CN105219241A - A kind of quick tablecloth coating and preparation method thereof - Google Patents
A kind of quick tablecloth coating and preparation method thereof Download PDFInfo
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- CN105219241A CN105219241A CN201510632171.0A CN201510632171A CN105219241A CN 105219241 A CN105219241 A CN 105219241A CN 201510632171 A CN201510632171 A CN 201510632171A CN 105219241 A CN105219241 A CN 105219241A
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Abstract
A kind of quick tablecloth coating of the present invention, calculate by weight, be made up of 30-40 part room-temperature self-crosslinking water-based polyurethane, 0.05-0.1 part flow agent, 1-10 part wetting agent, 1-3 part thickening material, 0.2-1 part defoamer, 0.10-0.30 part antimildew and antibacterial agent, 2-5 part film coalescence aid, 5-10 part water-based stripper and 10-20 part filler.Present invention also offers the preparation method of above-mentioned tablecloth coating, first in a reaction vessel, add partially wetting agent, defoamer and deionized water, through dispersed with stirring, add filler again, dispersed with stirring again, adds room-temperature self-crosslinking water-based polyurethane and remaining defoamer, wetting agent, flow agent, film coalescence aid, water-based stripper, Antisepticize and mildew preventive, thickening material stirring, continues dispersion, through filtering after mixing, obtain quick tablecloth coating.Quick tablecloth coating of the present invention is easy to coating, changes convenience, good economy performance and abrasion-resistant clear.
Description
Technical field
The invention belongs to polymeric material field, be specifically related to a kind of quick tablecloth coating and preparation method thereof.
Background technology
The social development in the present age is maked rapid progress, and for the people liking indoor life, work, desk is the good assistant that people live, work.Particularly desktop, almost every day, everyone will come into contacts with various desktop.Desktop will have certain wear resistance, resistance to soiling and ornamental when contacting with us.What, no matter be the desktop of material, be more or less all difficult to not change in use for some time.For this reason, everybody can cover one piece of tablecloth to desktop usually, and one is attractive in appearance, and two is protection desktop.Use for some time, tablecloth will can fog by pattern that is dirty, tablecloth, and tablecloth material agingly can cause degradation.For this reason, people often need to change tablecloth.And high-quality tablecloth is expensive, regular replacing tablecloth is also uneconomical.
Based on above background, need to develop a kind of environmental protection, be easy to be coated with, change the quick tablecloth coating and preparation method thereof of convenience, good economy performance, abrasion-resistant clear.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of quick tablecloth coating and preparation method thereof, described this quick tablecloth coating and preparation method thereof will solve tablecloth of the prior art to be needed often to change, not only contaminate environment but also uneconomic technical problem.
The invention provides a kind of quick tablecloth coating, calculate by weight, its raw material composition and content as follows:
Room-temperature self-crosslinking water-based polyurethane 30-40 part,
Flow agent 0.05-0.1 part,
Wetting agent 1-10 part,
Thickening material 1-3 part,
Defoamer 0.2-1 part,
Antimildew and antibacterial agent 0.10-0.30 part,
Film coalescence aid 2-5 part,
Water-based stripper 5-10 part,
Filler 10-20 part,
But when wherein said room-temperature self-crosslinking water-based polyurethane is a kind of room temperature film-forming there is the urethane resin of crosslinking curing in oneself;
Described flow agent is the flow agent of polydimethylsiloxane class;
Described wetting agent is the wetting agent of polyether-modified polysiloxane type;
Described thickening material is water-based non-ionic type association type rheology modifier;
Described defoamer is the mixture of polysiloxane mixture;
Described antimildew and antibacterial agent is isothiazolinone structure antimildew and antibacterial agent;
Described film coalescence aid is the mixture of any one or two kinds in dipropylene, alcohol ester 12;
Described water-based stripper is the mixture of any one or two kinds in silicon dioxide gel or organic silicon emulsion;
Described filler is any one in mica powder or talcum powder;
Further, calculate by weight, its raw material composition and content as follows:
Room-temperature self-crosslinking water-based polyurethane 30 parts,
Flow agent 0.05 part,
Wetting agent 1 part,
Thickening material 1 part,
Defoamer 0.2 part,
Antimildew and antibacterial agent 0.10 part,
Film coalescence aid 2 parts,
Water-based stripper 5 parts,
Filler 10 parts,
The aqueous polyurethane emulsion D-60A that wherein said room-temperature self-crosslinking water-based polyurethane provides for Guangzhou Boxing Chemical Technology Co., Ltd.;
Described flow agent is the BYK300 of BYK company;
Described wetting agent is the NP-100 of LG-DOW company;
Described thickening material is the RM825 of ROHM AND HAAS company limited;
Described defoamer is the NopcoNXZ of Henkel KGaA company;
Described antimildew and antibacterial agent is the XK-02B of the limited formula of the vast biochemistry in Nantong;
Described film coalescence aid is the dipropylene of Dow Chemical company;
Described water-based stripper is silicon dioxide gel;
Described filler is mica powder.
Further, calculate by weight, its raw material composition and content as follows:
Room-temperature self-crosslinking water-based polyurethane 40 parts,
Flow agent 0.1 part,
Wetting agent 10 parts,
Thickening material 3 parts,
Defoamer 1 part,
Antimildew and antibacterial agent 0.30 part,
Film coalescence aid 5 parts,
Water-based stripper 10 parts,
Filler 20 parts,
The aqueous polyurethane emulsion D-60A that wherein said room-temperature self-crosslinking water-based polyurethane provides for Guangzhou Boxing Chemical Technology Co., Ltd.;
Described flow agent is the BYK348 of BYK company;
Described wetting agent is the NP-100 of LG-DOW company;
The RM-8W water-based non-ionic type association type rheology modifier that described thickening material provides for Guangzhou Heng Yu Chemical Co., Ltd.;
Described defoamer is the NopcoNXZ of Henkel KGaA company;
Described antimildew and antibacterial agent is the XK-02B of the limited formula of the vast biochemistry in Nantong;
Described film coalescence aid is the alcohol ester 12 of U.S. Yi Shiman;
Described water-based stripper is organic silicon emulsion;
Described filler is talcum powder.
Present invention also offers the preparation method of above-mentioned a kind of quick tablecloth coating,
First take each reactive material according to weight percent, in a reaction vessel, first add the wetting agent of 30 ~ 50%, the defoamer of 30 ~ 50% and 10 ~ 50% of room-temperature self-crosslinking water-based polyurethane number deionized water, 15-20min is disperseed under 600-800r/min rotating speed, add filler again, after disperseing 30-50min under 1600-2800r/min rotating speed, rotating speed is down to 300r/min, add room-temperature self-crosslinking water-based polyurethane and remaining defoamer, remaining wetting agent, flow agent, film coalescence aid, water-based stripper, Antisepticize and mildew preventive, thickening material also stirs, continue dispersion 5-10min, through filtering filter residue after mixing, namely quick tablecloth coating is obtained.
The present invention is because the room-temperature self-crosslinking water-based polyurethane in raw material is as main film forming substance, containing numerous hydrogen bond and crosslinking structure after curing of coating, make this film close to or reach the high rigidity of solvent-based two-component urethane, high gloss and excellent water tolerance, meet environmental requirement simultaneously.This coating is liquid, is easy to coating; Layer of transparent film can be formed rapidly at desktop after coating.In use for some time, this rete gently can be peeled off from table-top surface have gentle hands, not only can not damage coated article surface, device appearance that also can be original is sparkling clean.
UV obtained above is solidified strippable water-based paint and adopts spread coating blade coating twice on the solid desktop crossed through acetone, Ethanol Treatment, be placed on ventilation drying at room temperature 2 ~ 4 hours, drying at room temperature film-forming.According to resistance to GB/T1763-1979 " paint film chemical reagent resistance assay method ", adopt (3%NaCl solution) to test the resistance to salt water of its mother above-mentioned, result display film 48 ~ 56 hours is without loss of gloss, variable color, the phenomenon such as bubble and get rusty; According to GB/T1730-1993 standard, (hardness of film of Tianjin material-testing machine factory to the quick tablecloth coating of above-mentioned gained is tested, and result shows, the hardness of film of the quick tablecloth coating of gained is 2 ~ 3H to adopt the hard instrument of QHQ film Pencil scratch.The CMT5104 electronic tension tester that stripping strength adopts Shenzhen newly to think carefully company at room temperature carries out the stripping test of 180 ° by GB/T2790-1995 standard " tackiness agent 180 ° of peeling strength test methods ", draw speed 50mm/min; Recording stripping strength is 0.23 ~ 0.27kN/m.
The present invention compares with prior art, and its technical progress is significant.The easy construction of one of the present invention quick tablecloth coating, film forming is easy.There is after film good resistance to salt water and transparent and easy separability.And its preparation method due to technique simple, easy to control, the maturation that therefore possesses skills, the feature such as quick, efficient, and be suitable for suitability for industrialized production.There is after this quick tablecloth is coated with coating film higher hardness of film, the transparency and easy separability, make it to be used in the technical fields such as the protection of desktop short-period used and furniture house ornamentation thereof.
Embodiment
Below by embodiment, the present invention is described in further detail, but do not limit the present invention.
In the raw material that various embodiments of the present invention are used except the special producer that shows and specification, other raw materials are commercially available, and specification is chemical pure.
The model of the various equipment that the present invention is used and the information of manufacturer as follows:
GFJ-0.4 type high speed dispersor, Shanghai Xin Nuo plant and instrument company limited produces;
Contact angle measurement JCZ000, Shanghai Zhongchen digital technology equipment Co., Ltd produces;
The hard instrument QHQ of film Pencil scratch, Tianjin material-testing machine factory produces;
The portable mirror luster meter of WGG-60, Shanghai is praised mapping test instrument company limited and is produced.
embodiment 1
A kind of quick tablecloth coating, calculates by weight, its raw material composition and content as follows:
Room-temperature self-crosslinking water-based polyurethane 30 parts,
Flow agent 0.05 part,
Wetting agent 1 part,
Thickening material 1 part,
Defoamer 0.2 part,
Antimildew and antibacterial agent 0.10 part,
Film coalescence aid 2 parts,
Water-based stripper 5 parts,
Filler 10 parts,
The aqueous polyurethane emulsion D-60A that wherein said room-temperature self-crosslinking water-based polyurethane provides for Guangzhou Boxing Chemical Technology Co., Ltd.;
Described flow agent is the BYK300 of BYK company;
Described wetting agent is the NP-100 of LG-DOW company;
Described thickening material is the RM825 of ROHM AND HAAS company limited;
Described defoamer is the NopcoNXZ of Henkel KGaA company;
Described antimildew and antibacterial agent is the XK-02B of the limited formula of the vast biochemistry in Nantong;
Described film coalescence aid is the dipropylene of Dow Chemical company;
Described water-based stripper is silicon dioxide gel;
Described filler is mica powder;
The preparation method of above-mentioned a kind of quick tablecloth coating, specifically comprises the steps:
According to formula, add 0.5 part of wetting agent, 0.1 part of defoamer and 15 parts of deionized waters, 15min is disperseed under 600r/min rotating speed, add 10 parts of fillers again, after disperseing 30min under 1600r/min rotating speed, rotating speed is down to 300r/min, add 30 parts of room-temperature self-crosslinking water-based polyurethanes and remaining 0.1 part of defoamer, 0.5 part of wetting agent, 0.05 part of flow agent, 2 parts of film coalescence aid, 5 parts of water-based strippers, 0.10 part of Antisepticize and mildew preventive, 1 part of thickening material also stirs, continue dispersion 5min, through filtering filter residue after mixing, namely quick tablecloth coating is obtained.
According to GB/T1730-1993 standard, (hardness of film of Tianjin material-testing machine factory to the quick tablecloth coating of above-mentioned gained is tested, and result shows, the hardness of film of the quick tablecloth coating of gained is 2H to adopt the hard instrument of QHQ film Pencil scratch.
The quick tablecloth coating of gained to be applied to after slide glass after natural air drying 3h, to detect this film according to visual method transparent.
According to resistance to GB/T1763-1979 " paint film chemical reagent resistance assay method ", adopt (3%NaCl solution) to test the resistance to salt water of its mother above-mentioned, result display film 48 hours is without loss of gloss, variable color, the phenomenon such as bubble and get rusty;
The CMT5104 electronic tension tester that stripping strength adopts Shenzhen newly to think carefully company at room temperature carries out the stripping test of 180 ° by GB/T2790-1995 standard " tackiness agent 180 ° of peeling strength test methods ", draw speed 50mm/min; Recording stripping strength is 0.23kN/m;
In sum, there is after the quick tablecloth of gained of the present invention is coated with coating film higher hardness of film, the transparency and easy separability.
embodiment 2
A kind of quick tablecloth coating, calculates by weight, its raw material composition and content as follows:
Room-temperature self-crosslinking water-based polyurethane 70 parts,
Flow agent 0.1 part,
Wetting agent 10 parts,
Thickening material 3 parts,
Defoamer 1 part,
Antimildew and antibacterial agent 0.30 part,
Film coalescence aid 5 parts,
Water-based stripper 10 parts,
Filler 20 parts,
The aqueous polyurethane emulsion D-60A that wherein said room-temperature self-crosslinking water-based polyurethane provides for Guangzhou Boxing Chemical Technology Co., Ltd.;
Described flow agent is the BYK348 of BYK company;
Described wetting agent is the NP-100 of LG-DOW company;
The RM-8W water-based non-ionic type association type rheology modifier that described thickening material provides for Guangzhou Heng Yu Chemical Co., Ltd.;
Described defoamer is the NopcoNXZ of Henkel KGaA company;
Described antimildew and antibacterial agent is the XK-02B of the limited formula of the vast biochemistry in Nantong;
Described film coalescence aid is U.S. Yi Shiman TEXANOL film coalescence aid alcohol ester 12;
Described water-based stripper is organic silicon emulsion;
Described filler is talcum powder;
According to formula, add 5 parts of wetting agents, 0.5 part of defoamer and 7 parts of deionized waters, 20min is disperseed under 800r/min rotating speed, add 20 parts of fillers again, after disperseing 50min under 2800r/min rotating speed, rotating speed is down to 300r/min, add 70 parts of room-temperature self-crosslinking water-based polyurethanes and remaining 0.5 part of defoamer, 5 parts of wetting agents, 0.1 part of flow agent, 5 parts of film coalescence aid, 10 parts of water-based strippers, 0.30 part of Antisepticize and mildew preventive, 3 parts of thickening materials stirring, continue dispersion 10min, through filtering filter residue after mixing, namely obtain quick tablecloth coating.
According to GB/T1730-1993 standard, (hardness of film of Tianjin material-testing machine factory to the quick tablecloth coating of above-mentioned gained is tested, and result shows, the hardness of film of the quick tablecloth coating of gained is 3H to adopt the hard instrument of QHQ film Pencil scratch.
The quick tablecloth coating of gained to be applied to after slide glass after natural air drying 2h, to detect this film according to visual method transparent.
According to resistance to GB/T1763-1979 " paint film chemical reagent resistance assay method ", adopt (3%NaCl solution) to test the resistance to salt water of its mother above-mentioned, result display film 56 hours is without loss of gloss, variable color, the phenomenon such as bubble and get rusty;
The CMT5104 electronic tension tester that stripping strength adopts Shenzhen newly to think carefully company at room temperature carries out the stripping test of 180 ° by GB/T2790-1995 standard " tackiness agent 180 ° of peeling strength test methods ", draw speed 50mm/min; Recording stripping strength is 0.27kN/m;
In sum, after the quick tablecloth of gained of the present invention is coated with coating film, there is higher pencil hardness (2H ~ 3H); There is the good transparency; Have good rippability, stripping strength is 0.23 ~ 0.27kN/m.
Described content be only the present invention conceive under basic explanation, and according to any equivalent transformation that technical scheme of the present invention is done, all should protection scope of the present invention be belonged to.
Claims (4)
1. a quick tablecloth coating, is characterized in that calculating by weight, its raw material composition and content as follows:
Room-temperature self-crosslinking water-based polyurethane 30-40 part,
Flow agent 0.05-0.1 part,
Wetting agent 1-10 part,
Thickening material 1-3 part,
Defoamer 0.2-1 part,
Antimildew and antibacterial agent 0.10-0.30 part,
Film coalescence aid 2-5 part,
Water-based stripper 5-10 part,
Filler 10-20 part,
But when wherein said room-temperature self-crosslinking water-based polyurethane is a kind of room temperature film-forming there is the urethane resin of crosslinking curing in oneself;
Described flow agent is the flow agent of polydimethylsiloxane class;
Described wetting agent is the wetting agent of polyether-modified polysiloxane type;
Described thickening material is water-based non-ionic type association type rheology modifier;
Described defoamer is the mixture of polysiloxane;
Described antimildew and antibacterial agent is isothiazolinone structure antimildew and antibacterial agent;
Described film coalescence aid is the mixture of any one or two kinds in dipropylene, alcohol ester 12;
Described water-based stripper is the mixture of any one or two kinds in silicon dioxide gel or organic silicon emulsion;
Described filler is any one in mica powder or talcum powder.
2. tablecloth coating as claimed in claim 1 a kind of quick, is characterized in that calculating by weight, its raw material composition and content as follows:
Room-temperature self-crosslinking water-based polyurethane 30 parts,
Flow agent 0.05 part,
Wetting agent 1 part,
Thickening material 1 part,
Defoamer 0.2 part,
Antimildew and antibacterial agent 0.10 part,
Film coalescence aid 2 parts,
Water-based stripper 5 parts,
Filler 10 parts,
Wherein said room-temperature self-crosslinking water-based polyurethane is the aqueous polyurethane emulsion D-60A of Guangzhou Boxing Chemical Technology Co., Ltd.;
Described flow agent is the BYK300 of BYK company;
Described wetting agent is the NP-100 of LG-DOW company;
Described thickening material is the RM825 of ROHM AND HAAS company limited;
Described defoamer is the NopcoNXZ of Henkel KGaA company;
Described antimildew and antibacterial agent is the XK-02B of the limited formula of the vast biochemistry in Nantong;
Described film coalescence aid is the dipropylene of Dow Chemical company;
Described water-based stripper is silicon dioxide gel;
Described filler is mica powder.
3. tablecloth coating as claimed in claim 1 a kind of quick, is characterized in that calculating by weight, its raw material composition and content as follows:
Room-temperature self-crosslinking water-based polyurethane 40 parts,
Flow agent 0.1 part,
Wetting agent 10 parts,
Thickening material 3 parts,
Defoamer 1 part,
Antimildew and antibacterial agent 0.30 part,
Film coalescence aid 5 parts,
Water-based stripper 10 parts,
Filler 20 parts,
The aqueous polyurethane emulsion D-60A that wherein said room-temperature self-crosslinking water-based polyurethane provides for Guangzhou Boxing Chemical Technology Co., Ltd.;
Described flow agent is the BYK348 of BYK company;
Described wetting agent is the NP-100 of LG-DOW company;
The RM-8W water-based non-ionic type association type rheology modifier that described thickening material provides for Guangzhou Heng Yu Chemical Co., Ltd.;
Described defoamer is the NopcoNXZ of Henkel KGaA company;
Described antimildew and antibacterial agent is the XK-02B of the limited formula of the vast biochemistry in Nantong;
Described film coalescence aid is the alcohol ester 12 of U.S. Yi Shiman;
Described water-based stripper is organic silicon emulsion;
Described filler is talcum powder.
4. claim 1, the preparation method of a kind of quick tablecloth coating described in 2 or 3, it is characterized in that: first take each reactive material according to weight percent, in a reaction vessel, first add the wetting agent of 30 ~ 50%, the defoamer of 30 ~ 50% and 10 ~ 50% of room-temperature self-crosslinking water-based polyurethane number deionized water, 15-20min is disperseed under 600-800r/min rotating speed, add filler again, after disperseing 30-50min under 1600-2800r/min rotating speed, rotating speed is down to 300r/min, add room-temperature self-crosslinking water-based polyurethane and remaining defoamer, remaining wetting agent, flow agent, film coalescence aid, water-based stripper, Antisepticize and mildew preventive, thickening material also stirs, continue dispersion 5-10min, through filtering filter residue after mixing, namely quick tablecloth coating is obtained.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510632171.0A CN105219241B (en) | 2015-09-29 | 2015-09-29 | A kind of quick tablecloth coating and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510632171.0A CN105219241B (en) | 2015-09-29 | 2015-09-29 | A kind of quick tablecloth coating and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107236436A (en) * | 2017-06-09 | 2017-10-10 | 海聚高分子材料科技（广州）有限公司 | A kind of aqueous polyurethane composition and its film and preparation method |
| CN108373835A (en) * | 2016-11-23 | 2018-08-07 | 上海家化联合股份有限公司 | Aqueous facial mask liquid for kitchen use |
| EP3407000A1 (en) * | 2017-05-25 | 2018-11-28 | Hamilton Sundstrand Corporation | Hydrophilic coating with enhanced properties to limit reactivity, limit dissolution, minimize contamination potential and provide anti-fungal properties |
-
2015
- 2015-09-29 CN CN201510632171.0A patent/CN105219241B/en not_active Expired - Fee Related
Non-Patent Citations (1)
| Title |
|---|
| 凌芳: "单组分自交联水性聚氨酯分散体涂料", 《应用化工》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108373835A (en) * | 2016-11-23 | 2018-08-07 | 上海家化联合股份有限公司 | Aqueous facial mask liquid for kitchen use |
| EP3407000A1 (en) * | 2017-05-25 | 2018-11-28 | Hamilton Sundstrand Corporation | Hydrophilic coating with enhanced properties to limit reactivity, limit dissolution, minimize contamination potential and provide anti-fungal properties |
| US11396606B2 (en) | 2017-05-25 | 2022-07-26 | Hamilton Sundstrand Corporation | Hydrophilic coating with enhanced properties to limit reactivity, limit dissolution, minimize contamination potential and provide anti-fungal properties |
| CN107236436A (en) * | 2017-06-09 | 2017-10-10 | 海聚高分子材料科技（广州）有限公司 | A kind of aqueous polyurethane composition and its film and preparation method |
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| CN105219241B (en) | 2018-04-06 |
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