CN105266007B - By health preserving rice noodle roll and the preparation technology thereof of peanut oil foot brush finish plate - Google Patents
By health preserving rice noodle roll and the preparation technology thereof of peanut oil foot brush finish plate Download PDFInfo
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- CN105266007B CN105266007B CN201510790158.8A CN201510790158A CN105266007B CN 105266007 B CN105266007 B CN 105266007B CN 201510790158 A CN201510790158 A CN 201510790158A CN 105266007 B CN105266007 B CN 105266007B
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
- C07D303/06—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms in which the oxirane rings are condensed with a carbocyclic ring system having three or more relevant rings
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/32—Separation; Purification
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Abstract
The invention discloses health preserving rice noodle roll and the preparation technology thereof of a kind of peanut oil foot brush finish plate, be mainly made up of the material of following weight portion: 100 500 parts of rice flour, Folium Psidii Guajavae extract 0.05 0.38 parts, 0.2 1.8 parts of water, Oleum Arachidis hypogaeae semen heel 0.1 2.5 parts.Preparation technology includes: prepared by Rice & peanut milk；Prepared by peanut oil foot；The steps such as health preserving rice noodle roll making.The present invention prepares and adds Folium Psidii Guajavae extract in the Rice & peanut milk of rice noodle roll, and rice noodle roll increases the function of health preserving, reduce blood pressure, blood fat evident in efficacy, it is achieved dietetic therapy.Utilize Folium Psidii Guajavae extract, resource can be made full use of, reduce production cost.There is substantial amounts of Folium Psidii Guajavae not to be utilized every year, become fallen leaves all over the mountains and plains.By the research and development to Folium Psidii Guajavae so that it is turn waste into wealth, can increase farmers' income.Peanut oil foot, through ultrasonic disperse, different types of oil plant disperses evenly, and macromole in oil plant is converted into low molecule, promotes oil variety.
Description
Technical field
The present invention relates to make rice noodle roll field, particularly relate to the technique that a kind of peanut oil foot brush finish plate makes rice noodle roll.
Background technology.
The making of currently known thin rice noodle roll, according to weight ratio, by flour 20%, 60-65 DEG C of warm water 80%, stirs evenly as face
Slurry, makes starch adhesive shift to an earlier date somewhat half-mature, and very bad assurance makes starch adhesive early-stage preparations, the tray area long 60cm* width 50cm of making,
The big baking oven of corresponding outfit, same 100 grams of starch adhesives pour on big pallet, and many times side's amount aspect is held inaccurate, and starch adhesive falls simultaneously
Obtain uneven, cause taste to have very big difference, mouthfeel not to be improved cooking aspect baking inequality.Brush finish plate simultaneously
Miscella low-quality covers with paint or varnish panel, causes the rice noodle roll mouthfeel made the most greasy, and that eats is unhealthy so that blood pressure blood fat liter
High.It should be noted that along with growth in the living standard, the food of health care progressively causes consumer to pay close attention to and favor, so
And current rice noodle roll function singleness, how by the function multiple material nourishing of rice noodle roll, it is the subject matter that solves of the present invention.
Plant Fructus psidii guajavae immaturus (Psidium guajava Linn.) is Myrtaceae (Myrtaceae) Psidium plant, for
Deciduous tree, high 5-10m.Bark fawn, twig square, tool white undercoat, the most then come off；Bud is close by white undercoat.
Single leaf alternate, rare verticillate, square round shape is oval to oval, and long 5-12cm, wide 3-5cm, that rubs has fragrance, keratin, tip
Round or short point, base portion is blunt to circular, Quan Yuan, above bottle green, vein nick or smooth, dredge raw undercoat time tender, below light green color,
Dredging raw glandula, close by pubescence, master pulse swells, and lateral vein 7-11 pair also swells, tiltedly go out nearly leaf margin and bend；Make handle long
4mm.Flower both sexes, raw 1-4 of axil；Calyx 5, green, oval；Petal white, avette, long 2-2.5cm；Stamen is most, with flower
Lobe is isometric, and filigree white, flower pesticide is light yellow, lobe；Gynoecium 1, style is longer than filigree, and stigma is circular, and ovary is the next, Room 3, ovule
Most.Berry is spherical, oval or bartlett pear shape, long 2.5-8cm, footpath 3-5cm, the usual yellow of sarcocarp, also has white or carmine
Color.Seed oval, pale.The month at florescence 5-8.The really phase 8-11 month.Folium Psidii Guajavae is dried leaves and the band leaf twig of Fructus psidii guajavae immaturus,
Another name chicken vow tea, kind Folium Persicae, that pull out leaf etc..Folium Psidii Guajavae is flat, sweet-puckery flavor, enters spleen, stomach, large intestine, Liver Channel, has drying damp and strengthening spleen,
Effect of heat-clearing and toxic substances removing, is folk therapy diabetes, enteritis and dysentery, the common drug of wound hemorrhage.
Folium Psidii Guajavae chemical composition is various, mainly includes phenolic acids, flavonoid, triterpenes and sesquiterpenoids.In recent years, kind
Sesquiterpenoids composition in Folium Granati attracts wide attention because of its good biological activity.Sesquiterpenoids
(sesquiterpenoids) be made up of 3 isoprene units, compound monoid containing 15 carbon atoms.Sesquiterpene is extensive
It is present in plant, microorganism, marine organisms and some insecticide, much there is important biological function and physiologically active, especially
It is sesquiterpene lactones, has antibacterial, antitumor, antiviral, cell toxicant, immunosuppressant, plant poison, insect hormone, antifeedant for insect
Isoreactivity, also has some to have nervous system activity.
Summary of the invention
Embodiment of the present invention technical problem to be solved is, it is provided that a kind of thickness is uniformly, adhesion lumps, mouthfeel is felt well
Sliding, outward appearance multilamellar volume, but also it is suitable for the multifunction health-preserving rice noodle roll that packing is taken out, contribute to little food operator and improve merchandising business
Achievement, reduces the technique making rice noodle roll with peanut oil foot brush finish plate of operating cost.
The technical scheme is that and be achieved in that:
Health preserving rice noodle roll with peanut oil foot brush finish plate, it is characterised in that: mainly it is made up of the material of following weight portion: rice flour
100-500 part, Folium Psidii Guajavae extract 0.05-0.38 part, water 0.2-1.8 part, Oleum Arachidis hypogaeae semen heel 0.1-2.5 part.
The structural formula of described Folium Psidii Guajavae extract (I) is as follows:
The preparation method of described Folium Psidii Guajavae extract (I) is as follows: comprise following operating procedure: (a) dry by Fructus psidii guajavae immaturus
Dry leaf is pulverized, and extracts with 70-80% alcohol heat reflux, united extraction liquid, is concentrated into without alcohol taste, successively by petroleum ether, acetic acid second
Ester and water saturated n-butanol extraction, respectively obtain petroleum ether extract, acetic acid ethyl ester extract and n-butyl alcohol extract；(b)
In step (a), n-butyl alcohol takes thing macroporous resin remove impurity, first with 6 column volumes of 10% ethanol elution, then with 70% ethanol elution 8
Individual column volume, collects 70% eluent, and concentrating under reduced pressure obtains 70% ethanol elution concentrate；70% ethanol elution in (c) step (b)
Concentrate purification on normal-phase silica gel separates, successively with the methylene chloride-methanol gradient elution that volume ratio is 40:1,20:1,10:1 and 5:1
Obtain 4 components；D in () step (c), component 4 separates further by purification on normal-phase silica gel, be 8:1,5:1 and 2:1 by volume ratio successively
Methylene chloride-methanol gradient elution obtain 3 components；In (e) step (d) component 2 with octadecylsilane be bonded anti-phase
Silica gel separates, and with the methanol aqueous solution isocratic elution that concentration expressed in percentage by volume is 70%, collects 8-12 column volume eluent, eluting
Liquid is concentrated under reduced pressure to give pure compound (I).
Compound (I) separates to be prepared and structural identification:
Main material, reagent source and instrument type: ethanol, petroleum ether, ethyl acetate, n-butyl alcohol, dichloromethane are for dividing
Analysing pure, purchased from Shanghai Ling Feng chemical reagent company limited, methanol, analytical pure, purchased from Jiangsu Han Bang chemical reagent company limited.
Compound (I) separates preparation: the dried leaves (10kg) of (a) Fructus psidii guajavae immaturus is pulverized, and extracts with 75% alcohol heat reflux
(25L × 3 time), united extraction liquid, it is concentrated into without alcohol taste (6L), successively with petroleum ether (6L × 3 time), ethyl acetate (6L × 3
Secondary) and water saturated n-butyl alcohol (6L × 3 time) extraction, respectively obtain petroleum ether extract, acetic acid ethyl ester extract (377g) and
N-butyl alcohol extract；B acetic acid ethyl ester extract AB-8 macroporous resin remove impurity in () step (a), first with 10% ethanol elution 6
Column volume, then with 8 column volumes of 70% ethanol elution, collect 70% eluent, concentrating under reduced pressure obtains 70% ethanol elution concentrate
(129g)；C in () step (b), 70% ethanol elution concentrate purification on normal-phase silica gel separates, be 40:1 (8 posts by volume ratio successively
Volume), 20:1 (8 column volumes), 10:1 (8 column volumes) and the methylene chloride-methanol gradient elution of 5:1 (10 column volumes)
Obtain 4 components；D in () step (c), component 4 (24g) separates further by purification on normal-phase silica gel, be 8:1 (8 by volume ratio successively
Column volume), the methylene chloride-methanol gradient elution of 5:1 (10 column volumes) and 2:1 (8 column volumes) obtain 3 components；(e)
The reverse phase silica gel that in step (d), component 2 (15g) is bonded by octadecylsilane separates, and is the first of 70% by concentration expressed in percentage by volume
Alcohol-water solution isocratic elution, collects 8～12 column volume eluents, and eluent is concentrated under reduced pressure to give pure compound (I)
(242mg)。
Structural identification: colorless solid；HR-ESIMS shows [M+Na]+For m/z 241.1620, can obtain in conjunction with nuclear-magnetism feature
Molecular formula is C15H22O, degree of unsaturation is 5.Hydrogen nuclear magnetic resonance modal data δH(ppm, DMSO-d6, 500MHz): H-1 (2.19, m),
H-2 (6.24, m), H-3 (6.23, m), H-4 (2.31, m), H-5 (1.49, m), H-6 (0.49, dd, J=11.6,9.0), H-7
(0.83, q, J=8.7), H-8 (1.48, m), H-8 (1.27, m), H-9 (2.27, m), H-12 (0.96, s), H-13 (1.08,
S), and H-14 (1.51, s), H-15 (0.92, d, J=6.8)；Carbon-13 nmr spectra data δC(ppm, DMSO-d6, 125MHz):
60.8 (CH, 1-C), 133.7 (CH, 2-C), 133.6 (CH, 3-C), 44.9 (CH, 4-C), 41.3 (CH, 5-C), 23.8 (CH, 6-
C), 20.6 (CH, 7-C), 34.4 (CH2, 8-C), 62.6 (CH, 9-C), 63.2 (C, 10-C), 21.7 (C, 11-C), 15.1 (CH3,
12-C), 27.9 (CH3, 13-C), 20.7 (CH3, 14-C), 15.7 (CH3, 15-C)；Carbon atom labelling sees Fig. 1.13CNMR spectrum is aobvious
15 carbon signals are shown, including four methyl, a methylene, eight methines (two olefinic methines, oxygen-containing first
Base), two quaternary carbons (an oxygen-containing quaternary carbon).Two olefinic proton signal δ H6.24 (m, H-2) and 6.23 (m, H-3) show C-2
And be double bond between C-3.Two High-Fields methine proton signal δ H0.49 (dd, J=11.6,9.0Hz, H-6) and 0.83 (q, J
=8.7Hz, H-7) show that this compound contains a cyclopropane base.Methyl proton signal Me-12 and Me-13 (δ in HMBC spectrum
H0.96, s and 1.08, s) with cyclopropane methine C-6 and C-7 (δ C23.8 and 20.6), Me-12 Yu C-13 (δ C27.9), Me-
13 with the dependency of C-12 (δ C15.1), and High-Field quaternary carbon signal δ C21.7 (C-11) shows that C-11 position is connected with two first
Base.Two oxygen-containing carbon signals (δ C62.6 and 63.2) show that this compound contains one 9,10-epoxide group；Me-in HMBC spectrum
14 with the relevance verification of C-10 and C-9, H-9 and C-10 above-mentioned inference.NOESY spectrum in, H-6 and Me-14, and H-7 with
The dependency of Me-14 shows that H-6, H-7 and Me-14 are beta comfiguration.These data simultaneous reactions H-1 and H-5 is contrary vertical
Body configuration.The peak that intersects that in NOESY spectrum, H-6 with Me-15 is strong indicates the relative configuration of C-4/C-5/C-6, as shown in structural formula.
Comprehensive hydrogen spectrum, carbon spectrum, HMBC spectrum and NOESY spectrum, and document is about correlation type nuclear magnetic data, can substantially determine this compound
As it is shown in figure 1, spatial configuration is determined by ECD test further, theoretical value and experiment value basically identical (Fig. 2).
Described Oleum Arachidis hypogaeae semen heel is mainly made up of the raw material of following weight content, Oleum Brassicae campestris 45-55%, olive oil 4-8%,
Flos Osmanthi Fragrantis cream 0.5-1.2%, Oleum sesami 0.8-2.3%, wolfberry fruit extract 0.2-0.9%, surplus are peanut oil foot；Described Fructus Lycii carries
The preparation method taking thing is: take ripe Fructus Lycii is cleaned dry after, be ground into coarse powder, cross 80 mesh sieves；It is added thereto to 1-6 times of body
The ethanol of long-pending concentration of volume percent 60%, temperature: 20-50 DEG C, nitrogen supercharging, pressure: 1.2MPa-2.50MPa；Stand 2-
Percolation after 8 hours, flow 80-120 drips per minute, is filtrated to get filtrate and filtering residue；At 55 DEG C, reclaim ethanol, be condensed into relatively
The concentrated solution A of density 1.1-1.3 is standby；Described filtering residue will add the second that concentration of volume percent is 85% of 1-6 times of volume
Alcohol, refluxes 5-10 hour at 80 DEG C, takes supernatant and carry out secondary filter, reclaims ethanol, be condensed into relative density at 60 DEG C
The concentrated solution B of 1.1-1.3 is standby；Concentrated solution A and concentrated solution B is merged, removes residue, centrifugation, separation liquid is done
After dry, i.e. obtain wolfberry fruit extract.
Preparation method with the health preserving rice noodle roll of peanut oil foot brush finish plate, it is characterised in that include following method step:
(1) prepared by Rice & peanut milk；
(2) prepared by peanut oil foot；
(3) health preserving rice noodle roll makes.
Prepared by described step (1) Rice & peanut milk, according to the brewed 1-5 of rice hour of weight portion, within artificial 1-3 hour, clean,
The water droplet of weight portion drenches in stone grinder surface, grinds pulping with brewed rice through stone grinder, the Folium Psidii Guajavae extract of weight fraction
Adding in Rice & peanut milk, mechanical agitation is uniformly.
Prepared by described step (2) peanut oil foot, add the percentage composition of component, ultrasonic disperse, room temperature in peanut oil foot
Static placement 5-10 days, filter screen.
Described step (3) health preserving rice noodle roll makes, and is uniformly coated with by peanut oil foot prepared by described step (2) and spills steaming plate 1-2 time,
After Rice & peanut milk prepared by step (1) is made an addition in steaming plate, put in steam box, steam box temperature: 110-180 DEG C, time 30s-60s.
Implement the embodiment of the present invention, have the advantages that
(1) embodiment of the present invention processing technology uses the self-control existing mill Rice & peanut milk of formula and peanut oil foot, mainly allows Oleum Arachidis hypogaeae semen
Foot lumps by rice noodle roll adhesion, allows Oleum Brassicae campestris discharge light fragrance, and is peeled off with steaming plate by lamellar rice noodle roll with shelling shovel and roll into
The way of multilamellar drum, thickness is uniform, adhesion lumps, smooth in taste has Semen arachidis hypogaeae and the multiple delicate fragrance of Semen Allii Tuberosi to make rice noodle roll accomplish
Taste, the present invention make rice noodle roll accomplish thickness uniformly, adhesion caking, smooth in taste with Semen arachidis hypogaeae delicate fragrance taste, ripe after when placing
Between longer, contribute to little food operator and improve sales achievement, reduce operating cost.
(2) preparing in the Rice & peanut milk of rice noodle roll interpolation Folium Psidii Guajavae extract, rice noodle roll increases the function of health preserving, reduces blood pressure, blood
Fat is evident in efficacy, it is achieved dietetic therapy.
(3) multi-functional rice noodle roll prepared by the present invention, effect unique to treatment intestinal tract disease.
(4) present invention makes rice noodle roll with Folium Psidii Guajavae extract and can treat intestinal tract disease, eliminating toxin and beautifying the skin.Being in of characteristic
There is stronger antibacterial and antioxidation in Folium Psidii Guajavae extract, can use as natural antiseptic agent, it is not necessary to additionally add
Artificial preservative.
(5) present invention is to utilize Folium Psidii Guajavae extract, can make full use of resource, reduces production cost.Have big every year
The Folium Psidii Guajavae of amount is not utilized, and becomes fallen leaves all over the mountains and plains.By the research and development to Folium Psidii Guajavae so that it is become give up into
Treasured, can increase farmers' income.
(6) peanut oil foot, through ultrasonic disperse, different types of oil plant disperses evenly, and is converted by macromole in oil plant
For low molecule, promote oil variety.
Accompanying drawing explanation
Fig. 1 is compound (I) structural formula；
Fig. 2 is that compound (I) calculates ECD and experiment ECD figure.
Detailed description of the invention
For making the object, technical solutions and advantages of the present invention clearer, the present invention will be made the most detailed below
Describe.
Embodiment 1
With the health preserving rice noodle roll of peanut oil foot brush finish plate, mainly it is made up of the material of following weight portion: rice flour 100 part, kind stone
Pomegranate leaf extract 0.05 part, 0.2 part of water, Oleum Arachidis hypogaeae semen heel 0.1 part.
The structural formula of described Folium Psidii Guajavae extract (I) is as follows:
The preparation method of described Folium Psidii Guajavae extract (I) is as follows: comprise following operating procedure: (a) dry by Fructus psidii guajavae immaturus
Dry leaf is pulverized, and extracts with 70% alcohol heat reflux, united extraction liquid, is concentrated into without alcohol taste, successively by petroleum ether, ethyl acetate
With water saturated n-butanol extraction, respectively obtain petroleum ether extract, acetic acid ethyl ester extract and n-butyl alcohol extract；(b) step
Suddenly in (a), n-butyl alcohol takes thing macroporous resin remove impurity, first with 6 column volumes of 10% ethanol elution, then with 70% ethanol elution 8
Column volume, collects 70% eluent, and concentrating under reduced pressure obtains 70% ethanol elution concentrate；C in () step (b), 70% ethanol elution is dense
Contracting thing purification on normal-phase silica gel separates, and obtains with the methylene chloride-methanol gradient elution that volume ratio is 40:1,20:1,10:1 and 5:1 successively
To 4 components；D in () step (c), component 4 separates further by purification on normal-phase silica gel, be 8:1,5:1 and 2:1 by volume ratio successively
Methylene chloride-methanol gradient elution obtains 3 components；E anti-phase silicon that in () step (d), component 2 is bonded by octadecylsilane
Glue separates, and with the methanol aqueous solution isocratic elution that concentration expressed in percentage by volume is 70%, collects 8-12 column volume eluent, eluent
It is concentrated under reduced pressure to give pure compound (I).
Described Oleum Arachidis hypogaeae semen heel is mainly made up of the raw material of following weight content, Oleum Brassicae campestris 45%, olive oil 4%, Flos Osmanthi Fragrantis
Cream 0.5%, Oleum sesami 0.8%, wolfberry fruit extract 0.2%, surplus are peanut oil foot；The preparation method of described wolfberry fruit extract
For: take ripe Fructus Lycii is cleaned dry after, be ground into coarse powder, cross 80 mesh sieves；The percent by volume being added thereto to 1 times of volume is dense
The ethanol of degree 60%, temperature: 20 DEG C, nitrogen supercharging, pressure: 1.2MPa；Percolation after standing 2 hours, flow 80 is per minute, mistake
Filter obtains filtrate and filtering residue；Reclaiming ethanol at 55 DEG C, the concentrated solution A being condensed into relative density 1.1 is standby；By in described filtering residue
Add the ethanol that concentration of volume percent is 85% of 1 times of volume, reflux 5 hours at 80 DEG C, take supernatant and carry out secondary mistake
Filter, reclaims ethanol at 60 DEG C, and the concentrated solution B being condensed into relative density 1.1 is standby；Concentrated solution A and concentrated solution B is merged, removes
Go residue, centrifugation, after being dried by separation liquid, i.e. obtain wolfberry fruit extract.
Preparation method with the health preserving rice noodle roll of peanut oil foot brush finish plate, it is characterised in that include following method step:
(1) prepared by Rice & peanut milk；
(2) prepared by peanut oil foot；
(3) health preserving rice noodle roll makes.
Prepared by described step (1) Rice & peanut milk, brewed 1 hour of the rice of foundation weight portion, within artificial 1 hour, cleans, weight
The water droplet of part drenches in stone grinder surface, grinds pulping with brewed rice through stone grinder, and the Folium Psidii Guajavae extract of weight fraction adds
In Rice & peanut milk, mechanical agitation is uniformly.
Prepared by described step (2) peanut oil foot, add the percentage composition of component, ultrasonic disperse, room temperature in peanut oil foot
Static placement 5-days, filter screen.
Described step (3) health preserving rice noodle roll makes, and is uniformly coated with by peanut oil foot prepared by described step (2) and spills steaming plate 2 times, after
Rice & peanut milk prepared by step (1) is made an addition in steaming plate, puts in steam box, steam box temperature: 110 DEG C, time 60s.
Embodiment 2
Health preserving rice noodle roll with peanut oil foot brush finish plate, it is characterised in that: mainly it is made up of the material of following weight portion: rice flour
500 parts, Folium Psidii Guajavae extract 0.38 part, water 0.2-1.8 part, Oleum Arachidis hypogaeae semen heel 0.1-2.5 part.
The structural formula of described Folium Psidii Guajavae extract (I) is as follows:
The preparation method of described Folium Psidii Guajavae extract (I) is as follows: comprise following operating procedure: (a) dry by Fructus psidii guajavae immaturus
Dry leaf is pulverized, and extracts with 70-80% alcohol heat reflux, united extraction liquid, is concentrated into without alcohol taste, successively by petroleum ether, acetic acid second
Ester and water saturated n-butanol extraction, respectively obtain petroleum ether extract, acetic acid ethyl ester extract and n-butyl alcohol extract；(b)
In step (a), n-butyl alcohol takes thing macroporous resin remove impurity, first with 6 column volumes of 10% ethanol elution, then with 70% ethanol elution 8
Individual column volume, collects 70% eluent, and concentrating under reduced pressure obtains 70% ethanol elution concentrate；70% ethanol elution in (c) step (b)
Concentrate purification on normal-phase silica gel separates, successively with the methylene chloride-methanol gradient elution that volume ratio is 40:1,20:1,10:1 and 5:1
Obtain 4 components；D in () step (c), component 4 separates further by purification on normal-phase silica gel, be 8:1,5:1 and 2:1 by volume ratio successively
Methylene chloride-methanol gradient elution obtain 3 components；In (e) step (d) component 2 with octadecylsilane be bonded anti-phase
Silica gel separates, and with the methanol aqueous solution isocratic elution that concentration expressed in percentage by volume is 70%, collects 8-12 column volume eluent, eluting
Liquid is concentrated under reduced pressure to give pure compound (I).
Described Oleum Arachidis hypogaeae semen heel is mainly made up of the raw material of following weight content, Oleum Brassicae campestris 55%, olive oil 8%, Flos Osmanthi Fragrantis
Cream 1.2%, Oleum sesami 2.3%, wolfberry fruit extract 0.9%, surplus are peanut oil foot；The preparation method of described wolfberry fruit extract
For: take ripe Fructus Lycii is cleaned dry after, be ground into coarse powder, cross 80 mesh sieves；The percent by volume being added thereto to 6 times of volumes is dense
The ethanol of degree 60%, temperature: 50 DEG C, nitrogen supercharging, pressure: 2.50MPa；Percolation after standing 8 hours, flow 120 is per minute,
It is filtrated to get filtrate and filtering residue；Reclaiming ethanol at 55 DEG C, the concentrated solution A being condensed into relative density 1.3 is standby；By described filtering residue
The ethanol that concentration of volume percent is 85% of middle 6 times of volumes of addition, refluxes 10 hours at 80 DEG C, takes supernatant and carry out secondary
Filtering, reclaim ethanol at 60 DEG C, the concentrated solution B being condensed into relative density 1.3 is standby；Concentrated solution A and concentrated solution B is merged,
Remove residue, centrifugation, after being dried by separation liquid, i.e. obtain wolfberry fruit extract.
Preparation method with the health preserving rice noodle roll of peanut oil foot brush finish plate, it is characterised in that include following method step:
(1) prepared by Rice & peanut milk；
(2) prepared by peanut oil foot；
(3) health preserving rice noodle roll makes.
Prepared by described step (1) Rice & peanut milk, brewed 5 hours of the rice of foundation weight portion, within artificial 3 hours, cleans, weight
The water droplet of part drenches in stone grinder surface, grinds pulping with brewed rice through stone grinder, and the Folium Psidii Guajavae extract of weight fraction adds
In Rice & peanut milk, mechanical agitation is uniformly.
Prepared by described step (2) peanut oil foot, add the percentage composition of component, ultrasonic disperse, room temperature in peanut oil foot
Static placement 5-10 days, filter screen.
Described step (3) health preserving rice noodle roll makes, and is uniformly coated with by peanut oil foot prepared by described step (2) and spills steaming plate 2 times, after
Rice & peanut milk prepared by step (1) is made an addition in steaming plate, puts in steam box, steam box temperature: 180 DEG C, time 30s.
Embodiment 3
Health preserving rice noodle roll with peanut oil foot brush finish plate, it is characterised in that: mainly it is made up of the material of following weight portion: rice flour
200 parts, Folium Psidii Guajavae extract 0.12 part, 0.4 part of water, Oleum Arachidis hypogaeae semen heel 0.2 part.
The structural formula of described Folium Psidii Guajavae extract (I) is as follows:
The preparation method of described Folium Psidii Guajavae extract (I) is as follows: comprise following operating procedure: (a) dry by Fructus psidii guajavae immaturus
Dry leaf pulverize, with 75% alcohol heat reflux extract, united extraction liquid, be concentrated into without alcohol taste, successively use petroleum ether, ethyl acetate and
Water saturated n-butanol extraction, respectively obtains petroleum ether extract, acetic acid ethyl ester extract and n-butyl alcohol extract；(b) step
A in (), n-butyl alcohol takes thing macroporous resin remove impurity, first with 6 column volumes of 10% ethanol elution, then with 8 posts of 70% ethanol elution
Volume, collects 70% eluent, and concentrating under reduced pressure obtains 70% ethanol elution concentrate；C in () step (b), 70% ethanol elution concentrates
Thing purification on normal-phase silica gel separates, and obtains with the methylene chloride-methanol gradient elution that volume ratio is 40:1,20:1,10:1 and 5:1 successively
4 components；D in () step (c), component 4 separates further by purification on normal-phase silica gel, be the two of 8:1,5:1 and 2:1 by volume ratio successively
Chloromethanes-methanol elution gradient obtains 3 components；E reverse phase silica gel that in () step (d), component 2 is bonded by octadecylsilane
Separate, with the methanol aqueous solution isocratic elution that concentration expressed in percentage by volume is 70%, collect 8-12 column volume eluent, eluent
It is concentrated under reduced pressure to give pure compound (I).
Described Oleum Arachidis hypogaeae semen heel is mainly made up of the raw material of following weight content, Oleum Brassicae campestris 48%, olive oil 5%, Flos Osmanthi Fragrantis
Cream 0.8%, Oleum sesami 1.1%, wolfberry fruit extract 0.4, surplus are peanut oil foot；The preparation method of described wolfberry fruit extract is:
Take ripe Fructus Lycii is cleaned dry after, be ground into coarse powder, cross 80 mesh sieves；It is added thereto to the concentration of volume percent of 2 times of volumes
The ethanol of 60%, temperature: 30 DEG C, nitrogen supercharging, pressure: 1.4MPa；Percolation after standing 4 hours, flow 100 is per minute, mistake
Filter obtains filtrate and filtering residue；Reclaiming ethanol at 55 DEG C, the concentrated solution A being condensed into relative density 1.15 is standby；By described filtering residue
The ethanol that concentration of volume percent is 85% of middle 2 times of volumes of addition, refluxes 6 hours at 80 DEG C, takes supernatant and carry out secondary
Filtering, reclaim ethanol at 60 DEG C, the concentrated solution B being condensed into relative density 1.15 is standby；Concentrated solution A and concentrated solution B is merged,
Remove residue, centrifugation, after being dried by separation liquid, i.e. obtain wolfberry fruit extract.
Preparation method with the health preserving rice noodle roll of peanut oil foot brush finish plate, it is characterised in that include following method step:
(1) prepared by Rice & peanut milk；
(2) prepared by peanut oil foot；
(3) health preserving rice noodle roll makes.
Prepared by described step (1) Rice & peanut milk, brewed 2 hours of the rice of foundation weight portion, within artificial 2 hours, cleans, weight
The water droplet of part drenches in stone grinder surface, grinds pulping with brewed rice through stone grinder, and the Folium Psidii Guajavae extract of weight fraction adds
In Rice & peanut milk, mechanical agitation is uniformly.
Prepared by described step (2) peanut oil foot, add the percentage composition of component, ultrasonic disperse, room temperature in peanut oil foot
Static placement 5-10 days, filter screen.
Described step (3) health preserving rice noodle roll makes, and is uniformly coated with by peanut oil foot prepared by described step (2) and spills steaming plate 1 time, after
Rice & peanut milk prepared by step (1) is made an addition in steaming plate, puts in steam box, steam box temperature: 120 DEG C, time 35s.
Embodiment 4
Health preserving rice noodle roll with peanut oil foot brush finish plate, it is characterised in that: mainly it is made up of the material of following weight portion: rice flour
350 parts, Folium Psidii Guajavae extract 0.12 part, 0.36 part of water, Oleum Arachidis hypogaeae semen heel 0.89 part.
The preparation method of described Folium Psidii Guajavae extract (I), with embodiment 1.
Described Oleum Arachidis hypogaeae semen heel is mainly made up of the raw material of following weight content, Oleum Brassicae campestris 48%, olive oil 4.5%, osmanthus
Flower cream 0.7%, Oleum sesami 1.1%, wolfberry fruit extract 0.6%, surplus are peanut oil foot；The preparation side of described wolfberry fruit extract
Method, with embodiment 1.
Preparation method with the health preserving rice noodle roll of peanut oil foot brush finish plate, it is characterised in that include following method step:
(1) prepared by Rice & peanut milk；
(2) prepared by peanut oil foot；
(3) health preserving rice noodle roll makes.
Prepared by described step (1) Rice & peanut milk, brewed 4 hours of the rice of foundation weight portion, within artificial 2.5 hours, cleans, weight
The water droplet of amount part drenches in stone grinder surface, grinds pulping with brewed rice through stone grinder, and the Folium Psidii Guajavae extract of weight fraction adds
Entering in Rice & peanut milk, mechanical agitation is uniformly.
Prepared by described step (2) peanut oil foot, add the percentage composition of component, ultrasonic disperse, room temperature in peanut oil foot
Static placement 6 days, filter screen.
Described step (3) health preserving rice noodle roll makes, and is uniformly coated with by peanut oil foot prepared by described step (2) and spills steaming plate 2 times, after
Rice & peanut milk prepared by step (1) is made an addition in steaming plate, puts in steam box, steam box temperature: 140 DEG C, time 40s.
Embodiment 5
Health preserving rice noodle roll with peanut oil foot brush finish plate, it is characterised in that: mainly it is made up of the material of following weight portion: rice flour
450 parts, Folium Psidii Guajavae extract 0.365 part, 1.35 parts of water, Oleum Arachidis hypogaeae semen heel 2.128 parts.
The structural formula of described Folium Psidii Guajavae extract (I) and preparation method are with embodiment 3.
Described Oleum Arachidis hypogaeae semen heel is mainly made up of the raw material of following weight content, Oleum Brassicae campestris 51.2%, olive oil 7.5%,
Flos Osmanthi Fragrantis cream 1.15%, Oleum sesami 2.18%, wolfberry fruit extract 0.78%, surplus are peanut oil foot；The system of described wolfberry fruit extract
Preparation Method is with embodiment 3.
Preparation method with the health preserving rice noodle roll of peanut oil foot brush finish plate, it is characterised in that include following method step:
(1) prepared by Rice & peanut milk；
(2) prepared by peanut oil foot；
(3) health preserving rice noodle roll makes.
Prepared by described step (1) Rice & peanut milk, brewed 4.5 hours of the rice of foundation weight portion, within artificial 2.5 hours, cleans,
The water droplet of weight portion drenches in stone grinder surface, and brewed rice grinds pulping through stone grinder, and the Folium Psidii Guajavae extract of weight fraction adds
Entering in Rice & peanut milk, mechanical agitation is uniformly.
Prepared by described step (2) peanut oil foot, add the percentage composition of component, ultrasonic disperse, room temperature in peanut oil foot
Static placement 9 days, filter screen.
Described step (3) health preserving rice noodle roll makes, and is uniformly coated with by peanut oil foot prepared by described step (2) and spills steaming plate 1-2 time,
After Rice & peanut milk prepared by step (1) is made an addition in steaming plate, put in steam box, steam box temperature: 170 DEG C, time 55s.
Health preserving rice noodle roll is obvious to blood pressure lowering effect, and after edible health preserving rice noodle roll 2-4 month, blood pressure lowering effect substantially embodies:
Lee, female, 45 years old, teacher, before eating, shrinks pressure 166mmHg, diastolic pressure 105mmHg, the edible embodiment of the present invention
1 rice noodle roll made 3 months, shrinks pressure 135mmHg, diastolic pressure 86mmHg.
Zhang, female, 58 years old, before eating, shrink pressure 152mmHg, diastolic pressure 93mmHg, the edible embodiment of the present invention 1 makes
Rice noodle roll 2.5 months, shrink pressure 132mmHg, diastolic pressure 84mmHg.
Liu, man, 38 years old, civil servant, before eating, shrink pressure 159mmHg, diastolic pressure 97mmHg, the edible present invention implements
The rice noodle roll that example 3 makes 2.5 months, shrinks pressure 129mmHg, diastolic pressure 82mmHg.
Chen, man, 37 years old, before eating, shrinking pressure was 220mmHg, and diastolic pressure is 120mmHg, the edible embodiment of the present invention 3
The rice noodle roll made 3.2 months, shrinking pressure is 128mmHg, and diastolic pressure is 85mmHg.
Above disclosed it is only one preferred embodiment of the present invention, certainly can not limit the power of the present invention with this
Profit scope, the equivalent variations therefore made according to the claims in the present invention, still belong to the scope that the present invention is contained.
Claims (6)
1. with the health preserving rice noodle roll of peanut oil foot brush finish plate, it is characterised in that: it is made up of the material of following weight portion: rice flour 100-
500 parts, Folium Psidii Guajavae extract 0.05-0.38 part, water 0.2-1.8 part, Oleum Arachidis hypogaeae semen heel 0.1-2.5 part；Described Folium Psidii Guajavae
The structural formula of extract (I) is as follows:
The preparation method of described Folium Psidii Guajavae extract (I) is as follows: concrete operation step is as follows: (a) is by the dried leaves of Fructus psidii guajavae immaturus
Pulverize, with 70-80% alcohol heat reflux extract, united extraction liquid, be concentrated into without alcohol taste, successively use petroleum ether, ethyl acetate and
Water saturated n-butanol extraction, respectively obtains petroleum ether extract, acetic acid ethyl ester extract and n-butyl alcohol extract；(b) step
A in (), n-butyl alcohol takes thing macroporous resin remove impurity, first with 6 column volumes of 10% ethanol elution, then with 8 posts of 70% ethanol elution
Volume, collects 70% eluent, and concentrating under reduced pressure obtains 70% ethanol elution concentrate；C in () step (b), 70% ethanol elution concentrates
Thing purification on normal-phase silica gel separates, and obtains with the methylene chloride-methanol gradient elution that volume ratio is 40:1,20:1,10:1 and 5:1 successively
4 components；D in () step (c), component 4 separates further by purification on normal-phase silica gel, be the two of 8:1,5:1 and 2:1 by volume ratio successively
Chloromethanes-methanol elution gradient obtains 3 components；E reverse phase silica gel that in () step (d), component 2 is bonded by octadecylsilane
Separating, with the methanol aqueous solution isocratic elution that concentration expressed in percentage by volume is 70%, collect 8-12 column volume eluent, eluent subtracts
Pressure is concentrated to give pure compound (I).
The health preserving rice noodle roll of peanut oil foot brush finish plate the most according to claim 1, it is characterised in that: described Oleum Arachidis hypogaeae semen heel
It is made up of the raw material of following weight content, Oleum Brassicae campestris 45-55%, olive oil 4-8%, Flos Osmanthi Fragrantis cream 0.5-1.2%, Oleum sesami 0.8-
2.3%, wolfberry fruit extract 0.2-0.9%, surplus are peanut oil foot；The preparation method of described wolfberry fruit extract is: take ripe Chinese holly
Qi is cleaned dry after, be ground into coarse powder, cross 80 mesh sieves；It is added thereto to the concentration of volume percent 60% of 1-6 times of volume
Ethanol, temperature: 20-50 DEG C, nitrogen supercharging, pressure: 1.2MPa-2.50MPa；Percolation after standing 2-8 hour, flow 80-120 drips
Per minute, it is filtrated to get filtrate and filtering residue；Reclaiming ethanol at 55 DEG C, the concentrated solution A being condensed into relative density 1.1-1.3 is standby
With；To add the ethanol that concentration of volume percent is 85% of 1-6 times of volume in described filtering residue, the 5-10 that refluxes at 80 DEG C is little
Time, taking supernatant and carry out secondary filter, at 60 DEG C, reclaim ethanol, the concentrated solution B being condensed into relative density 1.1-1.3 is standby；
Concentrated solution A and concentrated solution B is merged, removes residue, centrifugation, after being dried by separation liquid, i.e. obtain wolfberry fruit extract.
3. the preparation method with the health preserving rice noodle roll of peanut oil foot brush finish plate as claimed in claim 1, it is characterised in that specifically side
Method step is as follows:
(1) prepared by Rice & peanut milk；
(2) prepared by peanut oil foot；
(3) health preserving rice noodle roll makes.
4. require to use described in 3 the preparation method of the health preserving rice noodle roll of peanut oil foot brush finish plate according to profit, it is characterised in that described step
(1) prepared by Rice & peanut milk, according to the brewed 1-5 of rice hour of weight portion, within artificial 1-3 hour, cleans, the water droplet of weight portion drench in
Stone grinder surface, brewed rice grinds pulping through stone grinder, and the Folium Psidii Guajavae extract of weight fraction adds in Rice & peanut milk, mechanical agitation
Uniformly.
5. require to use described in 3 the preparation method of the health preserving rice noodle roll of peanut oil foot brush finish plate according to profit, it is characterised in that described step
(2) prepared by peanut oil foot, adds the percentage composition of component, ultrasonic disperse in peanut oil foot, and room temperature is static places 5-10 days, mistake
Screen net.
6. require to use described in 3 the preparation method of the health preserving rice noodle roll of peanut oil foot brush finish plate according to profit, it is characterised in that described step
(3) health preserving rice noodle roll make, peanut oil foot prepared by described step (2) is uniformly coated with and spills steaming plate 1-2 time, after prepared by step (1)
Rice & peanut milk make an addition in steaming plate, put in steam box, steam box temperature: 110-180 DEG C, time 30s-60s.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102696969A (en) * | 2012-04-17 | 2012-10-03 | 李展威 | Non-stick roll type steamed vermicelli roll and manufacturing process thereof |
| CN103549260A (en) * | 2013-10-16 | 2014-02-05 | 陆建益 | Health care preservative rice cake capable of assisting to reduce blood glucose, and preparation method thereof |
| CN103585400A (en) * | 2012-08-14 | 2014-02-19 | 广西金嗓子有限责任公司 | Composition having immunity enhancing and fatigue alleviating effects, and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102696969A (en) * | 2012-04-17 | 2012-10-03 | 李展威 | Non-stick roll type steamed vermicelli roll and manufacturing process thereof |
| CN103585400A (en) * | 2012-08-14 | 2014-02-19 | 广西金嗓子有限责任公司 | Composition having immunity enhancing and fatigue alleviating effects, and preparation method thereof |
| CN103549260A (en) * | 2013-10-16 | 2014-02-05 | 陆建益 | Health care preservative rice cake capable of assisting to reduce blood glucose, and preparation method thereof |
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