * 2010-03-10 2010-07-28 东南大学 Method for detecting diffusion capacity of regenerant in aged asphalt
CN103344528A (en) * 2013-07-02 2013-10-09 同济大学 Softening-point-test-based regenerant diffusion effect detection method
CN104809305A (en) * 2015-05-12 2015-07-29 武汉理工大学 Method for evaluating diffusion effect of reclaiming agent in aging asphalt

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04174342A (en) * 1990-08-01 1992-06-22 Sharp Corp Method for evaluating performance of liquid for forming sog file and its performance evaluation mechanism as well as manufacture of semiconductor device utilizing its performance evaluation method
JP2004117108A (en) * 2002-09-25 2004-04-15 Canon Inc Sample surface shape/infrared spectroscope combined evaluation apparatus, evaluation method, and measurement method
JP4482926B2 (en) * 2004-02-20 2010-06-16 富士フイルム株式会社 Scientific phenomenon evaluation apparatus, diffusion velocity measurement experimental apparatus, and manufacturing method thereof
DE102011003140A1 (en) * 2011-01-25 2012-07-26 Hamilton Bonaduz Ag Optical analysis method for liquid in a sample container and analysis device for carrying out the method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101788446A (en) * 2010-03-10 2010-07-28 东南大学 Method for detecting diffusion capacity of regenerant in aged asphalt
CN103344528A (en) * 2013-07-02 2013-10-09 同济大学 Softening-point-test-based regenerant diffusion effect detection method
CN104809305A (en) * 2015-05-12 2015-07-29 武汉理工大学 Method for evaluating diffusion effect of reclaiming agent in aging asphalt

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
改性再生剂在老化沥青中的扩散规律研究;沈凡等;《功能材料》;20141231;第45卷(第21期);全文 *
沥青再生剂扩散程度评价与影响因素研究;祁文洋等;《建筑材料学报》;20141231;第17卷(第6期);全文 *
沥青再生剂的再生效果与扩散性能研究;王凤楼等;《石化技术与应用》;20120131;第30卷(第1期);全文 *
沥青混合料渗水特性的试验研究;冯德成等;《建筑材料学报》;20100430;第13卷(第2期);全文 *

Also Published As

Publication number Publication date
CN105300845A (en) 2016-02-03

Similar Documents

Publication Publication Date Title
CN105300845B (en) Bitumen regenerant diffusion test device and method of testing
CN104406868B (en) Scouring freeze-thaw splitting test method for porous asphalt mixtures
CN105716999B (en) A kind of reclaimed asphalt mixture regenerative agent diffuser efficiency evaluation method
CN209368648U (en) The test of cement stabilizing RAP mixture Base Asphalt Pavement reflection crack and evaluating apparatus
CN104406993B (en) A kind of method of new Bituminous concrete surface degrees of fusion in detection heat regeneration asphalt mixture
CN101788446B (en) Method for detecting diffusion capacity of regenerant in aged asphalt
CN101738363A (en) Instrument and method for testing permeability coefficient
CN105571975A (en) Method for quantitatively analyzing adhesion of asphalt and aggregate
CN105236830B (en) Drainage asphalt mixture mix-ratio designing method based on volumetric parameters
CN102928325B (en) Tester and method for testing permeability of emulsified asphalt by using same
CN102539270B (en) Liquation evaluation method for inorganic micro powder type modified asphalt
CN104237296B (en) Permeability evaluating method of asphalt pavement recycling agent
CN107843723A (en) A kind of asphalt dynamic load salt water temperature various factors coupling experimental rig and its test method
CN105910976B (en) A kind of experimental rig and method for testing asphalt microcrack self-healing effect
CN108007811A (en) A kind of division methods of vaporous water dispersal pattern in asphalt mortar, bituminous mortar
CN103760103A (en) Asphalt and aggregate adhesiveness test device and test method
CN105938084B (en) A kind of chemistry imbibition agent permeance property evaluation method
CN104990839B (en) A kind of sealing material permeability test device of mist containing sand
CN103344528A (en) Softening-point-test-based regenerant diffusion effect detection method
CN106840950B (en) A kind of experimental rig and method for evaluating bituminous pavement resisting moving water performance of flushing
CN109115574A (en) DSR biplate test material preparation device and method and asphalt material damage-heal appraisal procedure
CN107727547A (en) A kind of pervious concrete space distributing homogeneity evaluation method
CN206220137U (en) A kind of experimental provision for measuring and analyzing banket steel-pipe pile sedimentation and emergent property
US11630097B2 (en) Quantitative evaluation method for workability of concrete based on bottom resistance analysis
CN204718928U (en) A kind of containing sand mist sealing material permeability test device

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant