CN105243599A - Method for building rice storage quality evaluation model - Google Patents

Method for building rice storage quality evaluation model Download PDF

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CN105243599A
CN105243599A CN201510669442.XA CN201510669442A CN105243599A CN 105243599 A CN105243599 A CN 105243599A CN 201510669442 A CN201510669442 A CN 201510669442A CN 105243599 A CN105243599 A CN 105243599A
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storage
rice
indicators
quality
storage quality
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王立峰
张怡一
夏金林
陈静宜
何荣
鞠兴荣
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Nanjing University of Finance and Economics
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Nanjing University of Finance and Economics
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Abstract

本发明公开了一种大米储藏品质评价模型的构建方法。筛选影响大米储藏品质的敏感性指标,从多项指标中找出与储藏时间与储藏方式相关性较好的指标作为敏感性指标,对上述指标进行方差分析确定脂肪酸值、还原糖含量、硬度以上三个指标为评价储藏品质的敏感性指标,再进行二次多项式回归分析,进而建立大米储藏品质评价模型:Y/10=-1.281+0.074*X1+3.845*X2+0.0011*X3。本发明方法可以评价利用并有效避免储藏过程中对大米的蒸煮品质和食用品质的下降,可行性并且适应性好。The invention discloses a method for constructing a rice storage quality evaluation model. Screen the sensitivity indicators that affect the storage quality of rice, and find out the indicators that have a good correlation with the storage time and storage method from the multiple indicators as the sensitivity indicators, and perform variance analysis on the above indicators to determine the fatty acid value, reducing sugar content, and hardness. The three indicators are the sensitivity indicators for evaluating the storage quality, and the quadratic polynomial regression analysis is carried out to establish the rice storage quality evaluation model: Y/10=-1.281+0.074*X 1 +3.845*X 2 +0.0011*X 3 . The method of the invention can evaluate, utilize and effectively avoid the reduction of cooking quality and eating quality of rice during storage, and has good feasibility and adaptability.

Description

一种大米储藏品质评价模型的构建方法A method for constructing a rice storage quality evaluation model

技术领域technical field

本发明涉及大米陈化模型的建立,该方法属于农业生产技术领域,具体涉及一种大米储藏品质评价模型的构建方法。The invention relates to the establishment of a rice aging model, and the method belongs to the technical field of agricultural production, in particular to a method for constructing a rice storage quality evaluation model.

背景技术Background technique

大米是我国人民的重要食品之一,由于没有稻壳保护,胚乳直接暴露在外,因此对外界温度、湿度、氧气浓度影响较为敏感;同时,害虫及霉菌的直接侵袭,导致大米营养物质流失加速,极易发生陈化降低储藏品质。Rice is one of the important foods of our people. Since there is no protection of rice husk and the endosperm is directly exposed, it is more sensitive to the influence of external temperature, humidity and oxygen concentration; at the same time, the direct invasion of pests and molds leads to accelerated loss of rice nutrients. It is prone to aging and reduces the storage quality.

与大米中含量较多的淀粉与蛋白质相比,脂类更容易导致大米陈化变质,在储藏中脂类受到空气和高温的影响,极易加速大米劣变的速度,导致大米食用品质下降,因此我国现行稻谷储存品质判定规则(GB/T20569-2006)是以游离脂肪酸值为标准来反映粮食的劣变程度和储存品质。然而,大米储藏品质的变化是一个动态过程,由于储藏过程中各指标变化敏感性不同,对大米新鲜度的影响存在着不同程度的差异,不能用一个孤立的指标来评价其储藏品质,因此建立一种科学有效的品质评价方法对大米的良好储藏具有实际意义,目前相关的研究报道很少。Compared with starch and protein in rice, lipids are more likely to cause aging and deterioration of rice. During storage, lipids are affected by air and high temperature, which can easily accelerate the rate of rice deterioration, resulting in a decline in the eating quality of rice. Therefore, my country's current rice storage quality judgment rules (GB/T20569-2006) use the free fatty acid value as a standard to reflect the degree of grain deterioration and storage quality. However, the change of rice storage quality is a dynamic process. Due to the different sensitivities of various indicators during the storage process, there are differences in the impact on the freshness of rice. An isolated indicator cannot be used to evaluate its storage quality. Therefore, the establishment of A scientific and effective quality evaluation method has practical significance for the good storage of rice, but there are few relevant research reports so far.

发明内容Contents of the invention

本发明要解决的问题是提供一个大米储藏品质的评价模型的构建方法,本方法利用方差分析(ANOVA)法筛选大米敏感性指标,并利用二次多项式回归分析法建立一种快速、准确的大米储藏品质评价指标体系。The problem to be solved by the present invention is to provide a method for constructing an evaluation model of rice storage quality. The method utilizes the analysis of variance (ANOVA) method to screen the rice sensitivity index, and utilizes the quadratic polynomial regression analysis method to establish a fast and accurate rice Storage quality evaluation index system.

为实现上述目的,本发明采用的技术方案是:In order to achieve the above object, the technical scheme adopted in the present invention is:

一种大米储藏品质评价模型的构建方法,A method for constructing a rice storage quality evaluation model,

(1)模拟大米储藏实验,筛选影响大米储藏品质的敏感性指标,对储藏大米脂肪酸值、总酸值、还原糖含量、硬度、糊化温度指标进行测定。(1) Simulate the rice storage experiment, screen the sensitive indicators that affect the rice storage quality, and measure the stored rice fatty acid value, total acid value, reducing sugar content, hardness, and gelatinization temperature indicators.

(2)从多项指标中找出与储藏时间与储藏方式相关性较好的指标作为敏感性指标,采用方差分析法对(1)中的指标进行储藏品质敏感度的筛选;(2) Find the index with better correlation with storage time and storage mode from multiple indexes as the sensitivity index, and use variance analysis to screen the index in (1) for the sensitivity of storage quality;

(3)利用二次多项式回归分析法建立大米储藏品质评价模型:(3) Using quadratic polynomial regression analysis to establish a rice storage quality evaluation model:

Y/10=-1.281+0.074*X1+3.845*X2+0.0011*X3Y/10=-1.281+0.074*X1 + 3.845*X2 + 0.0011* X3 ;

其中,Y为储藏时间,X1为脂肪酸值,mgKOH/100g干物质;X2为还原糖含量,mg葡萄糖/100g试样;X3为硬度,g。Among them, Y is the storage time, X1 is the fatty acid value, mgKOH/100g dry matter ; X2 is the reducing sugar content, mg glucose/100g sample; X3 is the hardness, g.

本发明所具有的优点是:The advantages that the present invention has are:

1.本发明建立了一种大米储藏品质评价模型,筛选敏感指标确立一个评价指标体系预测储藏品质比单一指标更为准确、可靠。1. The present invention establishes a rice storage quality evaluation model, and screening sensitive indicators to establish an evaluation index system to predict storage quality is more accurate and reliable than a single index.

2.本发明可以评价利用并有效避免储藏过程中对大米的蒸煮品质和食用品质的下降,可行性并且适应性好。2. The present invention can evaluate the use and effectively avoid the decline of the cooking quality and eating quality of rice during storage, and has good feasibility and adaptability.

3.本发明所涉及实验不繁琐,方便且数据准确,能够客观地反映储藏中大米品质的变化,实践中易行。3. The experiment involved in the present invention is not complicated, convenient and accurate in data, can objectively reflect the change of rice quality in storage, and is easy to implement in practice.

具体实施方式detailed description

下面结合实施例对本发明作进一步阐述,但不因此而现在本发明。The present invention will be further elaborated below in conjunction with embodiment, but does not therefore present the present invention.

实施例1Example 1

一种大米储藏品质评价模型的构建方法,包括以下步骤:A method for constructing a rice storage quality evaluation model, comprising the following steps:

(1)模拟储藏实验:采用市售编织袋包装大米样品,置于温度为15、25、30℃(60%RH)的人工气候箱中下模拟储藏实验。(1) Simulated storage experiment: Rice samples were packaged in commercially available woven bags, and placed in artificial climate chambers at temperatures of 15, 25, and 30° C. (60% RH) for simulated storage experiments.

(2)筛选储藏品质敏感性指标:在保留《稻谷储存品质判定规则》中脂肪酸指标的基础上,增加总酸值、还原糖含量、硬度、糊化温度指标,从多项指标中找出与储藏时间与储藏方式相关性较好的指标作为敏感性指标。对上述指标进行方差分析,与储藏时间与储藏方式都呈现显著性关系(P<0.05显著,P<0.01极其显著)的指标有:脂肪酸值、还原糖含量、硬度,选定以上三个指标为评价储藏品质的敏感性指标。(2) Screening storage quality sensitivity indicators: on the basis of retaining the fatty acid indicators in the "Rice Storage Quality Judgment Rules", increase the indicators of total acid value, reducing sugar content, hardness, and gelatinization temperature, and find out from a number of indicators that are closely related to The index with better correlation between storage time and storage method was used as the sensitivity index. Carry out variance analysis on the above indicators, and the indicators that have a significant relationship with the storage time and storage method (P<0.05 is significant, P<0.01 is extremely significant) include: fatty acid value, reducing sugar content, hardness, and the above three indicators are selected as Sensitive index for evaluating storage quality.

表1.Table 1.

储藏时间storage time 自由度degrees of freedom 平方和sum of square 均方mean square Ff 显著性significant 脂肪酸fatty acid 22 67612.57367612.573 1679.8211679.821 26.000026.0000 **** 总酸Acid value 22 30.38330.383 .069.069 4.9564.956 还原糖含量Reducing sugar content 55 2.0562.056 .411.411 653.484653.484 **** 硬度hardness 55 5.848E75.848E7 1.170E71.170E7 54.79154.791 **** 糊化温度gelatinization temperature 44 1558.0221558.022 389.505389.505 32.05932.059 储藏方式storage method 自由度degrees of freedom 平方和sum of square 均方mean square Ff 脂肪酸fatty acid 22 203.238203.238 101.619101.619 1.5731.573 总酸Acid value 22 .056.056 .028.028 2.0252.025 还原糖含量Reducing sugar content 22 .017.017 .008.008 13.28013.280 ****

硬度hardness 22 176366.144176366.144 88183.07288183.072 .413.413 糊化温度gelatinization temperature 22 53.57053.570 26.78526.785 2.2052.205

*表示P<0.05,显著相关;**表示P<0.01,极显著相关。* means P<0.05, significant correlation; ** means P<0.01, extremely significant correlation.

根据方差分析表查临界F值得:Check the critical F value according to the variance analysis table:

其中,改变储藏时间后,脂肪酸:F0.05(2,18)=3.55,F0.01(2,18)=6.01,因为F>F0.01(2,18),即P<0.01,故认为储藏时间对脂肪酸有显著影响。还原糖:F0.05(2,18)=3.55,F0.01(2,18)=6.01,因为F>F0.01(2,18),即P<0.01,故认为储藏时间对还原糖有显著影响。硬度:F0.05(5,16)=3.01,F0.05(5,16)=4.77,因为F>F0.05(5,16,即P<0.01,故认为储藏时间对硬度有显著影响;而改变储藏方式后,还原糖含量:F0.05(2,12)=3.26,F0.0,1(2,12)=5.41,因为F>F0.0,1(2,12),即P<0.01,故认为储藏方式对还原糖含量有显著影响。Among them, after changing the storage time, the fatty acid: F 0.05(2,18) = 3.55, F 0.01(2,18) = 6.01, because F>F 0.01(2,18) , that is, P<0.01, so it is considered that the storage time is Fatty acids have a significant effect. Reducing sugar: F 0.05(2,18) =3.55, F 0.01(2,18) =6.01, because F>F 0.01(2,18) , that is, P<0.01, it is considered that storage time has a significant impact on reducing sugar. Hardness: F 0.05(5,16) =3.01, F 0.05(5,16) =4.77, because F>F 0.05(5,16 , that is, P<0.01, it is considered that storage time has a significant impact on hardness; and changing storage After the method, reducing sugar content: F 0.05(2,12) = 3.26, F 0.0,1(2,12) = 5.41, because F>F 0.0,1(2,12) , that is, P<0.01, so it is considered that the storage The method had a significant effect on the reducing sugar content.

(3)建立大米储藏品质预测模型:(3) Establish a rice storage quality prediction model:

由上述可知,储藏时间对大米中脂肪酸含量、还原糖含量以及硬度这三个指标有极显著影响,根据实验所得数据由JMP软件进行回归分析所得:大米敏感性指标对储藏时间的回归计算公式为:It can be known from the above that the storage time has a very significant impact on the three indicators of fatty acid content, reducing sugar content and hardness in rice. According to the data obtained from the experiment, the regression analysis of the JMP software is obtained: the regression calculation formula of the rice sensitivity index on the storage time is :

Y/10=-1.281+0.074*X1+3.845*X2+0.0011*X3Y/10=-1.281+0.074*X1 + 3.845*X2 + 0.0011* X3 ;

F=94.858;相关系数R=0.922。F=94.858; correlation coefficient R=0.922.

以下公式中,Y为储藏时间,X1为脂肪酸值,mgKOH/100g干物质;X2为还原糖含量,mg葡萄糖/100g试样;X3为硬度,g。In the following formula, Y is storage time, X 1 is fatty acid value, mgKOH/100g dry matter; X 2 is reducing sugar content, mg glucose/100g sample; X 3 is hardness, g.

验证模型:Validation model:

1.将编织袋包装大米于15℃人工气候箱储藏30、60、90、120天后1. Store rice packed in woven bags in an artificial climate box at 15°C for 30, 60, 90, and 120 days

2.将编织袋包装大米于25℃人工气候箱储藏30、60、90、120天后2. Store rice packed in woven bags in an artificial climate box at 25°C for 30, 60, 90, and 120 days

3.将编织袋包装大米于30℃人工气候箱储藏30、60、90、120天后3. Store rice packed in woven bags in an artificial climate box at 30°C for 30, 60, 90, and 120 days

由上述可知,该回归方程基本满足。It can be seen from the above that the regression equation is basically satisfied.

Claims (1)

1.一种大米储藏品质评价模型的构建方法,其特征在于,筛选影响大米储藏品质的敏感性指标,从多项指标中找出与储藏时间与储藏方式相关性较好的指标作为敏感性指标,对上述指标进行方差分析确定脂肪酸值、还原糖含量、硬度以上三个指标为评价储藏品质的敏感性指标,再进行二次多项式回归分析,进而建立大米储藏品质评价模型:Y/10=-1.281+0.074*X1+3.845*X2+0.0011*X3;其中,Y为储藏时间,X1为脂肪酸值,mgKOH/100g干物质;X2为还原糖含量,mg葡萄糖/100g试样;X3为硬度,g。1. A method for constructing a rice storage quality evaluation model, characterized in that, screening sensitivity indicators that affect rice storage quality, finding an indicator that has better correlation with storage time and storage mode from multiple indicators as a sensitivity indicator , carry out analysis of variance to above-mentioned index and determine fatty acid value, reducing sugar content, the above three indexes of hardness are the sensitivity indexes of evaluating storage quality, then carry out quadratic polynomial regression analysis, and then establish the rice storage quality evaluation model: Y/10=- 1.281+0.074*X 1 +3.845*X 2 +0.0011*X 3 ; wherein, Y is storage time, X 1 is fatty acid value, mgKOH/100g dry matter; X 2 is reducing sugar content, mg glucose/100g sample; X 3 is hardness, g.
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