CN105054292A - Konjac breath-refreshing cigarette holder filter core and preparation method thereof - Google Patents
Konjac breath-refreshing cigarette holder filter core and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a konjac breath-refreshing cigarette holder filter core and a preparation method thereof. The preparation method comprises steps of preparing konjac glucomannan alkaline aqueous solution, preparing konjac glucomannan emulsion, preparing konjac glucomannan gel microspheres, drying konjac glucomannan gel microspheres, preparing mint konjac glucomannan gel microspheres, preparing medicine-carrying konjac glucomannan gel microspheres, preparing konjac fibers and preparing a filter core. The konjac breath-refreshing cigarette holder filter core takes konjac as the main raw material, the konjac has effective fiber plasticity, adsorbability and slow-release property, the amount of toxic substance reaching the oral cavity can be reduced, the case that after a person smokes, the teeth become yellow can be avoided; trace and slow-releasing medicine is contained in the filter core, the medicine effect is guaranteed; all the materials are very environmentally-friendly, and can be degraded in the air easily, are nonhazardous and do not pollute the environment; and the smoker can feel refreshed, the nasal cavity is not blocked, and the mental state of the smoker is better.
Description
Technical field
The present invention relates to a kind of cigarette filter core and preparation method thereof, be specifically related to tasty and refreshing gas cigarette filter core of a kind of konjaku and preparation method thereof.
Background technology
The history of mankind's smoking is from ancient times to the present approximately 523 years.In China, according to records, greatly about 16 to the 17th century of Christian era, tobacco is divided into South Road, North Road to import China into.North Road, at the beginning of the 17th century, imports China northeast into by Korea; South Road, about the middle and later periods in 16th century, reaches Guangdong, Fujian by Philippine.Therefore, cigarette is not only remote at China's influence time, more in human historical development, has profound influence.
Point out in western medium's report on January 10th, 2014, Chinese smoker accounts for the whole world 1/3, and number increases nearly 100,000,000, and quantity occupies first place in the world, and wherein 4% is women.Such data let us must cause enough attention to this event of smoking.
As everyone knows, Smoking is harmful to your health.Harmful material can be produced after cigarette lighter and be roughly divided into six large classes: (1) aldehydes, nitride, olefines (2) nicotine class (3) amine, cyanide and heavy metal (4) Benzpyrene, arsenic, cadmium, methyl hydrazine, amino phenols, other radioactive substance (5) phenolic compound, formaldehyde (6) carbon monoxide.Harm of smoking is in particular in: (1) smoking seriously can stimulate the respiratory tract of people, and long-term smoking can cause the diseases such as chronic pharyngitis, tracheitis, pulmonary emphysema, pneumonia.(2) smoking is easily addicted, and stimulate sympathetic nerve, impel dopamine to discharge in a large number, once non-smoking, dopamine level is not enough to excite nerve, and smoker just can dysphoria, dispirited.(3) smoking can directly cause poisoning, and excessive or long-term smoking can make poisonous substance accumulation, causes slow poisoning, seriously shortens human longevity.(4) smoking significantly improves canceration Probability, and can accelerate canceration process.(5) smoking can cause anthracemia, makes people short of breath, has a dizzy spell, and severe patient can cause shock.
In life, we suck many cigarettes directly or indirectly, and smoker not only can affect the healthy of oneself, often also can have influence on the physical and mental health of periphery people.Therefore, when banning on opium-smoking and the opium trade completely, people contemplate exploitation smoking cessation product.But the smoking cessation product that market occurs successively really cannot solve the problem of smoking cessation all the time, and people always guard against and relapse.2540 Multiple components are had in cigarette, complicated physical-chemical reaction is there is after burning, produce gas in have more than 400 kind of carcinogen, also have the meeting of kind more than 10 promote canceration, wherein to harm maximum be nicotine, tar, carbon monoxide, cyanide and radioactive substance.
Application number is the patent of invention " a kind of cigarette holder device being beneficial to smoking cessation " (applying date: 2009.01.23) of 201310031514.9, describes a kind of cigarette holder capable of stopping smoking device.This product is made up of cigarette holder part, smoking cessation inner core cartridge, cigarette connecting cylinder, employs the materials such as resistance filtering agent, activated carbon, traditional medicine volatile oil (as agalloch eaglewood volatile oil, Radix Linderae volatile oil, Fructus Citri Sarcodactylis volatile oil etc.).Adopt distribution smoking cessation, remove the brand-new smoking cessation approach of addicts to the physiological dependence of tobacco and psychological dependence gradually.But the traditional medicine volatile oil adopted in this invention probably just volatilizees totally after not using for a long time, thus affects result of use.The borneol used in this invention in addition has certain toxicity, Pharmacopoeia of the People's Republic of China version regulation use amount in 2010 is 0.15-0.3g/kg, for bringing the behavior adhered to for a long time of this needs of smoking cessation, be easy to cause user to suck borneol excessive and poisoning, there is potential safety hazard.
Application number be 201420420740.6 patent " tool bluetooth module can assisted user smoking cessation cigarette holder " (applying date: 2014.07.29), describe a kind of bluetooth cigarette holder capable of stopping smoking.This product forms by being difficult to articulate, with the tobacco rod be connected of being difficult to articulate, the cigarette seat be located at the filtration core assembly in tobacco rod and be connected to tobacco rod end.Its feature is to have in tobacco rod can carry out the bluetooth module of Bluetooth pairing with portable mobile termianl and detect the detecting element of user's smoking number of times or smoking frequency, the smoking information wireless of user can be transferred to mobile terminal, to manage with counting user smoking state and aiding smoking cessation.But the main deficiency that there are three aspects in this patent: is and whether uncertain institute holding equipment is enough sensitive, can record smoker's situation to accurate low error; Two is that the equipment such as this patent such as pedometer are the same, lacks practicality, and user specially can't go when smoking to connect bluetooth, and is confirmed whether to connect; Three be without any medicine and particular filter auxiliary under, the content of the harmful substances such as nicotine does not reach the effect of reduction, and the consciousness only by people goes smoking cessation, not only cannot give up smoking, and still with smoke common to be equally harmful to the health.
Application number is patent " a kind of health care cigarette holder capable of stopping smoking " (applying date: 2013.04.12) of 201320184827.3, describes a kind of health care cigarette holder capable of stopping smoking.This product by cigarette clamping part, band exhaust gases passes middle part and embed the suction nozzle of front end in the middle part of exhaust gases passes and form.Exhaust gases passes in suction nozzle and cigarette clamping part communicates with the exhaust gases passes at middle part, cigarette holder body is made up of high heat radiating metal material, the outer surface at the middle part of cigarette clamping part and band exhaust gases passes and inner surface structure or groove structure twist, the metal hair net that its inner filling rate of heat dissipation is large.This product is high with rate of heat dissipation, makes smoker suck thermal requirement to oral cavity more and more lower, finally reaches smoking cessation object.The index of this patent using heat as smoking cessation, reach smoking cessation object by the heat be reduced in smoker's mouth, effect may not significantly, without any medicine and particular filter auxiliary under, though the harmful substance contents such as nicotine have a little reduction, the effect of smoking cessation may do not reached.
Summary of the invention
The object of the present invention is to provide tasty and refreshing gas cigarette filter core of a kind of konjaku and preparation method thereof.Utilize adsorptivity and the slow release of konjak portuguese gansu polyose gel microsphere, and the plasticity of Rhizoma amorphophalli fiber, make a kind of with low cost, preparation is simple, can suitability for industrialized production, convenient and practical, Be very effective, can fresh breath, reduce smog toxicity, reduce the second-hand toxicity on inhalation of smoker's surrounding population, be suitable for health care of body, easily degraded simultaneously, the tasty and refreshing gas cigarette filter core of konjaku of environmentally safe.
The preparation method of the tasty and refreshing gas cigarette filter core of a kind of konjaku of the present invention, is characterized in that preparation process is as follows:
(1) preparation of konjaku glucomannan alkaline aqueous solution: by weight, get 0.5mol/L hydrochloric acid and the mixing of 65-70 part deionized water of 6-8 part, 15-19 part konjaku glucomannan is added in mixed liquor, mechanical agitation becomes gelatin, put into incubator 115 DEG C degraded 50-60min, take out and add 14-15 part 0.5mol/LNaOH solution, stir and make it all dissolve, elimination impurity, makes konjaku glucomannan alkaline aqueous solution;
(2) konjaku glucomannan emulsion preparation: by weight, get 1000-2000 part mixing oil phase, the perforated pipe be contained on mixer is inserted in mixing oil phase, the konjaku glucomannan alkaline aqueous solution of step (1) is added in pipe, the rotating speed regulating mixer is 4000r/min, mixing, makes konjaku glucomannan emulsion; Described mixing oil phase, refers to be atoleine by weight: benzinum=5:1, is made into mixed liquor by atoleine and benzinum, add emulsifying agent Span80, be made into mixing oil phase by weight for 3%-6%; Described perforated pipe, refers to that grade of steel is the general pipe of 10, pipe is high × and caliber × thickness=20cm × 3cm × 0.2cm, aperture 1000um, pitch of holes 1cm, parallel cloth hole, perforated pipe is buied by market;
(3) konjak portuguese gansu polyose gel microsphere preparation: toward in the emulsion of step (2) konjaku glucomannan, add 1-2 part crosslinking agent epoxychloropropane (ECH), 100r/min mechanical agitation is even, solidifies 4-4.5h after sealing at 60-65 DEG C; Microballoon after solidification is used benzinum, absolute ethyl alcohol and deionized water 3000r/min centrifuge washing circulation 2-3 time successively; Make konjak portuguese gansu polyose gel microsphere;
(4) drying of konjak portuguese gansu polyose gel microsphere: by the konjak portuguese gansu polyose gel microsphere 50-60 DEG C drying of step (3), to moisture content not higher than 5%-7%, takes out, obtains dry konjak portuguese gansu polyose gel microsphere;
(5) preparation of peppermint konjak portuguese gansu polyose gel microsphere: get menthol 1-5 part and put into 50-100ml beaker, 42 ~ 44 DEG C of heating water baths are to micro-molten, dry konjak portuguese gansu polyose gel microsphere is placed in one, take out after mixing, cooling, wipe the outside crystallization of microballoon away with hairbrush, obtain peppermint konjak portuguese gansu polyose gel microsphere;
(6) preparation of medicine carrying konjak portuguese gansu polyose gel microsphere: get 6-12 part tuber of dwarf lilyturf, radix scrophulariae 9-12 part, Radix Glycyrrhizae 2-10 part 200-300 part that adds water boils, decoct to 50-100ml, incline and fried liquid, so repeat 2-3 time; Merge fried liquid and filter, removing impurity, by centrifugal for filtrate 6000-8000r/min 3-5min, removing supernatant, obtain concentrate; Put in concentrate by dry konjak portuguese gansu polyose gel microsphere, take out after 20-24h, 50-60 DEG C is dried to moisture content not higher than 5%-7%, takes out, obtains medicine carrying konjak portuguese gansu polyose gel microsphere;
(7) preparation of Rhizoma amorphophalli fiber: get konjaku glucomannan 5-50 part, be incorporated as stirring and dissolving in its weight 30-40 purified water doubly, gelatinization leaves standstill 1-2h and obtains No. 1 sample for subsequent use; Get starch 25-250 part that purity is 75%-90%, mix with No. 1 sample for subsequent use, obtain No. 2 samples for subsequent use; Get dietary alkali 30-100 part that purity is 80%-90%, the edible alkali solution of preparation 100-200 part, mixes edible alkali solution with No. 2 samples for subsequent use, obtains No. 3 samples for subsequent use; Pour in filter core mould by No. 3 samples for subsequent use, at 80-110 DEG C, steam 50-70min, after taking-up, then the refrigerator and cooled putting into-40--50 DEG C freezes 20-24h, and taking-up is thawed, and being dried to moisture content at 50-60 DEG C is 5%-20%, obtains Rhizoma amorphophalli fiber;
(8) preparation of filter core:
A, preparation loquat Bulbus: get loguat leaf 3-8 part, Bulbus Fritillariae Cirrhosae 3-10 part, cross 40-100 mesh sieve after pulverizing, mix for subsequent use;
B, prepare filter core: by weight, get loquat Bulbus 5-10 part, activated carbon 10-20 part, dry konjak portuguese gansu polyose gel microsphere 10-15 part, peppermint konjak portuguese gansu polyose gel microsphere 20-25 part, medicine carrying konjak portuguese gansu polyose gel microsphere 20-25 part, Rhizoma amorphophalli fiber 10-30 part, absorbent cotton 10-15 part, become filter core with the winding of water suction body paper.The best assemble method of filter core: filter core is divided into 7 layers, putting in order of each material respectively is toward cigarette holder direction from chimney: Rhizoma amorphophalli fiber, activated carbon, absorbent cotton, dry konjac glucomannan gel micro-ball, loquat Bulbus, peppermint konjac glucomannan gel micro-ball and medicine carrying konjac glucomannan gel micro-ball load in mixture, Rhizoma amorphophalli fiber.The cigarette holder of different size uses the filter core of different size, and filter core is contained in cigarette holder.All material of the present invention is all buied by market.
Advantage of the present invention and beneficial effect: the preparation method of the tasty and refreshing gas cigarette filter core of a kind of konjaku of the present invention, take konjaku as primary raw material, with its effective fiber plasticity, adsorptivity and slow release, play a role: first, Rhizoma amorphophalli fiber can provide suction-operated in the filter of last essence, reduce the levels of toxic substances arriving oral cavity, yellow tooth after stopping smoking; The second, konjak portuguese gansu polyose gel microsphere provides perfect slow release effect, medicine can be made also not easily to lose efficacy in long-term no situation, in use can stablize, discharge constantly, improves, ensures drug effect; 3rd, konjak portuguese gansu polyose gel microsphere greatly can cover the bad smell of medicine, because be micro-slowly-releasing, human body not easily finds medicine special odor, thus reduces the discomfort reaction because smell causes; 4th, the material all very environmental protection that the various konjakus used are made, easily degrades in atmosphere, and nonhazardous effect is free from environmental pollution; 5th, konjak portuguese gansu polyose gel microsphere is divided into two parts, load different Chinese medicine separately: a part is filled with menthol, can pure and fresh smoker's implication, suck cigarette also not easily to make people around realize to have inhaled cigarette, can not cause other people discomfort, and smoker's spirit and QI cleaning, nose key can be made penetrating, the state of mind is better; Another part is filled with Chinese medicinal formulae, plays maintenance, health care, prevent the disease that some may cause due to smoking to human body, as throat discomfort, cough, lung heat etc., reduces harm of smoking.Specifically employ following Chinese medicine: the tuber of dwarf lilyturf, sweet, micro-hardship, is slightly cold.The thoughts of returning home, lung, stomach warp.There is nourishing Yin and promoting production of body fluid, the merit that moistening lung clears away heart-fire.For dryness of the lung dry cough, deficiency of Yin consumptive disease is coughed, larynx numbness pharyngalgia, and Tianjin wound is thirsty, and interior heat such as to be quenched one's thirst at the card; Radix scrophulariae, sweet, bitter, salty, be slightly cold.Return lung, stomach, kidney channel.Energy clearing heat and cooling blood, nourishing Yin and falling fire, detoxicating and resolving a mass.Enter ying blood for heat, febrile virulent maculae, consumption of YIN caused by febrile disease, the deep red polydipsia of tongue, constipation is hindered in Tianjin. and hectic fever due to yin labor is coughed, hot eyes, pharyngalgia, diphtheria, scrofula, the cards such as carbuncle sore tumefacting virus.Bulbus Fritillariae Cirrhosae, bitter, sweet, be slightly cold.Return lung, the heart channel of Hang-Shaoyin.Can clearing heat and moistening lung, preventing phlegm from forming and stopping coughing, dissipating bind disappears carbuncle.For lung-heat type cough, the few phlegm of dry cough, deficiency of Yin labor is coughed, blood-stained sputum, scrofula, the cards such as lung carbuncle; Radix Glycyrrhizae, sweet, flat.The thoughts of returning home, lung, spleen, stomach warp.Can invigorate the spleen and benefit qi, clearing heat and detoxicating, expelling phlegm and arresting coughing, relieving spasm to stop pain.For weakness of the spleen and the stomach, lassitude hypodynamia, palpitation, coughing with a lot of sputum, the anxious pain of gastral cavity abdomen, four limbs contraction, the cards such as carbuncle sore tumefacting virus; Loguat leaf, bitter, be slightly cold.Attach to the lung and stomach meridians.There is removing heat from the lung to relieve cough, the merit of stopping nausea and vomiting by lowering the adverse flow of QI.For cough with lung heat, the circulation of vital energy in the wrong direction breathes heavily urgency, and stomach energy is vomitted inverse, and dysphoria with smothery sensation is thirsty waits card.In addition, due to filtration, significantly reduce suction levels of toxic substances, have again the maintenance of Chinese medicine, smoker can be made to reduce dependence to cigarette gradually, thus naturally given up smoking.
Reliability and the security of the tasty and refreshing gas cigarette filter core of a kind of konjaku of the present invention meet relative national standards requirement completely, and the comparative result of the filter core prepared with prior art is in table 1.
The comparative result of table 1, the tasty and refreshing gas cigarette filter core of konjaku of the present invention and other filter cores
Detailed description of the invention
In order to fully disclose tasty and refreshing gas cigarette filter core of konjaku of the present invention and preparation method thereof, be illustrated below in conjunction with embodiment.
The preparation method of the tasty and refreshing gas cigarette filter core of embodiment 1 one kinds of konjakus
A preparation method for the tasty and refreshing gas cigarette filter core of konjaku, comprises the following steps:
(1) preparation of konjaku glucomannan alkaline aqueous solution: by weight, get 0.5mol/L hydrochloric acid and 65 parts of deionized water mixings of 8 parts, 15 parts of konjaku glucomannans are added in mixed liquor, mechanical agitation becomes gelatin, put into incubator 115 DEG C degraded 60min, take out and add 14 parts of 0.5mol/LNaOH solution, stir and make it all dissolve, elimination impurity, makes konjaku glucomannan alkaline aqueous solution;
(2) konjaku glucomannan emulsion preparation: get 1000 parts of mixing oil phases, the perforated pipe be contained on mixer is inserted in mixing oil phase, the konjaku glucomannan alkaline aqueous solution of step (1) is added in pipe, the rotating speed regulating mixer is 4000r/min, mixing, makes konjaku glucomannan emulsion; Described mixing oil phase, refers to by weight for atoleine: benzinum=5:1, is made into mixed liquor by atoleine and benzinum, is by weight 3% to add emulsifying agent Span80, is made into mixing oil phase;
(3) konjak portuguese gansu polyose gel microsphere preparation: toward in the emulsion of step (2) konjaku glucomannan, add 1 part of crosslinking agent epoxychloropropane (ECH), 100r/min mechanical agitation is even, solidifies 4h at sealing latter 60 DEG C; Microballoon after solidification is circulated 2 times with benzinum, absolute ethyl alcohol and deionized water 3000r/min centrifuge washing successively; Make konjak portuguese gansu polyose gel microsphere;
(4) drying of konjak portuguese gansu polyose gel microsphere: by the microballoon 60 DEG C of dryings made, to moisture content not higher than 5%, takes out, obtains dry konjak portuguese gansu polyose gel microsphere;
(5) preparation of peppermint konjak portuguese gansu polyose gel microsphere: get menthol 3 parts and put into 50ml beaker, 42 DEG C of heating water baths are to micro-molten, dry konjak portuguese gansu polyose gel microsphere is placed in one, take out after mixing, cooling, wipe the outside crystallization of microballoon away with hairbrush, obtain peppermint konjak portuguese gansu polyose gel microsphere;
(6) preparation of medicine carrying konjak portuguese gansu polyose gel microsphere: get the tuber of dwarf lilyturf 6 parts, radix scrophulariae 9 parts, 2 parts, Radix Glycyrrhizae add water 200 parts and boil, decoct to 100ml, incline and fried liquid, so repeat 2 times; Merge fried liquid and filter, removing impurity, by centrifugal for filtrate 6000r/min 3min, removing supernatant, obtain concentrate; Put in concentrate by dry konjak portuguese gansu polyose gel microsphere, take out after 20h, 60 DEG C are dried to moisture content not higher than 5%, take out, obtain medicine carrying konjak portuguese gansu polyose gel microsphere;
(7) preparation of Rhizoma amorphophalli fiber: get konjaku glucomannan 15 parts, is incorporated as stirring and dissolving in the purified water of its weight 30 times, and gelatinization leaves standstill 2h and obtains No. 1 sample for subsequent use; Get the starch 25 parts that purity is 75%, mix with No. 1 sample for subsequent use, obtain No. 2 samples for subsequent use; Get the dietary alkali 30 parts that purity is 80%, prepare the edible alkali solution of 100 parts, edible alkali solution is mixed with No. 2 samples for subsequent use, obtain No. 3 samples for subsequent use; Pour in filter core mould by No. 3 samples for subsequent use, at 80 DEG C, steam 50min, after taking-up, then the refrigerator and cooled putting into-40 DEG C freezes 20h, and taking-up is thawed, and being dried to moisture content at 60 DEG C is 5%, obtains Rhizoma amorphophalli fiber;
(8) preparation of filter core:
A, preparation loquat Bulbus: get loguat leaf 3 parts, Bulbus Fritillariae Cirrhosae 3 parts, cross 40 mesh sieves after pulverizing, mix for subsequent use;
B, prepare filter core: by weight, get loquat Bulbus 5 parts, activated carbon 10 parts, dry konjak portuguese gansu polyose gel microsphere 10 parts, peppermint konjak portuguese gansu polyose gel microsphere 20 parts, medicine carrying konjak portuguese gansu polyose gel microsphere 20 parts, Rhizoma amorphophalli fiber 10 parts, 10 parts, absorbent cotton, become filter core with the winding of water suction body paper; Filter core is divided into 7 layers, and putting in order of each material respectively is toward cigarette holder direction from chimney: Rhizoma amorphophalli fiber, activated carbon, absorbent cotton, dry konjac glucomannan gel micro-ball, loquat Bulbus, peppermint konjac glucomannan gel micro-ball and medicine carrying konjac glucomannan gel micro-ball load in mixture, Rhizoma amorphophalli fiber.Filter core is contained in the cigarette holder bought by market.
The preparation method of the tasty and refreshing gas cigarette filter core of embodiment 2 one kinds of konjakus
A preparation method for the tasty and refreshing gas cigarette filter core of konjaku, comprises 8 steps, and step (1)-(7) are identical with step (1)-(7) of embodiment 1; The preparation of step (8) filter core: A, get loguat leaf 5 parts, Bulbus Fritillariae Cirrhosae 7 parts, after pulverizing, cross 100 mesh sieves, for subsequent use.B, by weight, get loquat Bulbus 10 parts, activated carbon 10 parts, dry konjak portuguese gansu polyose gel microsphere 10 parts, peppermint konjak portuguese gansu polyose gel microsphere 20 parts, medicine carrying konjak portuguese gansu polyose gel microsphere 20 parts, Rhizoma amorphophalli fiber 20 parts, 10 parts, absorbent cotton, become filter core with the winding of water suction body paper.
The preparation method of the tasty and refreshing gas cigarette filter core of embodiment 3 one kinds of konjakus
A preparation method for the tasty and refreshing gas cigarette filter core of konjaku, comprises 8 steps, and step (1)-(7) are identical with step (1)-(7) of embodiment 1; Step (8)) preparation of filter core: A, get loguat leaf 8 parts, Bulbus Fritillariae Cirrhosae 10 parts, cross 100 mesh sieves after pulverizing, for subsequent use.B, by weight, get loquat Bulbus 10 parts, activated carbon 20 parts, dry konjak portuguese gansu polyose gel microsphere 10 parts, peppermint konjak portuguese gansu polyose gel microsphere 20 parts, medicine carrying konjak portuguese gansu polyose gel microsphere 20 parts, Rhizoma amorphophalli fiber 10 parts, 10 parts, absorbent cotton, become filter core with the winding of water suction body paper.
The foregoing is only preferred embodiment of the present invention, all equalizations done according to the present patent application the scope of the claims change and modify, and all should belong to covering scope of the present invention.
Claims (7)
1. a preparation method for the tasty and refreshing gas cigarette filter core of konjaku, is characterized in that preparation process is as follows:
(1) preparation of konjaku glucomannan alkaline aqueous solution: by weight, get 0.5mol/L hydrochloric acid and the mixing of 65-70 part deionized water of 6-8 part, 15-19 part konjaku glucomannan is added in mixed liquor, mechanical agitation becomes gelatin, put into incubator 115 DEG C degraded 50-60min, take out and add 14-15 part 0.5mol/LNaOH solution, stir and make it all dissolve, elimination impurity, makes konjaku glucomannan alkaline aqueous solution;
(2) konjaku glucomannan emulsion preparation: by weight, get 1000-2000 part mixing oil phase, the perforated pipe be contained on mixer is inserted in mixing oil phase, the konjaku glucomannan alkaline aqueous solution of step (1) is added in pipe, the rotating speed regulating mixer is 4000r/min, mixing, makes konjaku glucomannan emulsion; Described mixing oil phase, refers to be atoleine by weight: benzinum=5:1, is made into mixed liquor by atoleine and benzinum, add emulsifying agent Span80, be made into mixing oil phase by weight for 3%-6%; Described perforated pipe, refers to that grade of steel is the general pipe of 10, pipe is high × and caliber × thickness=20cm × 3cm × 0.2cm, aperture 1000um, pitch of holes 1cm, parallel cloth hole, perforated pipe is buied by market;
(3) konjak portuguese gansu polyose gel microsphere preparation: toward in the emulsion of step (2) konjaku glucomannan, add 1-2 part crosslinking agent epoxychloropropane (ECH), 100r/min mechanical agitation is even, solidifies 4-4.5h after sealing at 60-65 DEG C; Microballoon after solidification is used benzinum, absolute ethyl alcohol and deionized water 3000r/min centrifuge washing circulation 2-3 time successively; Make konjak portuguese gansu polyose gel microsphere;
(4) drying of konjak portuguese gansu polyose gel microsphere: by the konjak portuguese gansu polyose gel microsphere 50-60 DEG C drying of step (3), to moisture content not higher than 5%-7%, takes out, obtains dry konjak portuguese gansu polyose gel microsphere;
(5) preparation of peppermint konjak portuguese gansu polyose gel microsphere: get menthol 1-5 part and put into 50-100ml beaker, 42 ~ 44 DEG C of heating water baths are to micro-molten, dry konjak portuguese gansu polyose gel microsphere is placed in one, take out after mixing, cooling, wipe the outside crystallization of microballoon away with hairbrush, obtain peppermint konjak portuguese gansu polyose gel microsphere;
(6) preparation of medicine carrying konjak portuguese gansu polyose gel microsphere: get 6-12 part tuber of dwarf lilyturf, radix scrophulariae 9-12 part, Radix Glycyrrhizae 2-10 part 200-300 part that adds water boils, decoct to 50-100ml, incline and fried liquid, so repeat 2-3 time; Merge fried liquid and filter, removing impurity, by centrifugal for filtrate 6000-8000r/min 3-5min, removing supernatant, obtain concentrate; Put in concentrate by dry konjak portuguese gansu polyose gel microsphere, take out after 20-24h, 50-60 DEG C is dried to moisture content not higher than 5%-7%, takes out, obtains medicine carrying konjak portuguese gansu polyose gel microsphere;
(7) preparation of Rhizoma amorphophalli fiber: get konjaku glucomannan 5-50 part, be incorporated as stirring and dissolving in its weight 30-40 purified water doubly, gelatinization leaves standstill 1-2h and obtains No. 1 sample for subsequent use; Get starch 25-250 part that purity is 75%-90%, mix with No. 1 sample for subsequent use, obtain No. 2 samples for subsequent use; Get dietary alkali 30-100 part that purity is 80%-90%, the edible alkali solution of preparation 100-200 part, mixes edible alkali solution with No. 2 samples for subsequent use, obtains No. 3 samples for subsequent use; Pour in filter core mould by No. 3 samples for subsequent use, at 80-110 DEG C, steam 50-70min, after taking-up, then the refrigerator and cooled putting into-40--50 DEG C freezes 20-24h, and taking-up is thawed, and being dried to moisture content at 50-60 DEG C is 5%-20%, obtains Rhizoma amorphophalli fiber;
(8) filter core is prepared:
A, preparation loquat Bulbus: get loguat leaf 3-8 part, Bulbus Fritillariae Cirrhosae 3-10 part, cross 40-100 mesh sieve after pulverizing, mix for subsequent use;
B, prepare filter core: by weight, get loquat Bulbus 5-10 part, activated carbon 10-20 part, dry konjak portuguese gansu polyose gel microsphere 10-15 part, peppermint konjak portuguese gansu polyose gel microsphere 20-25 part, medicine carrying konjak portuguese gansu polyose gel microsphere 20-25 part, Rhizoma amorphophalli fiber 10-30 part, absorbent cotton 10-15 part, become filter core with the winding of water suction body paper.
2. the preparation method of the tasty and refreshing gas cigarette filter core of a kind of konjaku according to claim 1, it is characterized in that the preparation of described konjaku glucomannan alkaline aqueous solution: by weight, get 0.5mol/L hydrochloric acid and 65 parts of deionized water mixings of 8 parts, 15 parts of konjaku glucomannans are added in mixed liquor, mechanical agitation becomes gelatin, put into incubator 115 DEG C degraded 60min, taking-up adds 14 parts of 0.5mol/LNaOH solution, stirring makes it all dissolve, elimination impurity, makes konjaku glucomannan alkaline aqueous solution.
3. the preparation method of the tasty and refreshing gas cigarette filter core of a kind of konjaku according to claim 1, it is characterized in that the preparation of described medicine carrying konjak portuguese gansu polyose gel microsphere: get the tuber of dwarf lilyturf 6 parts, radix scrophulariae 9 parts, 2 parts, Radix Glycyrrhizae add water 200 parts and boil, decoct to 100ml, incline and fried liquid, so repeat 2 times; Merge fried liquid and filter, removing impurity, by centrifugal for filtrate 6000r/min 3min, removing supernatant, obtain concentrate; Put in concentrate by dry konjak portuguese gansu polyose gel microsphere, take out after 20h, 60 DEG C are dried to moisture content not higher than 5%, take out, obtain medicine carrying konjak portuguese gansu polyose gel microsphere.
4. the preparation method of the tasty and refreshing gas cigarette filter core of a kind of konjaku according to claim 1, it is characterized in that the preparation of described Rhizoma amorphophalli fiber: get konjaku glucomannan 15 parts, be incorporated as stirring and dissolving in the purified water of its weight 30 times, gelatinization leaves standstill 2h and obtains No. 1 sample for subsequent use; Get the starch 25 parts that purity is 75%, mix with No. 1 sample for subsequent use, obtain No. 2 samples for subsequent use; Get the dietary alkali 30 parts that purity is 80%, prepare the edible alkali solution of 100 parts, edible alkali solution is mixed with No. 2 samples for subsequent use, obtain No. 3 samples for subsequent use; Pour in filter core mould by No. 3 samples for subsequent use, at 80 DEG C, steam 50min, after taking-up, then the refrigerator and cooled putting into-40 DEG C freezes 20h, and taking-up is thawed, and being dried to moisture content at 60 DEG C is 5%, obtains Rhizoma amorphophalli fiber.
5. the preparation method of the tasty and refreshing gas cigarette filter core of a kind of konjaku according to claim 1, it is characterized in that describedly preparing filter core: by weight, get loquat Bulbus 5 parts, activated carbon 10 parts, dry konjak portuguese gansu polyose gel microsphere 10 parts, peppermint konjak portuguese gansu polyose gel microsphere 20 parts, medicine carrying konjak portuguese gansu polyose gel microsphere 20 parts, Rhizoma amorphophalli fiber 10 parts, 10 parts, absorbent cotton, become filter core with the winding of water suction body paper.
6. the preparation method of the tasty and refreshing gas cigarette filter core of a kind of konjaku according to claim 1 or 5, it is characterized in that the assemble method of described filter core: filter core is divided into 7 layers, putting in order of each material respectively is toward cigarette holder direction from chimney: Rhizoma amorphophalli fiber, activated carbon, absorbent cotton, dry konjac glucomannan gel micro-ball, loquat Bulbus, peppermint konjac glucomannan gel micro-ball and medicine carrying konjac glucomannan gel micro-ball load in mixture, Rhizoma amorphophalli fiber.
7. the tasty and refreshing gas cigarette filter core of the konjaku prepared by the either method described in claim 1-6.
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| CN112717890A (en) * | 2020-12-03 | 2021-04-30 | 云南中烟工业有限责任公司 | Baked fermented plant konjac glucomannan composite porous particle, preparation method and application thereof |
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