CN105231565A - Stab-resistant protective fabric comprising ice-cold material - Google Patents
Stab-resistant protective fabric comprising ice-cold material Download PDFInfo
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Abstract
The invention discloses stab-resistant protective fabric comprising an ice-cold material. The key points of the technical scheme are that plain woven fabric, produced from any one of ultrahigh-molecular-weight polyethylene fiber, aromatic polyamide fiber, poly(p-phenylene benzobisoxazole) fiber, carbon fiber, high-strength polyester fiber and man-made spider fiber, is taken as a base layer, and a plurality of base layers are arranged. Coolking fiber or Coolplus fiber capable of absorbing moisture and discharging sweat is blended in the fiber of the base layers. Shearing and thickening fluid is uniformly attached on the base layers and composited with the base layers by utilizing a static soaking method. The stab-resistant protective fabric has the advantages of softness, breathability and comfortability, is close to common fabric in comfortability when being used normally, and has sufficient strength when being impacted by external force; and daily office activity needs of policemen or other working personnel using the stab-resistant fabric can be met.
Description
Technical field
The present invention relates to protective materials technical field, more particularly, it relates to a kind of anti-stab protective fabric containing ice-cold material.
Background technology
Along with the process of global economic integration, various exchange activity is day by day frequent, and time particularly current terrorism and violence come back to some extent, people's self-protection consciousness strengthens gradually.Anti-terrorism becomes the event that international especially developed country receives much concern, and therefore the exploitation of individual protection product is also able to fast development.
For the many countries comprising China, the use management of firearms is strict, and the threat that army and police, law enforcement officer etc. face the sharp instruments such as dagger, cone, pin is relatively many, and the research and development of stab-resistant material is more and more come into one's own.Tradition stab-resistant material is thick and heavy, volume is large, dumb, only can protect the metastomium of limbs, and available protecting cannot be carried out to some joint parts such as knee etc., be faced with the contradiction that barrier propterty and flexibility are difficult to take into account, recent years is along with Kevlar, UHMWPE, PBO, the appearance of the contour performance synthetic fibers of carbon fiber, also high-performance fiber can be adopted to make lightweight flexible, be convenient to the stab-resistant material worn, but compared to common cloth, the gas permeability of this kind of stab-resistant material, comfortableness is poor, especially can seem abnormal sultry under the condition of high temperature in summer, if reduce the content of high-performance synthetic fibers, anti-stab hydraulic performance decline can be caused.
Summary of the invention
The object of the present invention is to provide a kind of comfortableness well to have the anti-stab protective materials of good anti-stab performance concurrently simultaneously.
For achieving the above object, the invention provides following technical scheme:
A kind of anti-stab protective fabric containing ice-cold material, this protective materials is with superhigh molecular weight polyethylene fibers, aromatic polyamide fibre, poly-wherein any one plain cloth to penylene benzo-dioxazole fiber, carbon fiber, high-strength polyester fibers, imitative spider silk fiber for basic unit, and this basic unit's multilayer is arranged;
In fiber in this basic unit, blending has Coolking fiber or the Coolplus fiber of energy moisture absorbing and sweat releasing;
This basic unit is evenly attached with shear thickening fluid, by utilizing static dipping method by shear thickening fluid and basic unit's compound.
Further setting: have modified nanoparticles in described shear thickening fluid, described nano particle is the SiO2 particle of different-grain diameter, and the mass fraction of described SiO2 particle is between 40%-45%.
Further setting: the particle diameter of described SiO2 particle is 160-380nm or 510-600nm.
Further setting: described basic unit is made up of netted pilotaxitic texture, basic unit is 20-500g/m
2surface density is containing microcellular structure, and have the aperture of 0.0l-0.3mm, porosity is not less than 10%.
Further setting: be compounded with resin matrix between described multilayer basic unit, described resin matrix is selected from high density polyethylene (HDPE).
Setting like this, adopt the basic unit that high-performance synthetic fibers are made, there is very high tensile property, elastic modelling quantity and energy absorption, but cost is higher, and do not possess the comfortableness of common fabric, in the fiber being made into basic unit, blending simultaneously enters Coolking fiber or Coolplus fiber, Coolking fiber or Coolplus fiber belong to new function fiber, fibre section is "+" type, surface is micro-grooves, there is countless trickle cavity, by the capillarity that these micro-grooves produce, the moisture of discharge skin surface and sweat spread via wicking, the effects such as transmission, Quick diffusing moisture and sweat, human body surface is made to keep dry and comfortable, refrigerant, comfortable, there is the effect of regulate body temperature.
In addition, this basic unit is also attached with shear thickening fluid, shear thickening fluid can enter in the micro-grooves in fiber and between fiber or in micro-control structure, the inside of shear thickening fluid there is nano particle, when being hit or compress, shear thickening fluid just becomes hard solid, absorb and consume impact energy, make fabric stronger and be difficult to be pierced, effectively improve barrier propterty, on the other hand, the nano particle be filled in the micro-grooves of fiber or micro-control structure adds the frictional force between fiber, further stop and elimination external impacts, thus play the effect improving protection effect.
When not by external impacts, shear thickening fluid keeps not changing, under this state, in the micro-grooves between the fiber in basic unit or micro-control structure do not filled by solid-state shear thickening fluid, keep original function, produce capillarity and carry out moisture absorbing and sweat releasing.
Adopt high-performance synthetic fibers and new function fiber blend, the use decreasing high-performance synthetic fibers relative under equal unit, and then reduce cost, simultaneously, basic unit is compounded with resin matrix, one is carried out to minimizing high-performance synthetic fibers and supplements, reach corresponding anti-stab requirement.
Further, the nano particle in shear thickening fluid is preferably SiO2, and carry out modification to it, modified SiO2 mass fraction is 40% ~ 45% time, and anti-stab ability can improve 1.66 times.
Realize the preparation method of a kind of anti-stab protective fabric containing ice-cold material of the present invention, comprise the following steps: (1) blending: adopt preferred superhigh molecular weight polyethylene fibers and the blending in advance of preferred Coolking fiber to make spun yarn, wherein, described superhigh molecular weight polyethylene fibers fineness is 1-150tex, and described Coolking fibre fineness is 1-85tex;
(2) weave: the spun yarn plain weave after blending is become to weave cotton cloth, and this to weave cotton cloth be weave in the mode of well word weaving closely, yarn linear density is 420-1400D; Mechanical strength is not less than 30cN/dtex; Woven fabric specification is for being 65-150 root/10cm through close and filling density; Fabric side density is 60-200g/m
2; Fabric thickness is 0.1-0.35mm;
(3) flood: adopt ball-milling method to prepare shear thickening fluid, by dispersed for modified nanoparticles in shear thickening fluid, then by scattered mixed liquor dipping plain cloth;
(4) dry: drying, encapsulation are carried out to the composite flooded.
Further setting: described basic unit and resin matrix adopt hot pressing compound, comprise the following steps, (1) pretreatment: plain cloth is carried out drying, time 1h, temperature 105 DEG C, carries out drying by resin matrix, time 2h, temperature 60 C;
(2) lamination: resin matrix and plain cloth are superimposed together by a graded, different superposition order will obtain the resin compounded layer of different structure, spaced apart with polytetrafluoroethylene (PTFE) release cloth between each composite bed;
(3) pressing: by the resin matrix that is superimposed and plain cloth preheating, then adopts press pressing, and heating certain hour, forms composite bed;
Further setting: described resin matrix and plain cloth have three kinds of complex methods: ABA, BAB, AB, wherein, A is resin matrix, and B is plain cloth.
By adopting technique scheme, hinge structure of the present invention is compared to be had: this anti-stab protective fabric not only has enough intensity, have excellent pliability and gas permeability concurrently simultaneously, under the state usually used, close to the comfort level of common fabric, by having enough intensity during external impacts, meeting and using the police of anti-stabbing lining or the routine office work activity need of other staff.
Accompanying drawing explanation
Fig. 1 is the pilotaxitic texture schematic diagram of a kind of anti-stab protective fabric containing ice-cold material of the present invention;
Fig. 2 is a kind of yarn schematic diagram of the anti-stab protective fabric containing ice-cold material;
Fig. 3 is a kind of hierarchical structure schematic diagram of the anti-stab protective fabric containing ice-cold material.
In figure: 1, one deck basic unit; 2, yarn; 21, superhigh molecular weight polyethylene fibers; 22, Coolking fiber; A, resin matrix; B, plain cloth.
Detailed description of the invention
Referring to figs. 1 through Fig. 3, a kind of anti-stab protective fabric embodiment containing ice-cold material of the present invention is described further.
In the present invention, high-performance synthetic fibers are preferably superhigh molecular weight polyethylene fibers, and new function fiber is preferably Coolplus fiber, the resin matrix of compound between multilayer basic unit, preferred high-density polyethylene material, the thin film be made up of high density polyethylene (HDPE).
In the present invention, nano particle in shear thickening fluid is preferably, be preferably SiO2, in the present invention, the preparation method of SiO2 is specific as follows: tetraethyl orthosilicate, ethanol, deionized water are mixed with solution by volume at 1: 2: 2, solution warms to 70 DEG C is stirred 1.5h, add appropriate catalyst in the solution again, milk white gel is formed after continuing to stir 1h, pH controls 5 ~ 6, after having reacted, and ageing, dry, grind to obtain gel powder, through Muffle furnace after 600 DEG C of high-temperature roasting 1 ~ 2h, obtain SiO2 powder.
Further, modification is carried out to the SiO2 powder obtained, the method of modification is specific as follows: the deionized water of the absolute ethyl alcohol of volume fraction 95% and 5% mixed, add the KH570 surfactant of volume fraction 6%, reaction 40-50min facilitation of hydrolysis and formation hydroxyl, add the single dispersing SiO2 nano particle prepared, and continues at 78 DEG C of reaction 60-80min after stirring, treat that particle sinks to bottom and liquid part poured out, with absolute ethyl alcohol rinsing 3 times.By modified SiO2 nanoparticulate dispersed to volume ratio be 1: 5 PEG, in absolute ethyl alcohol mixed liquor, with absolute ethanol washing 3 times after reaction 4-5h, 80 DEG C of dry 12h.Modified SiO2 mass fraction controls between 40% ~ 45%, and particle diameter is that son is between 160-380nm or 510-600n.
Embodiment one
The container that PEG200 is housed is fixed on miniature whirlpool mixed instrument, mass fraction 40% is added gradually in Vibratory Mixing process, average particle size is about 160nm, through the SiO2 nano particle of surface graft modification, Vibratory Mixing 2-3h, makes SiO2 be dispersed in decentralized medium PEG200 and forms shear thickening fluid.
Superhigh molecular weight polyethylene fibers and the blending in advance of Coolking fiber is adopted to make spun yarn, then plain weave is carried out, the fabric of braiding is netted pilotaxitic texture, stacked 16 layers jointly, this fabric, composition basic unit, fabric mechanical strength as basic unit is not less than 30cN/dtex, and woven fabric specification is for being 65-150 root/10cm through close and filling density; The surface density of basic unit is 197g/m
2surface density is containing microcellular structure, and have the aperture of 0.01-0.3mm, porosity about 15%, fabric thickness is 0.1-0.35mm.
By resin matrix film and the drying respectively of plain weave cloth, plain cloth: time 1h, temperature 105 DEG C, resin matrix: time 2h, temperature 60 C.Then resin matrix film and plain weave cloth being superimposed together by a graded, can be the mode lamination according to ABA, BAB, AB, in this programme, is preferably the mode of BAB, finally adopts press hot pressing compound.Wherein, A is resin matrix, and B is plain cloth.
It is to be understood that being superimposed together by a graded is superposition in order to orderly, refer to the overlay order of monolithic can not destroy compacting before overlay order, otherwise its anti-stab ability will decline.Why emphasizing will to peel off in order after suppressing in order superposition is because the face making guarantee base material like this and face can the face of carrying out of " fully " contact, and has avoided " cavity " to occur.
Plain weave cloth is cut into the sample of 42mm × 38mm, absolute ethyl alcohol is adopted to dilute by 1: 1 (mass ratio) the fluid prepared, being immersed by plain weave cloth after drying process is immersed in diluted system, take out after leaving standstill a period of time, the solution of removing excess surface, then put into 70 DEG C of dry 20min of air dry oven to remove alcohol solvent.
Comparative example one, takes the preparation method of embodiment one, but in example one, deduct the step that blending enters Coolking fiber, and other conditions are constant, make the stab-resistant material of identical faces density, the number of plies.
Comparative example two, takes the preparation method of embodiment one, but in example one, deduct the step adding resin matrix film, and other conditions are constant.
Comparative example three, takes the preparation method of embodiment one, but when example one prepares basic unit, by stacked 24 layers jointly, fabric.
By the cloth prepared by embodiment one, comparative example one, comparative example two, comparative example three, carry out gas permeability and detect and anti prick function detection.
Carry out gas permeability detection: adopt application number to be checkout equipment in the Chinese patent of 201120091799.1 and method, cloth is placed on the upper orifice of lower pipe, then joint sleeve is put, air penetration under observing in pipe is to the amount in upper pipe, in the water of upper pipe, form obvious bubble, directly draw the gas permeability of cloth.
Anti prick function detecting portion: sample is fixed on fixed mount, employing quality of dropping hammer is 2.40kg, drop hammer by magnet control on height-adjustable crossbeam, by regulating the distance adjustment impact energy of dropping hammer and between sample, dropping hammer during puncture experiment and doing the movement of falling object.Each sample is often planted test and is carried out 3 times, and the distance between each test point and between test point and sample edge is not less than 5cm, observes the number of plies that sample is pierced after test.
Table 1 (embodiment one and comparative example one to three products Performance comparision)
| Sequence number | The number of plies | Pierce through the number of plies | Gas permeability | Comfortableness |
| Embodiment one | 16 | 12 | Better | Soft |
| Comparative example one | 16 | 12 | Difference | Soft |
| Comparative example two | 16 | 16 | Good | Soft |
| Comparative example three | 24 | 13 | Better | Harder |
16 layers of compound fabric of embodiment one gained are placed in by the anti-stab standard NIJ0115.0 of America NI J and national standard GA68-2008 testing standard, result all meets standard-required, also find out from above-mentioned table 1, the preparation method of embodiment one obtains a comparatively suitable product, as preferred embodiment of the present invention.
Embodiment two
The container that PEG200 is housed is fixed on miniature whirlpool mixed instrument, mass fraction 40% is added gradually in Vibratory Mixing process, average particle size is about 370nm, through the SiO2 nano particle of surface graft modification, Vibratory Mixing 2-3h, makes SiO2 be dispersed in decentralized medium PEG200 and forms shear thickening fluid.
Superhigh molecular weight polyethylene fibers and the blending in advance of Coolking fiber is adopted to make spun yarn, then plain weave is carried out, the fabric of braiding is netted pilotaxitic texture, stacked 16 layers jointly, this fabric, composition basic unit, fabric mechanical strength as basic unit is not less than 30cN/dtex, and woven fabric specification is for being 65-150 root/10cm through close and filling density; The surface density of basic unit is 197g/m
2surface density is containing microcellular structure, and have the aperture of 0.01-0.3mm, porosity about 15%, fabric thickness is 0.1-0.35mm.
By resin matrix film and the drying respectively of plain weave cloth, plain cloth: time 1h, temperature 105 DEG C, resin matrix: time 2h, temperature 60 C.Then resin matrix film and plain weave cloth being superimposed together by a graded, can be the mode lamination according to ABA, BAB, AB, in this programme, is preferably the mode of BAB, finally adopts press hot pressing compound.Wherein, A is resin matrix, and B is plain cloth.
Plain weave cloth is cut into the sample of 42mm × 38mm, absolute ethyl alcohol is adopted to dilute by 1: 1 (mass ratio) the fluid prepared, being immersed by plain weave cloth after drying process is immersed in diluted system, take out after leaving standstill a period of time, the solution of removing excess surface, then put into 70 DEG C of dry 20min of air dry oven to remove alcohol solvent.
Embodiment three
The container that PEG200 is housed is fixed on miniature whirlpool mixed instrument, mass fraction 40% is added gradually in Vibratory Mixing process, average particle size is about 600nm, through the SiO2 nano particle of surface graft modification, Vibratory Mixing 2-3h, makes SiO2 be dispersed in decentralized medium PEG200 and forms shear thickening fluid.
Superhigh molecular weight polyethylene fibers and the blending in advance of Coolking fiber is adopted to make spun yarn, then plain weave is carried out, the fabric of braiding is netted pilotaxitic texture, stacked 16 layers jointly, this fabric, composition basic unit, fabric mechanical strength as basic unit is not less than 30cN/dtex, and woven fabric specification is for being 65-150 root/10cm through close and filling density; The surface density of basic unit is 197g/m
2surface density is containing microcellular structure, and have the aperture of 0.01-0.3mm, porosity about 15%, fabric thickness is 0.1-0.35mm.
By resin matrix film and the drying respectively of plain weave cloth, plain cloth: time 1h, temperature 105 DEG C, resin matrix: time 2h, temperature 60 C.Then resin matrix film and plain weave cloth being superimposed together by a graded, can be the mode lamination according to ABA, BAB, AB, in this programme, is preferably the mode of BAB, finally adopts press hot pressing compound.Wherein, A is resin matrix, and B is plain cloth.
Plain weave cloth is cut into the sample of 42mm × 38mm, absolute ethyl alcohol is adopted to dilute by 1: 1 (mass ratio) the fluid prepared, being immersed by plain weave cloth after drying process is immersed in diluted system, take out after leaving standstill a period of time, the solution of removing excess surface, then put into 70 DEG C of dry 20min of air dry oven to remove alcohol solvent.
Table 2 (embodiment one and embodiment two, embodiment three products Performance comparision)
| Sequence number | SiO 2 particle diameter | The number of plies | Pierce through the number of plies | Gas permeability |
| Embodiment one | 160 | 16 | 12 | Better |
| Embodiment two | 370 | 16 | 11 | Generally |
| Embodiment three | 600 | 16 | 10 | Poor |
16 layers of compound fabric of embodiment one, embodiment two, embodiment three gained are placed in by the anti-stab standard NIJ0115.0 of America NI J and national standard GA68-2008 testing standard, result all meets standard-required, also find out from above-mentioned table 2, along with the increase of particle diameter, the number of plies that is pierced of sample reduces to some extent, when wherein particle diameter is 160nm, it is 12 layers that sample pierces through the number of plies; When particle diameter is 370nm, it is 11 layers that sample pierces through the number of plies; As particle diameter 600nm, pierce through the number of plies and be reduced to 10 layers, but be not clearly in the degree reduced, therefore, can draw further, the embodiment of the present invention one is preferred embodiment.
The above is only preferred embodiment of the present invention, and protection scope of the present invention is also not only confined to above-described embodiment, does not also limit scope of the invention process.It should be pointed out that for those skilled in the art, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (8)
1. the anti-stab protective fabric containing ice-cold material, this protective materials is with superhigh molecular weight polyethylene fibers, aromatic polyamide fibre, poly-wherein any one plain cloth to penylene benzo-dioxazole fiber, carbon fiber, high-strength polyester fibers, imitative spider silk fiber for basic unit, and this basic unit's multilayer is arranged;
In fiber in this basic unit, blending has Coolking fiber or the Coolplus fiber of energy moisture absorbing and sweat releasing;
This basic unit is evenly attached with shear thickening fluid, by utilizing static dipping method by shear thickening fluid and basic unit's compound.
2. a kind of anti-stab protective fabric containing ice-cold material according to claim 1, it is characterized in that: in described shear thickening fluid, there is modified nanoparticles, described nano particle is the SiO2 particle of different-grain diameter, and the mass fraction of described SiO2 particle is between 40%-45%.
3. a kind of anti-stab protective fabric containing ice-cold material according to claim 1, is characterized in that: the particle diameter of described SiO2 particle is 160-380nm or 510-600nm.
4. a kind of anti-stab protective fabric containing ice-cold material according to claim 1, it is characterized in that: described basic unit is made up of netted pilotaxitic texture, basic unit is that 20-500g/ ㎡ surface density contains microcellular structure, and have the aperture of 0.01-0.3mm, porosity is not less than 10%.
5. a kind of anti-stab protective fabric containing ice-cold material according to claim 1, is characterized in that: be compounded with resin matrix between described multilayer basic unit, described resin matrix is selected from high density polyethylene (HDPE).
6. the preparation method containing the anti-stab protective fabric of ice-cold material, it is characterized in that: comprise the following steps: (1) blending: adopt preferred superhigh molecular weight polyethylene fibers and the blending in advance of preferred Coolking fiber to make spun yarn, wherein, described superhigh molecular weight polyethylene fibers fineness is 1-150tex, and described Coolking fibre fineness is 1-85tex;
(2) weave: the spun yarn plain weave after blending is become to weave cotton cloth, and this to weave cotton cloth be weave in the mode of well word weaving closely, yarn linear density is 420-1400D; Mechanical strength is not less than 30cN/dtex; Woven fabric specification is for being 65-150 root/10cm through close and filling density; Fabric side density is 60-200g/ ㎡; Fabric thickness is 0.1-0.35mm;
(3) flood: adopt ball-milling method to prepare shear thickening fluid, by dispersed for modified nanoparticles in shear thickening fluid, then by scattered mixed liquor dipping plain cloth;
(4) dry: drying, encapsulation are carried out to the composite flooded.
7. the preparation method of a kind of anti-stab protective fabric containing ice-cold material according to claim 6, it is characterized in that: described basic unit and resin matrix adopt hot pressing compound, comprise the following steps, (1) pretreatment: plain cloth is carried out drying, time 1h, temperature 105 DEG C, carries out drying by resin matrix, time 2h, temperature 60 C;
(2) lamination: resin matrix and plain cloth are superimposed together by a graded, different superposition order will obtain the resin compounded layer of different structure, spaced apart with polytetrafluoroethylene (PTFE) release cloth between each composite bed;
(3) pressing: by the resin matrix that is superimposed and plain cloth preheating, then adopts press pressing, and heating certain hour, forms composite bed.
8. the preparation method of a kind of anti-stab protective fabric containing ice-cold material according to claim 7, it is characterized in that: described resin matrix and plain cloth have three kinds of complex methods: ABA, BAB, AB, wherein, A is resin matrix, and B is plain cloth.
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| CN106120081A (en) * | 2016-06-29 | 2016-11-16 | 西安工程大学 | Multilamellar many raw materials flexible puncture-proof fabric and method for weaving thereof |
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| CN116254706A (en) * | 2023-03-03 | 2023-06-13 | 无锡威豪体育器材有限公司 | Puncture-resistant fabric for fencing clothes and preparation method thereof |
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| AU7152996A (en) * | 1995-08-22 | 1997-03-19 | Richard M. Basel | Cloning methods for high strength spider silk proteins |
| ITPO20030005A1 (en) * | 2003-04-14 | 2004-10-15 | Lenzi Egisto Spa | PERFORATION RESISTANT TEXTILE STRUCTURE ESPECIALLY FOR SHOE SOLES |
| CN101871748A (en) * | 2010-04-20 | 2010-10-27 | 深圳航天科技创新研究院 | Soft stab-proof/bulletproof material |
| CN102632665B (en) * | 2012-04-13 | 2016-03-23 | 中国兵器工业集团第五三研究所 | A kind of aramid fiber strengthens resin-based thorn-proof composite material |
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| CN103808210B (en) * | 2012-11-15 | 2016-03-02 | 南京理工大学 | A kind of Use of Flexible Protective Materials and preparation method thereof |
| CN103600536B (en) * | 2013-11-27 | 2016-01-20 | 浙江帅孚安全科技股份有限公司 | A kind of composite for bulletproof halmet and preparation method thereof |
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| CN106120081A (en) * | 2016-06-29 | 2016-11-16 | 西安工程大学 | Multilamellar many raw materials flexible puncture-proof fabric and method for weaving thereof |
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| CN107815870A (en) * | 2017-10-26 | 2018-03-20 | 天津工业大学 | A kind of preparation method of soft permanent seal cooling stab-resistant material |
| CN114250629A (en) * | 2021-12-02 | 2022-03-29 | 西安工程大学 | Preparation method of intelligent stab-resistant fabric, product and application thereof |
| CN114250629B (en) * | 2021-12-02 | 2023-07-25 | 西安工程大学 | Preparation method of intelligent stab-resistant fabric, product and application thereof |
| WO2024066874A1 (en) * | 2022-09-29 | 2024-04-04 | 中山莱圃新材料有限公司 | Lightweight puncture-resistant mesh fabric |
| CN116254706A (en) * | 2023-03-03 | 2023-06-13 | 无锡威豪体育器材有限公司 | Puncture-resistant fabric for fencing clothes and preparation method thereof |
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