CN105255252A - Printing ink for washing machine panel glass - Google Patents
Printing ink for washing machine panel glass Download PDFInfo
- Publication number
- CN105255252A CN105255252A CN201510773022.6A CN201510773022A CN105255252A CN 105255252 A CN105255252 A CN 105255252A CN 201510773022 A CN201510773022 A CN 201510773022A CN 105255252 A CN105255252 A CN 105255252A
- Authority
- CN
- China
- Prior art keywords
- parts
- ink
- surface sheet
- sheet glass
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000011521 glass Substances 0.000 title abstract description 17
- 238000005406 washing Methods 0.000 title abstract description 5
- 238000007639 printing Methods 0.000 title abstract description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 21
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 21
- -1 propylene glycol fatty acid ester Chemical class 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 15
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 claims abstract description 14
- DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 13
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 13
- 239000003822 epoxy resin Substances 0.000 claims abstract description 8
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 8
- OPLCSTZDXXUYDU-UHFFFAOYSA-N 2,4-dimethyl-6-tert-butylphenol Chemical compound CC1=CC(C)=C(O)C(C(C)(C)C)=C1 OPLCSTZDXXUYDU-UHFFFAOYSA-N 0.000 claims abstract description 7
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 7
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 7
- 229930195729 fatty acid Natural products 0.000 claims abstract description 7
- 239000000194 fatty acid Substances 0.000 claims abstract description 7
- 239000008103 glucose Substances 0.000 claims abstract description 7
- 239000006188 syrup Substances 0.000 claims abstract description 7
- 235000020357 syrup Nutrition 0.000 claims abstract description 7
- 239000004200 microcrystalline wax Substances 0.000 claims abstract description 6
- 235000019808 microcrystalline wax Nutrition 0.000 claims abstract description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 42
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- 239000005357 flat glass Substances 0.000 claims description 20
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 16
- 239000013530 defoamer Substances 0.000 claims description 14
- ZMARGGQEAJXRFP-UHFFFAOYSA-N 1-hydroxypropan-2-yl 2-methylprop-2-enoate Chemical compound OCC(C)OC(=O)C(C)=C ZMARGGQEAJXRFP-UHFFFAOYSA-N 0.000 claims description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 10
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims description 10
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 10
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims description 10
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 8
- DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical compound [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 claims description 8
- 239000003999 initiator Substances 0.000 claims description 8
- 239000000377 silicon dioxide Substances 0.000 claims description 8
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 claims description 8
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 6
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical group OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 6
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 6
- 229960004418 trolamine Drugs 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 3
- 239000002202 Polyethylene glycol Substances 0.000 abstract 1
- 239000002518 antifoaming agent Substances 0.000 abstract 1
- 229920001223 polyethylene glycol Polymers 0.000 abstract 1
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000032683 aging Effects 0.000 description 1
- 238000004378 air conditioning Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses ink for washing machine panel glass. The ink comprises the following raw materials in parts by weight: 100-120 parts of epoxy resin, 30-45 parts of allyl alcohol, 10-15 parts of microcrystalline wax, 20-30 parts of polyethylene glycol, 10-18 parts of ethyl acetate, 18-25 parts of propylene glycol fatty acid ester, 4-8 parts of acrylic resin, 1-4 parts of 2, 4-dimethyl-6-tert-butylphenol, 0.3-0.8 part of citric acid, 2-6 parts of glucose syrup and 2-6 parts of defoaming agent. The printing ink for the washing machine panel glass takes the epoxy resin as a main raw material, is safe and environment-friendly, integrally improves the adhesion performance and the waterproof performance of the printing ink by being supplemented with other raw materials, and is suitable for the washing machine panel glass.
Description
Technical field
The present invention relates to a kind of protection ink for washer surface sheet glass, belong to glass working arts field.
Background technology
In the household electrical appliances such as electric cooker, refrigerator, washing machine or air-conditioning, have the display comprising various layer and arrange, display is arranged based on technique of display layer, generally can be made up of glass.
Along with the raising of people's living standard and the development in house ornamentation market, the aesthetic standards of people are strengthened day by day, more and more higher to the requirement of glass appearance, and therefore the application of typography on glasswork is also increasingly extensive.Ink just can the main raw of effective reinforcing glass products appearance sight.At present, the glass ink on market mainly contains unorganic glass ink and two kinds, synthetic glass ink.All there are some shortcomings in actual applications in two kinds of ink, is mainly manifested in the poor adhesive force to glass baseplate, poor water resistance, coating easily comes off, easy to change, and the life-span is shorter.In addition, some glass ink is containing toxic stronger organic solvent, and these solvents will produce peculiar smell and affect the healthy of glass printing product user.
Summary of the invention
In order to overcome the deficiencies in the prior art, the invention provides a kind of ink for washer surface sheet glass.
The present invention is achieved through the following technical solutions:
A kind of ink for washer surface sheet glass, comprise the raw material of following parts by weight: epoxy resin 100-120 part, vinylcarbinol 30-45 part, microcrystalline wax 10-15 part, polyoxyethylene glycol 20-30 part, ethyl acetate 10-18 part, propylene glycol fatty acid ester 18-25 part, acrylic resin 4-8 part, 2,4 dimethyl 6 tert butyl phenol 1-4 part, citric acid 0.3-0.8 part, glucose syrup 2-6 part and defoamer 2-6 part.
Described a kind of ink for washer surface sheet glass, described acrylic resin is obtained by following steps: methyl methacrylate, Rocryl 410, ethyl propenoate, vinylformic acid, ethylene glycol, initiator and water are placed in reactor, temperature be 90-100 DEG C, pressure carries out polyreaction under being the condition of 1-1.5KPa.
Described a kind of ink for washer surface sheet glass, in the parts by weight 100 parts of water, the parts by weight of described methyl methacrylate, Rocryl 410, ethyl propenoate, vinylformic acid, ethylene glycol and initiator are respectively: 10-15 part, 6-12 part, 2-6 part, 4-8 part, 1-3 part and 0.2-0.6 part.
Described a kind of ink for washer surface sheet glass, described initiator is trolamine.
Described a kind of ink for washer surface sheet glass, described defoamer is the mixture of tributyl phosphate, polypropylene glycerol aether, water drain silica and sodium-chlor.
Described a kind of ink for washer surface sheet glass, the parts by weight of each raw material of described defoamer are respectively: tributyl phosphate 50-60 part, polypropylene glycerol aether 15-20 part, water drain silica 1-4 part and sodium-chlor 0.4-0.8 part.
The beneficial effect that the present invention reaches:
Ink for washer surface sheet glass of the present invention take epoxy resin as main raw material, safety and environmental protection, and by being aided with other raw materials, entirety improves adhesion property and the water resistance of ink, is applicable to washer surface sheet glass and uses.
The acrylic resin that the present invention prepares has good adhesive capacity, acts synergistically and improve the absorption property of ink on face glass together with defoamer.Meanwhile, vinylcarbinol, microlite, polyoxyethylene glycol and ethyl acetate improve the mobility of ink; Propylene glycol fatty acid ester, 2,4 dimethyl 6 tert butyl phenol, citric acid and glucose syrup improve water resistance and the ageing resistance of ink, extend the work-ing life of ink.
Defoamer of the present invention is the mixture of tributyl phosphate, polypropylene glycerol aether, water drain silica and sodium-chlor, reduces the tension force of ink on face glass surface, jointly improves the absorption property of ink on face glass with acrylic resin.
Embodiment
Embodiment 1
A kind of ink for washer surface sheet glass, comprise the raw material of following parts by weight: epoxy resin 100 parts, vinylcarbinol 45 parts, microcrystalline wax 10 parts, polyoxyethylene glycol 30 parts, ethyl acetate 10 parts, propylene glycol fatty acid ester 25 parts, acrylic resin 4 parts, 2,4 dimethyl 6 tert butyl phenol 4 parts, citric acid 0.3 part, glucose syrup 6 parts and defoamer 6 parts.
Described acrylic resin is obtained by following steps: methyl methacrylate, Rocryl 410, ethyl propenoate, vinylformic acid, ethylene glycol, initiator and water are placed in reactor, temperature be 90-100 DEG C, pressure carries out polyreaction under being the condition of 1-1.5KPa.In the parts by weight 100 parts of water, the parts by weight of described methyl methacrylate, Rocryl 410, ethyl propenoate, vinylformic acid, ethylene glycol and initiator are respectively: 10 parts, 12 parts, 6 parts, 4 parts, 3 parts and 0.2 part.
The parts by weight of each raw material of described defoamer are respectively: tributyl phosphate 50 parts, polypropylene glycerol aether 20 parts, water drain silica 1 part and 0.8 part, sodium-chlor.
Embodiment 2
A kind of ink for washer surface sheet glass, comprise the raw material of following parts by weight: epoxy resin 120 parts, vinylcarbinol 30 parts, microcrystalline wax 15 parts, polyoxyethylene glycol 20 parts, ethyl acetate 18 parts, propylene glycol fatty acid ester 18 parts, acrylic resin 8 parts, 2,4 dimethyl 6 tert butyl phenol 1 part, citric acid 0.8 part, glucose syrup 2 parts and defoamer 2 parts.
Described acrylic resin is obtained by following steps: methyl methacrylate, Rocryl 410, ethyl propenoate, vinylformic acid, ethylene glycol, trolamine and water are placed in reactor, temperature be 90-100 DEG C, pressure carries out polyreaction under being the condition of 1-1.5KPa.In the parts by weight 100 parts of water, the parts by weight of described methyl methacrylate, Rocryl 410, ethyl propenoate, vinylformic acid, ethylene glycol and trolamine are respectively: 15 parts, 12 parts, 2 parts, 8 parts, 1 part and 0.6 part.
The parts by weight of each raw material of described defoamer are respectively: tributyl phosphate 60 parts, polypropylene glycerol aether 15 parts, water drain silica 4 parts and 0.4 part, sodium-chlor.
Embodiment 3
A kind of ink for washer surface sheet glass, comprise the raw material of following parts by weight: epoxy resin 116 parts, vinylcarbinol 40 parts, microcrystalline wax 12 parts, polyoxyethylene glycol 24 parts, ethyl acetate 15 parts, propylene glycol fatty acid ester 20 parts, acrylic resin 6 parts, 2,4 dimethyl 6 tert butyl phenol 3 parts, citric acid 0.6 part, glucose syrup 5 parts and defoamer 5 parts.
Described acrylic resin is obtained by following steps: methyl methacrylate, Rocryl 410, ethyl propenoate, vinylformic acid, ethylene glycol, trolamine and water are placed in reactor, temperature be 90-100 DEG C, pressure carries out polyreaction under being the condition of 1-1.5KPa.In the parts by weight 100 parts of water, the parts by weight of described methyl methacrylate, Rocryl 410, ethyl propenoate, vinylformic acid, ethylene glycol and trolamine are respectively: 13 parts, 10 parts, 3 parts, 5 parts, 2 parts and 0.4 part.
The parts by weight of each raw material of described defoamer are respectively: tributyl phosphate 56 parts, polypropylene glycerol aether 18 parts, water drain silica 2 parts and 0.5 part, sodium-chlor.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle; can also make some improvement and distortion, these improve and distortion also should be considered as protection scope of the present invention.
Claims (6)
1. the ink for washer surface sheet glass, it is characterized in that, comprise the raw material of following parts by weight: epoxy resin 100-120 part, vinylcarbinol 30-45 part, microcrystalline wax 10-15 part, polyoxyethylene glycol 20-30 part, ethyl acetate 10-18 part, propylene glycol fatty acid ester 18-25 part, acrylic resin 4-8 part, 2,4 dimethyl 6 tert butyl phenol 1-4 part, citric acid 0.3-0.8 part, glucose syrup 2-6 part and defoamer 2-6 part.
2. a kind of ink for washer surface sheet glass according to claim 1, it is characterized in that, described acrylic resin is obtained by following steps: methyl methacrylate, Rocryl 410, ethyl propenoate, vinylformic acid, ethylene glycol, initiator and water are placed in reactor, temperature be 90-100 DEG C, pressure carries out polyreaction under being the condition of 1-1.5KPa.
3. a kind of ink for washer surface sheet glass according to claim 2, it is characterized in that, in the parts by weight 100 parts of water, the parts by weight of described methyl methacrylate, Rocryl 410, ethyl propenoate, vinylformic acid, ethylene glycol and initiator are respectively: 10-15 part, 6-12 part, 2-6 part, 4-8 part, 1-3 part and 0.2-0.6 part.
4. a kind of ink for washer surface sheet glass according to Claims 2 or 3, is characterized in that, described initiator is trolamine.
5. a kind of ink for washer surface sheet glass according to claim 1, is characterized in that, described defoamer is the mixture of tributyl phosphate, polypropylene glycerol aether, water drain silica and sodium-chlor.
6. a kind of ink for washer surface sheet glass according to claim 5, it is characterized in that, the parts by weight of each raw material of described defoamer are respectively: tributyl phosphate 50-60 part, polypropylene glycerol aether 15-20 part, water drain silica 1-4 part and sodium-chlor 0.4-0.8 part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510773022.6A CN105255252A (en) | 2015-11-13 | 2015-11-13 | Printing ink for washing machine panel glass |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510773022.6A CN105255252A (en) | 2015-11-13 | 2015-11-13 | Printing ink for washing machine panel glass |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105255252A true CN105255252A (en) | 2016-01-20 |
Family
ID=55095205
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510773022.6A Pending CN105255252A (en) | 2015-11-13 | 2015-11-13 | Printing ink for washing machine panel glass |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105255252A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106082906A (en) * | 2016-05-31 | 2016-11-09 | 石鸿娟 | A kind of environment protecting thermal insulating mortar and preparation method thereof |
| CN110104942A (en) * | 2019-05-28 | 2019-08-09 | 安徽凤阳赛弗节能玻璃有限公司 | A kind of Washing Machine Panel method for glass preparation |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102719146A (en) * | 2012-07-04 | 2012-10-10 | 佛山市高明绿色德化工有限公司 | Three-dimensional printing ink |
| CN102719136A (en) * | 2012-05-11 | 2012-10-10 | 佛山市高明绿色德化工有限公司 | Colorful crystal glass printing ink |
| CN103242705A (en) * | 2013-04-25 | 2013-08-14 | 深圳市美丽华油墨涂料有限公司 | ITO (Indium Tin Oxide) conductive glass temporary protection printing ink and preparation method thereof |
| CN103865330A (en) * | 2014-02-27 | 2014-06-18 | 安徽颍美彩印包装有限公司 | Rosin gravure printing ink for glass paper and preparation method thereof |
| CN104250472A (en) * | 2013-06-27 | 2014-12-31 | 罗小丰 | Glass UV frosted ink |
-
2015
- 2015-11-13 CN CN201510773022.6A patent/CN105255252A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102719136A (en) * | 2012-05-11 | 2012-10-10 | 佛山市高明绿色德化工有限公司 | Colorful crystal glass printing ink |
| CN102719146A (en) * | 2012-07-04 | 2012-10-10 | 佛山市高明绿色德化工有限公司 | Three-dimensional printing ink |
| CN103242705A (en) * | 2013-04-25 | 2013-08-14 | 深圳市美丽华油墨涂料有限公司 | ITO (Indium Tin Oxide) conductive glass temporary protection printing ink and preparation method thereof |
| CN104250472A (en) * | 2013-06-27 | 2014-12-31 | 罗小丰 | Glass UV frosted ink |
| CN103865330A (en) * | 2014-02-27 | 2014-06-18 | 安徽颍美彩印包装有限公司 | Rosin gravure printing ink for glass paper and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106082906A (en) * | 2016-05-31 | 2016-11-09 | 石鸿娟 | A kind of environment protecting thermal insulating mortar and preparation method thereof |
| CN110104942A (en) * | 2019-05-28 | 2019-08-09 | 安徽凤阳赛弗节能玻璃有限公司 | A kind of Washing Machine Panel method for glass preparation |
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160120 |
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| RJ01 | Rejection of invention patent application after publication |