CN105254315A - Blast-furnace stemming for tapping hole - Google Patents
Blast-furnace stemming for tapping hole Download PDFInfo
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- CN105254315A CN105254315A CN201510735389.9A CN201510735389A CN105254315A CN 105254315 A CN105254315 A CN 105254315A CN 201510735389 A CN201510735389 A CN 201510735389A CN 105254315 A CN105254315 A CN 105254315A
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Abstract
The invention discloses blast-furnace stemming for a tapping hole. The blast-furnace stemming is characterized by being prepared from the following ingredients in parts by weight: 15 to 20 parts of 3-1mm magnesia-chrome spinel, 5 to 8 parts of 1-0mm corundum, 10 to 15 parts of 1-0mm sillimanite, 8 to 15 parts of 0.5-0mm magnesium oxide iron, 8 to 13 parts of clay powder, 3 to 7 parts of cobalt oxide aluminum powder, 5 to 10 parts of cutting powder, 7 to 25 parts of graphite powder, 5 to 10 parts of compound carbon powder, 0 to 1 part of cobaltosic oxide powder and 1 to 2 parts of medium temperature asphalt. The stemming has the advantages that the hole diameter of the tapping hole can be protected to be stable and to be not easily changed; the tapping is stable; in addition, in the long-time storage process of the stemming, the use performance and the operation performance are not lowered.
Description
Technical field
The invention belongs to blast furnace ironmaking plastic refractory field, be specifically related to a kind of iron notch blast furnace mud and preparation method.
Background technology
Blast furnace is the main equipment of smelting molten iron, and after blast-furnace smelting iron, needs molten iron to release through blast furnace iron notch to carry out continuously to ensure to smelt, and iron notch must be blocked, blocks the material of iron notch, be stemming.At present, when smelting some particular iron ore such as containing the iron ore that vanadium titanium is high, because vanadium, titanyl compound fusing point are very high, it is higher than tapping temperature, can not be melted when tapping a blast furnace, and can be deposited on iron notch, cause tying thicker and thicker, cause the aperture of iron notch to change
;generally cannot process in time again iron notch under high temperature, the change of iron notch has had a strong impact on the stable of iron mouth and has tapped a blast furnace, shakiness when causing tapping a blast furnace, and very easily causes molten iron to run large stream, flame arrow, gives and arrange the production program that blast furnace normally taps a blast furnace to bring difficulty.
Summary of the invention
The object of this invention is to provide a kind of aperture that can ensure iron notch to stablize, can stablize and tap a blast furnace, stemming easy to use and production method thereof.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs: a kind of iron notch blast furnace mud, it is characterized in that described blast furnace mud is made up of the component of following weight part: 3-1mm magnesia chrome spinel: 15 ~ 20 parts; 1-0mm corundum: 5 ~ 8 parts; 1-0mm sillimanite: 10 ~ 15 parts; 0.5-0mm magnesium oxide iron: 8 ~ 15 parts; Inclined clay powder: 8 ~ 13 parts; Cobalt oxide aluminium powder 3-7 part, cutting powder: 5 ~ 10 parts; Graphite Powder 99: 7 ~ 25 parts, compound powdered carbon 5-10 part, cobaltosic oxide 0 ~ 1 part, mid-temperature pitch powder: 1 ~ 2 part; Additional modification tar: 13 ~ 16 parts; Described modification tar is that 100 parts of modification tar include 97 parts, tar, N-methyl pyrrole network alkane ketone 2 parts, ethylene glycol 1 part, is the product that three kinds of materials are in harmonious proportion.
Described compound powdered carbon is hard charcoal, sugar charcoal, the mixture of pitch coke weight ratio 1:2:7.
Described inclined clay powder reaches the substance A of more than 60% for first clay obtains weight ratio shared by the composition of metakaolin after Overheating Treatment, and substance A and white garnet, dextrin mix by weight 8.5:1.2:0.3, are inclined clay powder.
Described cutting powder is the cutting powder cutting silicon single crystal generation in monocrystalline silicon production process, and described main component is SiC50-70%; Elemental silicon 30-50%.
Further, the preparation method of described a kind of iron notch blast furnace mud, is characterized in that adopting following processing method to obtain: the first step produces stemming, by 3-1mm magnesia chrome spinel: 15 ~ 20 parts; 1-0mm corundum: 5 ~ 8 parts; 1-0mm sillimanite: 10 ~ 15 parts; 0.5-0mm magnesium oxide iron: 8 ~ 15 parts; Inclined clay powder: 8 ~ 13 parts; Cobalt oxide aluminium powder 3-7 part, cutting powder: 5 ~ 10 parts; Graphite Powder 99: 7 ~ 25 parts, compound powdered carbon 5-10 part, mid-temperature pitch powder: 1 ~ 2 part, puts into wheeled mixing pan, first pre-mixing 15 minutes; Then 85% of modification tar total amount is added, wet stone roller 35 minutes; Add 15% remaining modification tar, rewetting grinds 15 minutes; Through stemming microtome, then through mud extruder, squeeze mud shaping, be as cold as room temperature after cutting section, the crowded mud temperature in this step is set as 55 DEG C; Second step joins basting agent, by zirconic acid calcium powder, and Graphite Powder 99, potassium silicate solution is made into Homogeneous phase mixing liquid by weight 38:32:30 stirring and is basting agent, stand-by; 3rd step, smears surface by cooled stemming basting agent, reinstalls packing bag, be finished product after drying.
Beneficial effect of the present invention: the stemming adopting this technical scheme to produce and the used stemming of blast furnace contrast, use the iron notch aperture of stemming of the present invention very stable, there is not the situation that iron notch aperture obviously diminishes, also without the phenomenon of obvious reaming, meet completely blast furnace normally tap a blast furnace produce needs, for iron and steel enterprise and user have saved cost, effectively can improve current blast furnace due to the varying aperture of iron notch thus the molten iron discharging caused is unstable, the easy race caused due to flowing molten iron instability when tapping a blast furnace is flowed greatly, the problems such as flame arrow.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1: a kind of for 1080m3 blast furnace mud, is characterized in that described blast furnace mud is made up of the component of following weight part: 3-1mm magnesia chrome spinel: 20 parts; 1-0mm corundum: 8 parts; 1-0mm sillimanite: 15 parts; 0.5-0mm magnesium oxide iron: 15 parts; Inclined clay powder: 9 parts; Cobalt oxide aluminium powder 3 parts, cutting powder: 5 parts; Graphite Powder 99: 14 parts, compound powdered carbon 9 parts, cobaltosic oxide 1 part, mid-temperature pitch powder: 1 part; The preparation method of stemming: above-mentioned raw materials is put into mixing pan, first pre-mixing 15 minutes; Prepare 13 parts, modification tar, first add 85% of modification tar total amount, wet stone roller 35 minutes; Add 15% remaining modification tar, rewetting grinds 15 minutes; Through stemming microtome, then shaping through squeezing mud, be as cold as room temperature after cutting section, the crowded mud temperature in this step is set as 55 DEG C; Second step joins basting agent, by zirconic acid calcium powder, and Graphite Powder 99, potassium silicate solution is made into Homogeneous phase mixing liquid by weight 38:32:30 stirring and is basting agent, stand-by; 3rd step, smears surface by cooled stemming basting agent, reinstalls packing bag, be finished product after drying.
Embodiment 2: a kind of for 2500m3 blast furnace mud, is characterized in that described blast furnace mud is made up of the component of following weight part: 3-1mm magnesia chrome spinel: 19 parts; 1-0mm corundum: 7 parts; 1-0mm sillimanite: 14 parts; 0.5-0mm magnesium oxide iron: 15 parts; Inclined clay powder: 10 parts; Cobalt oxide aluminium powder 5 parts, cutting powder: 5 parts; Graphite Powder 99: 18 parts, compound powdered carbon 6 parts, mid-temperature pitch powder: 1 part.The preparation method of stemming: all raw materials are put into mixing pan, first pre-mixing 15 minutes; Prepare 14 parts, modification tar, first add 85% of modification tar total amount, wet stone roller 35 minutes; Add 15% remaining modification tar, rewetting grinds 15 minutes; Through stemming microtome, then through mud extruder, squeeze mud shaping, be as cold as room temperature after cutting section, the crowded mud temperature in this step is set as 55 DEG C; Second step joins basting agent, by zirconic acid calcium powder, and Graphite Powder 99, potassium silicate solution is made into Homogeneous phase mixing liquid by weight 38:32:30 stirring and is basting agent, stand-by; 3rd step, smears surface by cooled stemming basting agent, reinstalls packing bag, be finished product after drying.
Embodiment 3: a kind of for 3000m3 blast furnace mud, is characterized in that described blast furnace mud is made up of the component of following weight part: 3-1mm magnesia chrome spinel: 20 parts; 1-0mm corundum: 6 parts; 1-0mm sillimanite: 14 parts; 0.5-0mm magnesium oxide iron: 13 parts; Inclined clay powder: 10 parts; Cobalt oxide aluminium powder 5 parts, cutting powder: 5 parts; Graphite Powder 99: 20 parts, compound powdered carbon 6 parts, mid-temperature pitch powder: 1 part.The preparation method of stemming: all raw materials are put into the first pre-mixing of mixing pan 15 minutes; Prepare 15 parts, modification tar, first add 85% of modification tar total amount, wet stone roller 35 minutes; Add 15% remaining modification tar, rewetting grinds 15 minutes; Through stemming microtome, then through mud extruder, squeeze mud shaping, be as cold as room temperature after cutting section, the crowded mud temperature in this step is set as 55 DEG C; Second step joins basting agent, by zirconic acid calcium powder, and Graphite Powder 99, potassium silicate solution is made into Homogeneous phase mixing liquid by weight 38:32:30 stirring and is basting agent, stand-by; 3rd step, smears surface by cooled stemming basting agent, reinstalls packing bag, be finished product after drying.
Embodiment 4: a kind of for 3200m3 blast furnace mud, is characterized in that described blast furnace mud is made up of the component of following weight part: 3-1mm magnesia chrome spinel: 15 parts; 1-0mm corundum: 8 parts; 1-0mm sillimanite: 11 parts; 0.5-0mm magnesium oxide iron: 11 parts; Inclined clay powder 10 parts; Cobalt oxide aluminium powder 7 parts, cutting powder: 10 parts; Graphite Powder 99: 20 parts, compound powdered carbon 5 parts, cobaltosic oxide 1 part, mid-temperature pitch powder: 2 parts.The preparation method of stemming: all raw materials are put into mixing pan, first pre-mixing 15 minutes; Prepare 16 parts, modification tar, first add 85% of modification tar total amount, wet stone roller 35 minutes; Add 15% remaining modification tar, rewetting grinds 15 minutes; Through stemming microtome, then through mud extruder, squeeze mud shaping, be as cold as room temperature after cutting section, the crowded mud temperature in this step is set as 55 DEG C; Second step joins basting agent, by zirconic acid calcium powder, and Graphite Powder 99, potassium silicate solution is made into Homogeneous phase mixing liquid by weight 38:32:30 stirring and is basting agent, stand-by; 3rd step, smears surface by cooled stemming basting agent, reinstalls packing bag, be finished product after drying.
Comparative example: the used stemming of blast furnace will be tested, carry out performance comparison with stemming of the present invention; The use properties detected result of above-described embodiment 1 ~ 4 and comparative example the results are shown in following table (experimental period is 3 months).
Product of the present invention uses through curstomer's site workman, unanimously thinks: easily beat mud, iron mouth appropriate depth, and the mean pressure big gun time is short, and rapidly, anti-slag iron aggressiveness is good for sintering, and iron notch aperture is stablized, and taps a blast furnace stable, without spray rocket phenomenon.
This specific embodiment is only explanation of the invention; it is not the restriction to invention; those skilled in the art can make any amendment to the present embodiment after reading this specification as required, as long as but be all subject to the protection of patent law in right of the present invention.
Claims (5)
1. an iron notch blast furnace mud, is characterized in that described blast furnace mud is made up of the component of following weight part: 3-1mm magnesia chrome spinel: 15 ~ 20 parts; 1-0mm corundum: 5 ~ 8 parts; 1-0mm sillimanite: 10 ~ 15 parts; 0.5-0mm magnesium oxide iron: 8 ~ 15 parts; Inclined clay powder: 8 ~ 13 parts; Cobalt oxide aluminium powder 3-7 part, cutting powder: 5 ~ 10 parts; Graphite Powder 99: 7 ~ 25 parts, compound powdered carbon 5-10 part, tricobalt tetroxide 0 ~ 1 part, mid-temperature pitch powder: 1 ~ 2 part; Additional modification tar: 13 ~ 16 parts; Described modification tar is that 100 parts of modification tar include 97 parts, tar, N-methyl pyrrole network alkane ketone 2 parts, ethylene glycol 1 part, through the product that three kinds of materials are in harmonious proportion.
2. a kind of iron notch blast furnace mud according to claim 1, is characterized in that: described compound powdered carbon is hard charcoal, sugar charcoal, pitch coke three kinds of substance weights are than the mixture of 1:2:7.
3. a kind of iron notch blast furnace mud according to claim 1, it is characterized in that: described inclined clay powder reaches the substance A of more than 60% for first clay obtains weight ratio shared by the composition of metakaolin after Overheating Treatment, substance A mixes by weight 8.5:1.2:0.3 with white garnet, dextrin, is inclined clay powder.
4. a kind of iron notch blast furnace mud according to claim 1, is characterized in that: described cutting powder is the cutting powder cutting silicon single crystal generation in monocrystalline silicon production process, and described main component is SiC50-70%, elemental silicon 30-50%.
5. the preparation method of a kind of iron notch blast furnace mud as claimed in claim 1, is characterized in that adopting following processing method to obtain: the first step produces stemming, by 3-1mm magnesia chrome spinel: 15 ~ 20 parts; 1-0mm corundum: 5 ~ 8 parts; 1-0mm sillimanite: 10 ~ 15 parts; 0.5-0mm magnesium oxide iron: 8 ~ 15 parts; Inclined clay powder: 8 ~ 13 parts; Cobalt oxide aluminium powder 3-7 part, cutting powder: 5 ~ 10 parts; Graphite Powder 99: 7 ~ 25 parts, compound powdered carbon 5-10 part, tricobalt tetroxide 0 ~ 1 part, mid-temperature pitch powder: 1 ~ 2 part, puts into wheeled mixing pan, first pre-mixing 15 minutes; Then 85% of modification tar total amount is added, wet stone roller 35 minutes; Add 15% remaining modification tar, rewetting grinds 15 minutes; Through stemming microtome, then through mud extruder, squeeze mud shaping, be as cold as room temperature after cutting section, the crowded mud temperature in this step is set as 55 DEG C; Second step joins basting agent, by zirconic acid calcium powder, and Graphite Powder 99, potassium silicate solution is made into Homogeneous phase mixing liquid by weight 38:32:30 stirring and is basting agent, prepares stand-by; 3rd step, smears surface by cooled stemming basting agent, reinstalls packing bag, be finished product after drying.
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| CN201510735389.9A CN105254315A (en) | 2015-11-03 | 2015-11-03 | Blast-furnace stemming for tapping hole |
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| CN201510735389.9A CN105254315A (en) | 2015-11-03 | 2015-11-03 | Blast-furnace stemming for tapping hole |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102603312A (en) * | 2011-12-09 | 2012-07-25 | 河北省首钢迁安钢铁有限责任公司 | Anhydrous stemming for maintaining blast-furnace hearth and preparation method of anhydrous stemming |
| CN102757241A (en) * | 2011-04-25 | 2012-10-31 | 宝山钢铁股份有限公司 | Stemming and purpose thereof |
| CN103979985A (en) * | 2014-05-15 | 2014-08-13 | 武汉钢铁(集团)公司 | Environment-friendly converter bedding-face repairing material and preparation method thereof |
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- 2015-11-03 CN CN201510735389.9A patent/CN105254315A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102757241A (en) * | 2011-04-25 | 2012-10-31 | 宝山钢铁股份有限公司 | Stemming and purpose thereof |
| CN102603312A (en) * | 2011-12-09 | 2012-07-25 | 河北省首钢迁安钢铁有限责任公司 | Anhydrous stemming for maintaining blast-furnace hearth and preparation method of anhydrous stemming |
| CN103979985A (en) * | 2014-05-15 | 2014-08-13 | 武汉钢铁(集团)公司 | Environment-friendly converter bedding-face repairing material and preparation method thereof |
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Application publication date: 20160120 |