CN104998437A - Oil-water separation method - Google Patents

Oil-water separation method Download PDF

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CN104998437A
CN104998437A CN201510432733.7A CN201510432733A CN104998437A CN 104998437 A CN104998437 A CN 104998437A CN 201510432733 A CN201510432733 A CN 201510432733A CN 104998437 A CN104998437 A CN 104998437A
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cyclone
water
oil
underflow
item
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CN104998437B (en
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吴超
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Yunxiao Food Inspection Center
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Quzhou Yifan Design Co Ltd
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Abstract

The present application discloses an oil-water separation system, which comprises an oil-water separation portion and a water treatment portion, wherein the oil-water separation portion separates an oil-water mixture into oil and intermediate water, the intermediate water enters the water treatment portion so as to further be separated into heavy impurity and water, the oil-water mixture is separated into a light item branch and a weight item branch by the crude separation cyclone of the oil-water separation portion, and the heavy product separated from the light item is led to the weight item branch so as to be enriched, such that the sorting efficiency of the light item is improved, and the sorting precision of the weight item is improved; although the sorting precision of the light item is not obtained and one part of the oil runs out from the underflow of the first cyclone, the whole light item only uses the one-stage cyclone, ie., the first cyclone, and no other cyclones are subjected to re-selection and recirculation cleaning, such that the light item sorting is simple and is easy to control; and for the heavy item, with the adjustability of the closed circuit recirculation cleaning formed by the second cyclone and the third cyclone, the oil running defect of the light item can be overcome, and all sorting errors in the closed circuit recirculation cleaning can be solved.

Description

A kind of oil-water separation method
The present invention is the divisional application of patent of invention " a kind of oil-water separation method ", and the applying date of original application is on March 28th, 2014, and the application number of original application is 201410121534X, and the invention and created name of original application is " a kind of oil-water separation method ".
Technical field
The application relates to a kind of oil-water separation method, is specifically related to a kind of method utilizing gravity separation device to carry out water-oil separating.
Background technology
Cyclone is the conventional equipment in water-oil separating, and it has little, the easy-operating advantage of energy consumption.Typical cyclone water-oil separating at present mainly contains two kinds, and one is that profit is discharged as light item from overfall by cyclone, and heavily assorted from underflow discharge, light item carries out water-oil separating further.The shortcoming of this separation is, choose in dividing of reality, because worry that oil is run out of from underflow, because this reducing heavily assorted discharge precision, make the heavily assorted not centrifugal fully of a part and enter overfall, and heavily assorted very large for the damage of water-oil separating precision equipment, and also this kind equipment accurately will isolate a certain item in the first stage, have a strong impact on selected amount, made the setting that the sorting load of whole sorting flow process is uneven.One is also had to be with cyclone rough segmentation water oil two, then weight two segments separately in two branch roads, this sorting makes overall sorting flow process more smooth, but it is long especially that the shortcoming of this sorting is flow process, cyclone itself is a kind of screening installation of adjustability difference, the sorting reliability of the longer entirety of flow process is poorer, therefore the urgently simple separation system efficiently of a set of flow process.
In addition, the impact of water-oil separating on environment can not be ignored, and middle water and heavily assorted process are difficult problems; this relates generally to the ability that separating heavy is assorted from water; heavily mix in prior art and be separated or low precision with water, or need to shut down cleaning, online non-stop-machine continuous seepage cannot be realized.
Summary of the invention
The object of the present invention is to provide a kind of oil-water separation method, solve the defect of water-oil separating in aforesaid prior art.
The present invention realizes by the following method: oil water mixture is first separated into oil and middle water by water-oil separating radicals by which characters are arranged in traditional Chinese dictionaries, middle water enters water-handling portion would and is separated into heavily assorted and water further, it is characterized in that, water-oil separating portion uses rough segmentation cyclone oil water mixture to be separated into light item and heavy item two branch roads, the isolated heavy product of light item guides the enrichment of heavy item branch road into, and water-handling portion would processes middle water continuously.
Be more preferably, water-oil separating portion mainly comprises rough segmentation cyclone and first, second and third cyclone, oil water mixture is carried out rough segmentation by rough segmentation cyclone, in stoste, the oil of 70%-75% enters overflow and enters the first cyclone, and underflow introduces the second cyclone, being connected of the second servo loop that the entrance of rough segmentation cyclone separates with the underflow of three cuff technique, the overflow that rough segmentation cyclone is separated and the large branch road of underflow two, i.e. light item and heavy item two branch roads, for light item, improve the efficiency of separation; For heavy item, improve sharpness of separation.
Be more preferably, it is the purity ensureing overfall oil that the described raising efficiency of separation is specially the first cyclone design, the water of the overwhelming majority and the oil of a part enter underflow, charger is provided with at the first cyclone inlet place, the overflow of the first cyclone enters three-phase Gravity Separation machine, three-phase Gravity Separation machine utilizes the triangular gravity of gas, oil, water different with density and occurs layering, be separated three-phase, the gas that charger is filled with is discharged from exhaust outlet after upwards being floated from aqueous phase by oil in three-phase Gravity Separation machine.
Be more preferably, the described raising sharpness of separation cyclone that to be the second cyclone be designs based on the purity of overfall oil, the underflow of rough segmentation cyclone and the first cyclone enters the second cyclone, through being separated, second cyclone overflow is that high-purity oil enters three-phase Gravity Separation machine, underflow is the water, heavily assorted of sub-fraction oil and the overwhelming majority, and underflow enters three cuff technique, oil is there is not in three cuff technique underflow, the overflow of three cuff technique is filled and is permitted to occur that more water mixes with oil and turns back to the arrival end of the second cyclone, detecting devices is all established at the overfall of three cuff technique and underflow opening, two detecting devices are connected with detector, the overfall of three cuff technique and underflow opening are also provided with the first control valve and the second control valve, underflow also has the first loop Jiang Shui to guide the entrance of three cuff technique into, also there is the entrance that water is guided into rough segmentation cyclone by second servo loop, when the underflow of three cuff technique be detected Equipment Inspection go out to have oil to run out of time, second control valve is to underflow current limliting, water is forced to overfall, 3rd control valve in the first loop is opened simultaneously, to the entrance moisturizing of three cuff technique, also be the process of supercharging simultaneously, oil in three cuff technique moves to overfall more fully, if when too many water appears in the overfall of three cuff technique, the problem not existing and run oil is described in underflow, and at this moment the first control valve current limliting, forces out underflow opening by water, ensures that in overflow, oil is controlled with the ratio of water.
Be more preferably, water-handling portion would comprises three groove trash separators, it is made up of the first to three groove, the aqueous phase of three-phase Gravity Separation machine mixes the first-stage tank being entered three groove trash separators by first-stage tank entrance with the underflow of three cuff technique, the exit normal of first-stage tank entrance is downward, the port of export has shunting disk, shunting disk is the horizontally disposed disk with radial curved grooves, current under the guiding of shunting disk by curved grooves slow after enter first-stage tank, first-stage tank is subsider, bottom first-stage tank during impurities removal, first-stage tank water level decreasing also goes out impurity discharging port by heavily assorted; Be connected by one-way pump between first-stage tank with second-level groove, one-way pump is from first-stage tank outlet to second-level groove entrance pumping clarified solution, sieve structure is tiltedly installed with between the second-level groove entrance of second-level groove and second-level groove export, it is a two-way pump structure between second-level groove and three grades of grooves, water after filtration is passed through second-level groove outlet pump to three grades of groove entrances by two-way pump structure, and second-level groove also has impurity discharging port.
Be more preferably, impeller is provided with near second-level groove outlet, during second-level groove outlet reverse drainage, impeller raises backward erosion compass screen surface by waterborne, when water treatment, water after filtration is passed through second-level groove outlet pump to three grades of groove entrances by two-way pump structure, when compass screen surface blocks, compass screen surface can increase due to the effect deflection of hydraulic pressure, the water-head of compass screen surface both sides also can become large, utilize compass screen surface deflection and/or compass screen surface both sides water level difference to judge whether compass screen surface blocks, when testing agency finds that compass screen surface blocks, two-way pump structure reversing pump water, the water of three grades of grooves is oppositely fed second-level groove, by discharging to the effect of compass screen surface reverse cleaning the granule blocked at compass screen surface, granule glides and discharges with the impurity discharging port of current from second-level groove, during second-level groove outlet reverse drainage, waterborne raising is washed away compass screen surface by impeller, in the impurities removal stage, the work of one-way pump does not stop, the water of second-level groove entrance ejection and second-level groove export the water sprayed and form combined-flow, combined-flow disturbance is stronger, better discharge granule.
Beneficial effect:
1) the application proposes an important sorting principle, namely for light item, improves the efficiency of separation; For heavy item, improve sharpness of separation, and carried out relative arrangement according to this principle.For light item, although sacrifice sharpness of separation, part oil is run out of from the first cyclone underflow, but whole light item only employs this one-level cyclone of the first cyclone in assorting room, other cyclone is not had to select and Hui Xuan again, the sorting of so light item is very simple, easily controls; And for heavy item, the adjustability of the closed circuit Hui Xuan of second, third cyclone composition can overcome the race oil defect of light item, all solution is chosen to fall at closed circuit time all sorting errors, operating personnel only need simply to adjust arbitrary rank cyclone number of closed circuit time choosing part, greatly reduce the layout difficulty of cyclone;
2) choose for closed circuit time in the application, the overfall of three cuff technique and underflow are equipped with detecting devices, by the control of detector, can control the discharge of underflow accurately, realize the dynamic conditioning of separation operation;
3) present application addresses the process difficult problem for water middle in continuous water-oil separating operation, the three groove trash separators that inventor proposes utilize the judgement to compass screen surface stopping state, backward erosion compass screen surface, achieve Hand scarf compass screen surface, for water-oil separating, portion provides sound assurance.
Accompanying drawing explanation
Fig. 1 is the schematic diagram of oil-water separation system;
In figure: 1, rough segmentation cyclone; 2, abundant equipment; 3, the first cyclone; 4, three-phase Gravity Separation machine; 5, the second cyclone; 6, three cuff technique; 7, detector; 8, the first control valve; 9, the second control valve; 10, the 3rd control valve; 11, three groove trash separators; 12, first-stage tank entrance; 13, first-stage tank outlet; 14, one-way pump; 15, second-level groove entrance; 16, second-level groove outlet; 17, two-way pump structure; 18, three grades of groove entrances; 19, sieves; 20, impurity discharging port.
Detailed description of the invention
Be described further below in conjunction with accompanying drawing:
Water-oil separating portion in the present embodiment is primarily of rough segmentation cyclone 1 and the first to three cuff technique composition, oil mixing with water stoste is carried out rough segmentation by rough segmentation cyclone 1, the operation of cyclonic separation is also had because overflow is follow-up, so the overflow of rough segmentation cyclone to be not oil more pure better, consider mobility and the separability of overflow, the oil being preferably 70%-75% in stoste enters overflow item and enters the first cyclone 3, remaining oil, water and major part be heavily assorted to enter underflow and introduces the second cyclone 5, if the purity of only unilateral pursuit rough segmentation cyclone 1 overflow, this oil is because too thick and cannot cyclonic separation again, and the selected amount of whole piece-rate system reduces greatly, therefore the separation theory in the application is thought, in the cyclonic separation of initial one-level, should directly not be separated fuel-displaced or heavily assorted, but rough segmentation oil water mixture, the task of segmentation is placed on subsequent treatment.The water management of the second servo loop that the inlet pressure of rough segmentation cyclone 1 and flow are separated by the end i.e. underflow of three cuff technique in whole water-oil separating portion, three cuff technique has description later, if it is lower that rough segmentation cyclone 1 is selected in pressure, then improve pressure by moisturizing thus increase the oil mass entering overflow.The overflow that rough segmentation cyclone 1 is separated and the large branch road of underflow two, i.e. light item and heavy item, the application proposes an important sorting principle, namely for light item, improves the efficiency of separation; For heavy item, improve sharpness of separation.And carry out following apparatus arrangement according to this principle.
First cyclone 3 is designed to the purity ensureing overfall oil, the water of such overwhelming majority and the oil of a part enter underflow, charger 2 is preferably provided with in the first cyclone 3 porch, find in the practical operation of sorting, gas in cyclone when overfall eddy current catch end is close, there is very strong impetus to oil droplet, can help to collect oil droplet.First cyclone is in order to ensure the efficiency be separated, sacrifice the precision of sorting in a way, there is race oil to a certain degree, but the overflow item that rough segmentation cyclone 1 is separated and light item, only need a sorting just can ensure the purity of oil, it contains a small amount of water, hardly containing heavily assorted, this is a kind of well protection to follow-up three-phase Gravity Separation machine 4 and other accurate screening installation, that is the eddy flow shunting only having carried out first this one-level of cyclone 3 just reaches high sorting standard, centre does not have loop gravity treatment, there is no the selected cyclone of multistage layout, this substantially reduces sorting flow process, improve the efficiency of separation.Three-phase Gravity Separation machine 4 is prior art, utilize the triangular gravity of gas, oil, water different with density and occur layering, be separated three-phase, the gas that charger 2 is filled with is discharged from exhaust outlet after upwards being floated from aqueous phase by oil in three-phase Gravity Separation machine.
Second cyclone 5 is also the cyclone designed based on the purity of overfall oil, the underflow of rough segmentation cyclone 1 and the first cyclone 3 enters the second cyclone 5, through being separated, second cyclone 5 overflow is that high-purity oil enters three-phase Gravity Separation machine 4, underflow is the water, heavily assorted of sub-fraction oil and the overwhelming majority, and underflow enters three cuff technique 6.Three cuff technique 6 is designed to ensure not occur oil in underflow, for this reason, relax the requirement of the overflow of three cuff technique 6 as far as possible, more water can be there is and turn back to the arrival end of the second cyclone 5 in the overflow of three cuff technique 6, underflow due to three cuff technique 6 is the three groove trash separators that directly will enter water treatment stage, therefore requirement that will be stricter for the underflow of three cuff technique 6, detecting devices is all established at the overfall of three cuff technique 6 and underflow opening, two detecting devices are connected with detector 7, the overfall of three cuff technique 6 and underflow opening are also provided with the first control valve 8 and the second control valve 9, underflow also has the first loop Jiang Shui to guide the entrance of three cuff technique 6 into, also there is the entrance that water is guided into rough segmentation cyclone 1 by second servo loop.
When the underflow of three cuff technique 6 be detected Equipment Inspection go out to have oil to run out of time, second control valve 9 pairs underflow current limliting, water is forced to overfall, 3rd control valve 10 in the first loop is opened simultaneously, to the entrance moisturizing of three cuff technique 6, also be the process of supercharging, the oil in three cuff technique 6 moves to overfall more fully simultaneously.If when there is too many water in the overfall of three cuff technique 6, the problem not existing and run oil is described in underflow, the operating pressure that in overflow, water increases the second cyclone 5 too much on the contrary, overall sorting capability declines, at this moment the first control valve 8 current limliting, water is forced out underflow opening, ensures that in overflow, oil is controlled with the ratio of water.Detector 7 and detecting devices itself are prior aries, do not repeat them here; It is emphasized that for water-oil separating field, treat that the component ratio of point mixed flow is stable, therefore for detector 7, also can artificial sampling detect, this can't pay the artificial of larger amount.
Rough segmentation cyclone 1 and the first cyclone 3 underflow form through the 2nd three cuff technique select the high-precision You Heshui that has been separated of structure for closed circuit time, and introduce detector 7, more ensure that the reliability of water-oil separating.All in all water-oil separating part, overflow for rough segmentation cyclone 1 adopts high efficiency water-oil separating, and the cyclone that be mixed by the underflow of rough segmentation cyclone 1 underflow and the first cyclone feeding second and three cuff technique form selects structure for closed circuit time, by the sorting across branch road, form the sorting focused on efficiency and focus on separation accuracy mixed principle.In the water-oil separating of reality, the production capacity of what we paid close attention to is valuable oil, oil yield is substantially constant for oil well, we reduce the layout to the complexity of light item branch road for this reason, all sorting errors are all concentrated on heavy item branch road, can increase or reduce the group number of the closed circuit Hui Xuan of cyclone according to the actual needs, also second can be adjusted according to production capacity, three cuff technique number separately, focus for whole production just concentrates on heavy item branch road, and this branch road also introduces the detector 7 automatically controlled, reduce further the difficulty of control, for the closed-loop path of the 2nd three cuff technique composition, just the overfall of the second cyclone and the underflow of three cuff technique are paid close attention to, overflow for three cuff technique is general concern, it is only the auxiliary detection for underflow discharge.System is selected again in the cyclone composition loop that closed-loop path does not have employing more than three grades or three grades, this is because as previously described, cyclone is a kind of screening installation of adjustability difference, cyclone level can affect what sharpness of separation last too much, sometimes needs to use pump class to ensure selected pressure.So the closed circuit Hui Xuan that the application only adopts the cyclone of two-stage to form, and be furnished with detector 7, can also adjust the quantity of the cyclone of any one-level, thus be suitable for the sorting of the oil water mixture of different moisture content.
Continuous seepage due to water-oil separating portion causes an important technical problem, namely create a large amount of containing heavily assorted middle water, according to the standard of China's mining industry draining, this kind of water cannot directly discharge, therefore need one can continuous seepage, water treatment system that disposal ability is large support water-oil separating portion, otherwise whole oil-water separation system just cannot run normally.For this reason, inventor proposes three groove trash separators 11, effectively solves this technical problem.
Three groove trash separators 11 are made up of the first to three groove, the aqueous phase of three-phase Gravity Separation machine 4 mixes the first-stage tank together being entered three groove trash separators 11 by first-stage tank entrance 12 with the underflow of three cuff technique, the exit normal of first-stage tank entrance 12 is downward, the port of export has water flow speed reduction device, water flow speed reduction device is preferably shunting disk, shunting disk is the horizontally disposed disk with radial curved grooves, and current, under the guiding of shunting disk, enter first-stage tank again by the slow of curved grooves.First-stage tank is subsider, the heavily assorted bottom being deposited in first-stage tank as much as possible, and being preferably first-stage tank has the higher degree of depth, and bottom first-stage tank during impurities removal, first-stage tank water level decreasing also goes out impurity discharging port by heavily assorted.Be connected by one-way pump 14 between first-stage tank with second-level groove, one-way pump 14, from first-stage tank outlet 13 to second-level groove entrance 15 pumping clarified solution, it should be noted that first-stage tank outlet 13 should away from first-stage tank entrance 12, prevent current short circuit from crossing first-stage tank and directly enter second-level groove, thus first-stage tank was lost efficacy.The second-level groove entrance 15 of second-level groove and second-level groove are tiltedly installed with sieve structure between exporting 16, sieve structure is for removing the granule easily suspended, but sieve structure has a shortcoming to need periodic cleaning exactly, the short grained compass screen surface of sorting is different from other compass screen surface, granule is very easy to block discharges in sieve aperture instead of along compass screen surface downslide, if mesh is blocked to a certain extent in prior art, just must shut down cleaning or change compass screen surface, this cannot adapt to aforesaid water-oil separating part, certainly also to have in the prior art and granule do not processed and directly discharge, only that bulky grain or similar easy recovery section are reclaimed, but this causes huge pressure to plant area's surrounding enviroment.
In order to solve this technical problem, be a two-way pump structure 17 between second-level groove and three grades of grooves in the present embodiment, when water treatment, water after filtration is exported 16 pumps to three grades of groove entrances 18 by second-level groove by two-way pump structure 17, when compass screen surface blocks, compass screen surface can increase due to the effect deflection of hydraulic pressure, the water-head of compass screen surface both sides also can become large, what those skilled in the art can know is, can utilize including but not limited to deflection and water level difference to judge whether compass screen surface blocks, when testing agency finds that compass screen surface blocks, two-way pump structure reversing pump water, the water of three grades of grooves is oppositely fed second-level groove, by discharging to the effect of compass screen surface reverse cleaning the granule blocked at compass screen surface, granule glides and discharges with the impurity discharging port 20 of current from second-level groove, preferably export 16 places in second-level groove and be provided with impeller, when second-level groove exports 16 reverse drainage, waterborne raising is washed away compass screen surface by impeller.In the impurities removal stage, the work of one-way pump 14 does not stop, and the water that second-level groove entrance 15 sprays and second-level groove export 16 water sprayed and form combined-flow, and combined-flow disturbance is comparatively strong, better discharges granule.Therefore, no matter be water treatment or impurities removal stage, whole three groove trash separators are operating always, and for the continual process of middle water in water-oil separating stage, the needing of solution shuts down clear assorted or change the technical barrier of compass screen surface.
Although carried out special description with reference to embodiment to the disclosed oil-water separation method related to; embodiment described above is illustrative and not restrictive; without departing from the present invention, all changes and amendment are all within protection scope of the present invention.

Claims (1)

1. an oil-water separation system, have water-oil separating portion and water-handling portion would, it is characterized in that, water-oil separating portion uses the overflow of rough segmentation cyclone (1) to be light item branch road, the underflow of the overflow of rough segmentation cyclone (1) is attached most importance to a branch road, and light item branch road has will the heavily assorted pipeline discharged to heavy item branch road;
Water-oil separating portion comprises rough segmentation cyclone (1) and first, second and third cyclone, and the overflow pipe of rough segmentation cyclone is communicated with the first cyclone (3), and the underflow pipe of rough segmentation cyclone is communicated with the second cyclone,
Second cyclone overflow pipe connects three-phase Gravity Separation machine, and the second cyclone underflow pipe connects three cuff technique (6); Three cuff technique (6) overflow pipe connects the arrival end of the second cyclone (5), detecting devices is all established at the overfall of three cuff technique and underflow opening, two detecting devices are connected with detector (7), the overfall of three cuff technique is also provided with the first control valve (8), the underflow opening of three cuff technique is also provided with the second control valve (9), the underflow opening of three cuff technique also has the first loop Jiang Shui to guide the entrance of three cuff technique into, also has the entrance that water is guided into rough segmentation cyclone (1) by second servo loop;
Be more preferably, the overflow of the first cyclone (3) is connected with three-phase Gravity Separation machine, and the underflow opening of three cuff technique is connected with three-phase Gravity Separation machine.
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