CN105060305A - Water glass preparation technology - Google Patents

Water glass preparation technology Download PDF

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Publication number
CN105060305A
CN105060305A CN201510464434.1A CN201510464434A CN105060305A CN 105060305 A CN105060305 A CN 105060305A CN 201510464434 A CN201510464434 A CN 201510464434A CN 105060305 A CN105060305 A CN 105060305A
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CN
China
Prior art keywords
reactor
sodium silicate
quartz sand
soda ash
heating chamber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510464434.1A
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Chinese (zh)
Inventor
肖飞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Powerful Industrial Co Ltd Of Huoshan County Of Anhui Province
Original Assignee
Powerful Industrial Co Ltd Of Huoshan County Of Anhui Province
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Powerful Industrial Co Ltd Of Huoshan County Of Anhui Province filed Critical Powerful Industrial Co Ltd Of Huoshan County Of Anhui Province
Priority to CN201510464434.1A priority Critical patent/CN105060305A/en
Publication of CN105060305A publication Critical patent/CN105060305A/en
Pending legal-status Critical Current

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  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

The invention discloses a water glass preparation technology. The technology mainly comprises the steps of material selection and filtration, material fusion, and discharging. The technology is simple, allows solid water glass to be produced, effectively saves energy consumption in the production process, reduces the resource investment for heating of the solid water glass, improves the resource utilization rate, and improves the water glass production quality, and the quality of the produced solid water glass is good.

Description

A kind of sodium silicate preparation technology
Technical field
The present invention relates to a kind of preparation technology of sodium silicate.
Background technology
Water glass (Na 2si0 2), have another name called sodium silicate, water glass (XNa 20.YSi0 2), colourless, dark green or brown solid or thick liquid, sodium silicate purposes widely, almost throughout each department of national economy, be used for manufacturing silica gel, white charcoal ?, zeolite molecular sieve, Starso silicon sol, layer silicon and instant powdery sodium silicate at chemical system, the various silicates product such as sodium-potassium silicate is the basic raw material of silicon compound; Being indispensable raw material in the lotion such as washing powder, soap in light industry, is also the light agent of water quality, washing assistant; For helping dye, bleaching and sizing in textile industry; Casting, emery wheel manufacture and anticolodal etc. are widely used in machinery industry; For the manufacture of rapid hardening cement, acid-proof cement dubbin, soil-solidified-agent, refractory materials etc. in building trade, in addition, as tackiness agent; Si0 is used in medical 2refine, non-phosphorus builder best at present.
Summary of the invention
The object of this invention is to provide a kind of sodium silicate preparation technology, effectively can save energy consumption, improve resource utilization, promote sodium silicate production quality.
In order to solve the problem existing for background technology, the present invention by the following technical solutions:
A preparation method for sodium silicate, includes following steps:
1. filtration chosen by material: raw material quartz sand, soda ash are filtered through sodium silicate screen apparatus respectively, and deposited respectively by the material after filtering;
2. material melts: quartz sand conveying the first reactor be placed in heating chamber after filtering is melted, and by fusing after quartz sand import the first trash eliminator carry out impurity except from, by through impurity except from after quartz sand import heating chamber side the 3rd reactor in, soda ash is added to its inside by the top of the second reactor in heating chamber, and by fusing after soda ash import the second magazine separator carry out impurity except from, and the soda ash after filtering through melting trash eliminator is imported in the 3rd reactor, in soda ash and the 3rd reactor, quartz sand weight ratio is 1:2, by the stirring mechanism of the 3rd reactor inside, mixing raw material is stirred, and control heating chamber intraventricular pressure and suppress by force, pressure controls as 4-6MPa, and keep pressure in the 3rd reactor to be at 400-800Pa,
3. discharging: blowing is carried out to the liquid sodium silicate that the 3rd reaction kettle for reaction obtains completely, be output in fusing body of heater, the furnace body wall top of fusing body of heater is provided with bocca, bocca is provided with downward inclination angle, its inclination angle is 18-32 °, and liquid sodium silicate is transported on the mould of rotation via the feeding-distribution device melting body of heater side and shapes, and is provided with water cycle crushed aggregates device above mould, cooling shrend can be carried out to the sodium silicate in mould, after shrend, obtain solid sodium silicate.
Beneficial effect of the present invention: the present invention effectively can save energy consumption, improves resource utilization, greatly improves sodium silicate production quality, effectively can promote the production of high-quality sodium silicate.
Embodiment
A preparation method for sodium silicate, includes following steps:
1. filtration chosen by material: raw material quartz sand, soda ash are filtered through sodium silicate screen apparatus respectively, and deposited respectively by the material after filtering;
2. material melts: quartz sand conveying the first reactor be placed in heating chamber after filtering is melted, and by fusing after quartz sand import the first trash eliminator carry out impurity except from, by through impurity except from after quartz sand import heating chamber side the 3rd reactor in, soda ash is added to its inside by the top of the second reactor in heating chamber, and by fusing after soda ash import the second magazine separator carry out impurity except from, and the soda ash after filtering through melting trash eliminator is imported in the 3rd reactor, in soda ash and the 3rd reactor, quartz sand weight ratio is 1:2, by the stirring mechanism of the 3rd reactor inside, mixing raw material is stirred, and control heating chamber intraventricular pressure and suppress by force, pressure controls as 4-6MPa, and keep pressure in the 3rd reactor to be at 400-800Pa,
3. discharging: blowing is carried out to the liquid sodium silicate that the 3rd reaction kettle for reaction obtains completely, be output in fusing body of heater, the furnace body wall top of fusing body of heater is provided with bocca, bocca is provided with downward inclination angle, its inclination angle is 18-32 °, and liquid sodium silicate is transported on the mould of rotation via the feeding-distribution device melting body of heater side and shapes, and is provided with water cycle crushed aggregates device above mould, cooling shrend can be carried out to the sodium silicate in mould, after shrend, obtain solid sodium silicate.

Claims (1)

1. a preparation method for sodium silicate, includes following steps:
1. filtration chosen by material: raw material quartz sand, soda ash are filtered through sodium silicate screen apparatus respectively, and deposited respectively by the material after filtering;
2. material melts: quartz sand conveying the first reactor be placed in heating chamber after filtering is melted, and by fusing after quartz sand import the first trash eliminator carry out impurity except from, by through impurity except from after quartz sand import heating chamber side the 3rd reactor in, soda ash is added to its inside by the top of the second reactor in heating chamber, and by fusing after soda ash import the second magazine separator carry out impurity except from, and the soda ash after filtering through melting trash eliminator is imported in the 3rd reactor, in soda ash and the 3rd reactor, quartz sand weight ratio is 1:2, by the stirring mechanism of the 3rd reactor inside, mixing raw material is stirred, and control heating chamber intraventricular pressure and suppress by force, pressure controls as 4-6MPa, and keep pressure in the 3rd reactor to be at 400-800Pa,
3. discharging: blowing is carried out to the liquid sodium silicate that the 3rd reaction kettle for reaction obtains completely, be output in fusing body of heater, the furnace body wall top of fusing body of heater is provided with bocca, bocca is provided with downward inclination angle, its inclination angle is 18-32 °, and liquid sodium silicate is transported on the mould of rotation via the feeding-distribution device melting body of heater side and shapes, and is provided with water cycle crushed aggregates device above mould, cooling shrend can be carried out to the sodium silicate in mould, after shrend, obtain solid sodium silicate.
CN201510464434.1A 2015-07-29 2015-07-29 Water glass preparation technology Pending CN105060305A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510464434.1A CN105060305A (en) 2015-07-29 2015-07-29 Water glass preparation technology

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510464434.1A CN105060305A (en) 2015-07-29 2015-07-29 Water glass preparation technology

Publications (1)

Publication Number Publication Date
CN105060305A true CN105060305A (en) 2015-11-18

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CN201510464434.1A Pending CN105060305A (en) 2015-07-29 2015-07-29 Water glass preparation technology

Country Status (1)

Country Link
CN (1) CN105060305A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106976886A (en) * 2017-04-28 2017-07-25 福建省三明正元化工有限公司 A kind of preparation method of high dispersive silica sodium silicate solid
CN107162012A (en) * 2017-05-25 2017-09-15 肖飞 A kind of high mode flower bulb alkali preparation method
CN107416853A (en) * 2017-05-25 2017-12-01 肖飞 A kind of sodium silicate preparation technology

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202016876U (en) * 2011-03-16 2011-10-26 相庆柱 Kiln for producing sodium silicate
CN103787347A (en) * 2012-11-02 2014-05-14 岳阳恒忠新材料有限公司 Process for producing liquid high-modulus water glass by combination of dry method and wet method

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202016876U (en) * 2011-03-16 2011-10-26 相庆柱 Kiln for producing sodium silicate
CN103787347A (en) * 2012-11-02 2014-05-14 岳阳恒忠新材料有限公司 Process for producing liquid high-modulus water glass by combination of dry method and wet method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
丁翼: "《化工工人安全卫生培训教材 无机盐》", 31 July 1990, 化学工业出版社 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106976886A (en) * 2017-04-28 2017-07-25 福建省三明正元化工有限公司 A kind of preparation method of high dispersive silica sodium silicate solid
CN107162012A (en) * 2017-05-25 2017-09-15 肖飞 A kind of high mode flower bulb alkali preparation method
CN107416853A (en) * 2017-05-25 2017-12-01 肖飞 A kind of sodium silicate preparation technology
CN107416853B (en) * 2017-05-25 2020-06-19 凤阳常隆科技材料有限公司 Preparation process of sodium silicate

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Application publication date: 20151118

RJ01 Rejection of invention patent application after publication