CN105271223A - Preparation method of granular active carbon used for water purification - Google Patents
Preparation method of granular active carbon used for water purification Download PDFInfo
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- CN105271223A CN105271223A CN201510767872.5A CN201510767872A CN105271223A CN 105271223 A CN105271223 A CN 105271223A CN 201510767872 A CN201510767872 A CN 201510767872A CN 105271223 A CN105271223 A CN 105271223A
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Abstract
The invention relates to the field of active carbon preparation, in particular to a preparation method of granular active carbon used for water purification. The preparation method includes the steps that 1, in pulverizing, bituminous coal is placed into a pulverizer to be pulverized, wherein the granularity is 325 meshes and achieves a 80% passing rate; 2, in mixing, pulverized coal powder, coal tar and water are mixed according to the weight ratio, wherein the weight ratio is 80:12:8, and mixing temperature is 35 DEG C-60 DEG C; 3, in granulation, a mixed material is added into a granulator to be granulated, wherein the working frequency of the granulator is 30 Hz, and the granule diameter is 9.0 mm-10.0 mm; (4), in drying, granules are dried inside a drying machine, wherein drying temperature is 90 DEG C-110 DEG C. The method is reasonable in design, and on the premise of lowering the production cost and reducing environment pollution, the granular active carbon produced through the method is good in sewage treatment effect.
Description
Technical field
The present invention relates to gac preparation field, be specially a kind of preparation method of water purification granulated active carbon.
Background technology
Gac is a kind of carbon adsorbent with selective adsorption, inorganic or organic carbonaceous material can be raw material by coal, shell, wood chip etc., be made by physics high-temperature activation or chemical activation.Existing granulated active carbon for liquid phase adsorption also has Powdered Activated Carbon.Granulated active carbon be with some kind coal through fragmentation, abrasive dust, shaping, charing, activate and make, have certain physical strength, of many uses.
Mostly conventional water purification active carbon is that with bituminous coal, hard coal, coking coal, tar be raw material, produce through abrasive dust, companding shaping, charing, activation, screening production process, there is following shortcoming, 1. production process coal blending more complicated using in process in this method, influence factor is many; 2. in use coal is many, tar consumption, and occupied ground is many; 3. couple worker is healthy unfavorable; 4. production cost is high.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of production method of water purification granulated active carbon is provided, by the change to coal blending in manufacturing processed, replaces companding shaping with granulating and forming, reduce production cost, reduce environmental pollution.
The present invention adopts following technical scheme to realize:
A preparation method for water purification granulated active carbon, comprises the steps:
(1), abrasive dust: bituminous coal is put into pulverizing mill and carry out abrasive dust, granularity requirements 325 order 80% passes through;
(2), mixing: the pulverized-coal distribution of milled oil, water are mixed with the part by weight of 80:12:8, mixing temperature is 35 DEG C ~ 60 DEG C;
(3), granulation: added by compound in tablets press and carry out granulation, tablets press operating frequency is 30Hz, and granulation material diameter is 9.0 ~ 10.0mm;
(4), dry: granulation material carries out drying in drying machine, and drying temperature is 90 DEG C ~ 110 DEG C;
(5), carbonize: dried feed is added converter and carbonizes, temperature is 600 DEG C ~ 650 DEG C, and discharging time is 30min;
(6), broken: particulate state carbonized material being crushed to 3-8mm.
(7), activate: the carbonized material broken is added Slapple activating furnace and activates, temperature is 880 DEG C ~ 960 DEG C, and discharging time is 60h;
(8), screening packaging: activated material is crushed to 8-30 object granular active carbon and packs.
Compared with prior art, the inventive method advantage specific as follows:
1, use bituminous coal to replace hard coal can save a large amount of expensive hard coal, reduce production cost.
2, gained gac intensity is good, has good adsorptive power.
3, the atmospheric pollution in worker-house is decreased.
4, gained gac may be used for the industries such as water treatment, decolouring, taste removal.
The inventive method is reasonable in design, produces the water purification charcoal product meeting market demands with less coal, granulating and forming.Under the prerequisite reducing production cost and environmental pollution, the granulated active carbon produced by this method is respond well in sewage disposal.
Embodiment
Below specific embodiments of the invention are described in detail.
embodiment 1
A production method for water purification granulated active carbon, comprises the following steps:
1, abrasive dust: bituminous coal is put into pulverizing mill and carry out abrasive dust, granularity requirements 325 order 80% passes through;
2, mix: the pulverized-coal distribution of milled oil, water are mixed with the ratio of 80:12:8, mixing temperature is 60 DEG C;
3, granulation: compound is added in tablets press and carry out granulation, tablets press operating frequency is 30Hz, and granulation material diameter is 9.0 ~ 10.0mm;
4, dry: granulation material carries out drying in drying machine, and drying temperature is 90 DEG C;
5, carbonize: dried feed is added converter and carbonizes, temperature is 650 DEG C, and discharging time is 30min, and load is 20t/d;
6, broken: particulate state carbonized material being crushed to 3-8mm.
7, activate: the carbonized material broken is added Slapple activating furnace and activates, temperature is 900 DEG C, and discharging time is 60h, and load is 4t/d;
8, screening packaging: activated material is crushed to 8-30 object granular active carbon and packs.
embodiment 2
A production method for water purification granulated active carbon, comprises the following steps:
1, abrasive dust: bituminous coal is put into pulverizing mill and carry out abrasive dust, granularity requirements 325 order 80% passes through;
2, mix: the pulverized-coal distribution of milled oil, water are mixed with the ratio of 80:12:8, mixing temperature is 35 DEG C DEG C;
3, granulation: compound is added in tablets press and carry out granulation, tablets press operating frequency is 30Hz, and granulation material diameter is 9.0 ~ 10.0mm;
4, dry: granulation material carries out drying in drying machine, and drying temperature is 100 DEG C;
5, carbonize: dried feed is added converter and carbonizes, temperature is 620 DEG C, and discharging time is 30min, and load is 20t/d;
6, broken: particulate state carbonized material being crushed to 3-8mm.
7, activate: the carbonized material broken is added Slapple activating furnace and activates, temperature is 880 DEG C, and discharging time is 60h, and load is 4t/d;
8, screening packaging: activated material is crushed to 8-30 object granular active carbon and packs.
embodiment 3
A production method for water purification granulated active carbon, comprises the following steps:
1, abrasive dust: bituminous coal is put into pulverizing mill and carry out abrasive dust, granularity requirements 325 order 80% passes through;
2, mix: the pulverized-coal distribution of milled oil, water are mixed with the ratio of 80:12:8, mixing temperature is 50 DEG C;
3, granulation: compound is added in tablets press and carry out granulation, tablets press operating frequency is 30Hz, and granulation material diameter is 9.0 ~ 10.0mm;
4, dry: granulation material carries out drying in drying machine, and drying temperature is 110 DEG C;
5, carbonize: dried feed is added converter and carbonizes, temperature is 600 DEG C, and discharging time is 30min, and load is 20t/d;
6, broken: particulate state carbonized material being crushed to 3-8mm.
7, activate: the carbonized material broken is added Slapple activating furnace and activates, temperature is 960 DEG C, and discharging time is 60h, and load is 4t/d;
8, screening packaging: activated material is crushed to 8-30 object granular active carbon and packs.
It should be noted last that; above embodiment is only in order to illustrate technical scheme of the present invention and unrestricted; although be described in detail with reference to the embodiment of the present invention; those of ordinary skill in the art is to be understood that; technical scheme of the present invention is modified or equivalent replacement; do not depart from the spirit and scope of technical scheme of the present invention, it all should be contained in claims of the present invention.
Claims (1)
1. a preparation method for water purification granulated active carbon, is characterized in that: comprise the steps:
(1), abrasive dust: bituminous coal is put into pulverizing mill and carry out abrasive dust, granularity requirements 325 order 80% passes through;
(2), mixing: the pulverized-coal distribution of milled oil, water are mixed with the part by weight of 80:12:8, mixing temperature is 35 DEG C ~ 60 DEG C;
(3), granulation: added by compound in tablets press and carry out granulation, tablets press operating frequency is 30Hz, and granulation material diameter is 9.0 ~ 10.0mm;
(4), dry: granulation material carries out drying in drying machine, and drying temperature is 90 DEG C ~ 110 DEG C;
(5), carbonize: dried feed is added converter and carbonizes, temperature is 600 DEG C ~ 650 DEG C, and discharging time is 30min;
(6), broken: particulate state carbonized material being crushed to 3-8mm;
(7), activate: the carbonized material broken is added Slapple activating furnace and activates, temperature is 880 DEG C ~ 960 DEG C, and discharging time is 60h;
(8), screening packaging: activated material is crushed to 8-30 object granular active carbon and packs.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107840333A (en) * | 2017-11-08 | 2018-03-27 | 山西新华化工有限责任公司 | The production method of the hollow activated carbon of desulphurization denitration |
CN108314042A (en) * | 2018-04-17 | 2018-07-24 | 温州德润日用品有限公司 | A kind of complex spherical active carbon purifying particle and preparation method thereof |
CN109368637A (en) * | 2018-12-14 | 2019-02-22 | 上海熙碳环保科技有限公司 | A kind of the high-efficiency multi-function active carbon and its preparation process of superpower absorption |
-
2015
- 2015-11-12 CN CN201510767872.5A patent/CN105271223A/en active Pending
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107840333A (en) * | 2017-11-08 | 2018-03-27 | 山西新华化工有限责任公司 | The production method of the hollow activated carbon of desulphurization denitration |
CN108314042A (en) * | 2018-04-17 | 2018-07-24 | 温州德润日用品有限公司 | A kind of complex spherical active carbon purifying particle and preparation method thereof |
CN109368637A (en) * | 2018-12-14 | 2019-02-22 | 上海熙碳环保科技有限公司 | A kind of the high-efficiency multi-function active carbon and its preparation process of superpower absorption |
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Application publication date: 20160127 |