CN105067398A - Method for manufacturing small-size rock slice sample - Google Patents

Method for manufacturing small-size rock slice sample Download PDF

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Publication number
CN105067398A
CN105067398A CN201510423858.3A CN201510423858A CN105067398A CN 105067398 A CN105067398 A CN 105067398A CN 201510423858 A CN201510423858 A CN 201510423858A CN 105067398 A CN105067398 A CN 105067398A
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CN
China
Prior art keywords
rock
sample
section
microslide
core
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Pending
Application number
CN201510423858.3A
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Chinese (zh)
Inventor
李舰
王国钧
张国斌
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Petrochina Co Ltd
Daqing Oilfield Co Ltd
Original Assignee
Petrochina Co Ltd
Daqing Oilfield Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Petrochina Co Ltd, Daqing Oilfield Co Ltd filed Critical Petrochina Co Ltd
Priority to CN201510423858.3A priority Critical patent/CN105067398A/en
Publication of CN105067398A publication Critical patent/CN105067398A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a method for manufacturing a small-size rock slice sample. The method mainly solves the problems that the existing slice sample is single in identification and the slice identification efficiency cannot be fully exerted. The method is characterized in that: the method comprises the following steps: a. firstly, drilling a rock sample into a small cylindrical rock core with the diameter of 5-8 mm according to different lithologies; b. b, slicing the small cylindrical rock core drilled in the step a, wherein the thickness of the small cylindrical rock core is 1.0-2.0 mm; c. sticking the cut rock slices on a glass slide; d. c, putting the rock slice sample on the glass slide in the step c on a rock slice grinding machine for grinding; e. and (3) carrying out coarse grinding, fine grinding and fine grinding on the rock slice sample on the glass slide to reach the standard thickness of 0.03 +/-0.1 mm. According to the method for manufacturing the small-size rock slice sample, the multiple rock slice samples can be manufactured by one glass slide, so that the core loss is reduced, and the comparison and identification are convenient.

Description

Small size petrographic thin section sample production method
Technical field
The present invention relates to a kind of core sample method for making in In Oil Field Exploration And Development technical field, especially a kind of small size petrographic thin section sample production method.
Background technology
Rock core is rare and valuable geology geological material, and it can reflect architectural feature and the mineral composition of rock stratum truly.Drilling and coring delivery, every block rock core somewhat expensive, drilling through core sample if a large amount of, is the huge waste to rock core.Small size petrographic thin section sample can save a large amount of rock core, general petrographic thin section sample is all that stickup one piece of diameter is the sample that 25mm rock grinds on one piece of microslide, such thin slice makes in relative technique comparatively simple, and the rock sample ground is all single sample.But because sample diameter is relatively large, time-consuming in the process ground, effort, produces the inclined phenomenon of mill often.When doing thin section identification, one piece of sample is just corresponding to one piece of chip sample, can not contrast qualification, can not improve determination rates for same layer position.
Summary of the invention
The invention reside in overcome in background technology and there is the single problem of rock sample that existing petrographic thin section manufacture craft simply grinds, and provide oneplant small size petrographic thin section sample production method.This small size petrographic thin section sample production method, one piece of microslide can produce how soon petrographic thin section sample, reduces rock core loss, improves thin section identification efficiency, be convenient to carry out contrast and identify.
The present invention solves its problem and reaches by following technical scheme: oneplant small size petrographic thin section sample production method, comprise the following steps:
A, first according to the difference of lithology, rock sample is drilled to the small column rock core of diameter 5 ~ 8mm;
B, cut into slices to the small column rock core be drilled in step a, thickness is at 1.0 ~ 2.0mm;
C, by the rock cut down section adhere in glass slide;
D, the rock section sample on microslide in step c is put on rock wafer lapping machine grinds;
Rock section sample on e, microslide reaches standard thickness 0.03 ± 0.1mm after corase grind, fine grinding, fine grinding.
The present invention can have following beneficial effect compared with above-mentioned background technology: this small size petrographic thin section sample production method, be that the rock sample being stained with the similar and different lithology of polylith with one piece of microslide carries out grinding petrographic thin section sample, such chip sample tool has the following advantages.The first, for the rock core of same well, contrast qualification can be carried out according to identical lithology, identical layer position petrographic thin section; The second, for different well, identical layer position, different lithology can carry out thin section identification; Three, thin section identification is carried out for the lithology that different well is identical: four, for different well can be same layer position, the core sample of different layers position sample of laminating carries out thin section identification.Five, identification equipment can be made to play maximum qualification function, improve determination rates, make thin section identification more rationally, science more.Six, the disposable chip sample that grinds can carry out lithology independent assortment as required, exactly polylith lithology is placed on same and carries preparation efficiency thin slice grinding and improves petrographic thin section, owing to using small size chip sample, the use amount of rock core can be saved.The method existing equipment, cost are low, and simple to operate being easy to is grasped, and reduces rock core loss, compensate for the deficiency of current adding rock chip sample method.
embodiment:
Below in conjunction with specific embodiment, the invention will be further described:
Preparation machine:
(1) rock sample machine for placing one, for drilling through core sample plunger.
(2) small size series drill bit, diameter is 5 ~ 8mm.
(2) core cutter one (commercially available prod), for cutting core sample capo thin slice.
(3) rock microslide (commercially available prod).
(4) rock grinding machine (commercially available prod).
Embodiment 1
1, first by same well, the rock core of different layers position is placed on the fixture of rock sample machine for placing respectively, fixing rock core; Transmitting gear rocking handle makes hollow bit move downward, and drills through core column; The length of drill sampling capo will control within the scope of 20mm;
2, in rock core, small size core column is taken out;
3, small size core column is first cut out a plane, then carry out rock section on this basis, thickness is at 1.0 ~ 2.0mm;
4, rock section is adhered on rock microslide respectively, every sheet microslide is pasted 6 pieces of rock sections;
5, every block rock section is numbered, is identified;
6, the rock section on microslide is put on wafer lapping machine and is ground;
7, the rear degree that each the block rock section sample on microslide grinds is reached 0.03 ± 0.1mm.
Embodiment 2
1, first by same well, the rock core of identical layer position is placed on the fixture of rock sample machine for placing, fixing rock core; Transmitting gear rocking handle makes hollow bit move downward, and drills through core column; The length of drill sampling capo will control within the scope of 20mm;
2, in rock core, small size core column is taken out;
3, small size core column is first cut out a plane, then carry out rock section on this basis, thickness is at 1.0 ~ 2.0mm;
4, rock section is adhered on rock microslide respectively, every sheet microslide is pasted 6 pieces of rock sections;
5, every block rock section is numbered, is identified;
6, the rock section on microslide is put on wafer lapping machine and is ground;
7, the rear degree that each the block rock section sample on microslide grinds is reached 0.03 ± 0.1mm.
Embodiment 3
1, first the rock core of different well identical layer position is placed on the fixture of rock sample machine for placing respectively, fixing rock core; Transmitting gear rocking handle makes hollow bit move downward, and drills through core column; The length of drill sampling capo will control within the scope of 20mm;
2, in rock core, small size core column is taken out;
3, small size core column is first cut out a plane, then carry out rock section on this basis, thickness is at 1.0 ~ 2.0mm;
4, rock section is adhered on rock microslide respectively, every sheet microslide is pasted 8 pieces of rock sections;
5, every block rock section is numbered, is identified;
6, the rock section on microslide is put on wafer lapping machine and is ground;
7, the rear degree that each the block rock section sample on microslide grinds is reached 0.03 ± 0.1mm.
Embodiment 4
1, first the rock core of different well different layers position is placed on the fixture of rock sample machine for placing respectively, fixing rock core; Transmitting gear rocking handle makes hollow bit move downward, and drills through core column; The length of drill sampling capo will control within the scope of 20mm;
2, in rock core, small size core column is taken out;
3, small size core column is first cut out a plane, then carry out rock section on this basis, thickness is at 1.0 ~ 2.0mm;
4, rock section is adhered on rock microslide respectively, every sheet microslide is pasted 8 pieces of rock sections;
5, every block rock section is numbered, is identified;
6, the rock section on microslide is put on wafer lapping machine and is ground;
7, the rear degree that each the block rock section sample on microslide grinds is reached 0.03 ± 0.1mm.
Drilling and coring delivery, small size petrographic thin section sample can save a large amount of rock cores, what is more important pastes the section of polylith rock on same microslide can make scientific research personnel carry out physical property contrast, thus more directly perceived, more scientific qualification result is played to the physical property qualification of rock, the invention of this technology has extensive promotional value and practicality.

Claims (6)

1. oneplant small size petrographic thin section sample production method, it is characterized in that: comprise the following steps:
A, first according to the difference of lithology, rock sample is drilled to the small column rock core of diameter 5 ~ 8mm;
B, cut into slices to the small column rock core be drilled in step a, thickness is at 1.0 ~ 2.0mm;
C, by the rock cut down section adhere in glass slide;
D, the rock section sample on microslide in step c is put on rock wafer lapping machine grinds;
Rock section sample on e, microslide reaches standard thickness 0.03 ± 0.1mm after corase grind, fine grinding, fine grinding.
2. small size petrographic thin section sample production method according to claim 1, is characterized in that: drill through small column rock core in described step a and use small size hollow bit.
3. chip sample method for making according to claim 1, is characterized in that: described in cut down rock section be glued on microslide with 502.
4. chip sample method for making according to claim 1, is characterized in that: multiple rock section formation one piece of chip sample cut down adheres in glass slide.
5. chip sample method for making according to claim 1, is characterized in that: in described step c, 6 ~ 8 pieces of rock samples pasted by every block microslide.
6. chip sample method for making according to claim 1, is characterized in that: the rock section that described one piece of microslide is stained with has similar and different lithology.
CN201510423858.3A 2015-07-20 2015-07-20 Method for manufacturing small-size rock slice sample Pending CN105067398A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510423858.3A CN105067398A (en) 2015-07-20 2015-07-20 Method for manufacturing small-size rock slice sample

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510423858.3A CN105067398A (en) 2015-07-20 2015-07-20 Method for manufacturing small-size rock slice sample

Publications (1)

Publication Number Publication Date
CN105067398A true CN105067398A (en) 2015-11-18

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2661527C1 (en) * 2017-06-14 2018-07-17 Федеральное государственное бюджетное образовательное учреждение высшего образования "Саратовский национальный исследовательский государственный университет имени Н.Г. Чернышевского" Method of non-abrasive grinding of petrographic thin sections of argillites of bazhenov group and similar rocks
CN116413093A (en) * 2021-12-30 2023-07-11 大庆油田有限责任公司 Preparation method of shale continuous sheet

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
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CN103471883A (en) * 2013-08-20 2013-12-25 中国石油天然气股份有限公司 Method for manufacturing rock slice in visual real core model
CN203626769U (en) * 2014-01-03 2014-06-04 中国石油天然气股份有限公司 Real sandstone microcosmic oil displacement model
CN104076038A (en) * 2013-03-29 2014-10-01 中国石油天然气股份有限公司 Carbonate rock common diagenesis characteristic characterization and cause identification method

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4185963B2 (en) * 2008-05-16 2008-11-26 株式会社日立製作所 Sample analysis method and sample preparation method
CN202330861U (en) * 2011-11-02 2012-07-11 浙江海洋学院 Glass slide
CN104076038A (en) * 2013-03-29 2014-10-01 中国石油天然气股份有限公司 Carbonate rock common diagenesis characteristic characterization and cause identification method
CN103471883A (en) * 2013-08-20 2013-12-25 中国石油天然气股份有限公司 Method for manufacturing rock slice in visual real core model
CN203626769U (en) * 2014-01-03 2014-06-04 中国石油天然气股份有限公司 Real sandstone microcosmic oil displacement model

Non-Patent Citations (3)

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Title
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孙国忠: "饱含油岩心样品薄片的制作技术", 《石油实验地质》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2661527C1 (en) * 2017-06-14 2018-07-17 Федеральное государственное бюджетное образовательное учреждение высшего образования "Саратовский национальный исследовательский государственный университет имени Н.Г. Чернышевского" Method of non-abrasive grinding of petrographic thin sections of argillites of bazhenov group and similar rocks
CN116413093A (en) * 2021-12-30 2023-07-11 大庆油田有限责任公司 Preparation method of shale continuous sheet

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