The content of the invention
In order to overcome shortcoming and defect present in prior art, it is an object of the invention to provide a kind of heavy scummer
Ash-retention efficiency measuring method, technical solution of the present invention is simple, required time of measuring is short, accuracy of measurement is high.
The purpose of the present invention is achieved through the following technical solutions:A kind of measuring method of the ash-retention efficiency of heavy scummer, bag
Include following steps:
Step A, sample:Sampled using sample cock in the stock inlet of scummer, good slurry outlet and slurry exit, with title
Amount equipment weighs M1Gram enter to starch sample, M2Gram good slurry sample and M3Gram slurry sample, save backup;
Step B, the measurement of concetration of sample:Each sample of separation of solid and liquid, isolated solid is placed in baking oven and is dried to
Constant weight, and the quality recorded into after isolated solid drying to the constant weight of slurry sample, good slurry sample, slurry sample is weighed respectively
m1、m2、m3, then calculated and measured into slurry sample solution concentration C respectively by concentration formula C=m/MEnter, good slurry sample solution concentration CIt is good, slurry examination
Sample concentration CSlag;
Step C, ash-retention efficiency calculates:Pass through formula CT=CSlag/CEnterTry to achieve enrichment factor CT, finally by formula S=(CSlag-CIt is good×
CT)/(CSlag-CIt is good) × 100% measures the ash-retention efficiency S of heavy scummer.
The present invention need not measure the flow into slurry, good slurry and slurry, it is only necessary to measure the concentration into slurry, good slurry and slurry
The ash-retention efficiency of heavy scummer can be drawn by data processing, scheme is simple, and required time of measuring is short, efficiency high, and passes through
The ash-retention efficiency of heavy scummer is directly calculated in concentration, and intuitively, the degree of accuracy is high.
Wherein, the flow that enters to starch of scummer is FEnter, the good slurry flow of scummer is FIt is good,The slurry flow of scummer is FSlag,
Then:
FEnter=FIt is good+FSlag、FEnter×CEnter=FIt is good×CIt is good+FSlag×CSlag,
→ → →
→ → =ash-retention efficiency,
So ash-retention efficiency==。
Wherein, the weighing equipment is the electronic balance that precision is 0.01g.Electronic balance precision is high, and it is accurate to weigh, deslagging
The degree of accuracy of rate measurement result is high.
Wherein, it is described to enter to starch sample, good slurry sample, the mass M of slurry sample1、M2、M3It is 25g.Meeting to measure need
On the premise of asking, by sample sampling quality control in rational scope, the waste of resource is avoided.
Wherein, equipment is bottle,suction used by separation of solid and liquid.In the actual use of the present invention, first funnel is sealed and pacified
It on bottle,suction, then will be attached to dry filter paper in funnel, start air exhauster, realize separation of solid and liquid.Consolidated by bottle,suction
Liquid separating sample, speed is fast, and solid separation is abundant, ensure that the degree of accuracy for measuring ash-retention efficiency.
Wherein, the suction filtration time that the bottle,suction carries out separation of solid and liquid is 11-15min.Proper extension filters the time, to the greatest extent may be used
The moisture in solid can be reduced, shortens the drying time of baking oven, improves efficiency.
Wherein, the drying temperature of the baking oven is 125-145C °, drying time 30-35min.Drying temperature and drying
Time is reasonable in design, and solid is dried thoroughly, avoids containing moisture among sample, so as to influence the degree of accuracy of ash-retention efficiency measurement..
Wherein, the group number of each sample is 5 groups, and the ash-retention efficiency is remaining each group after 5 groups of samples remove invalid group
The average value of sample measurement result.Using multigroup sampling, the invalid group of measuring method averaged is removed, ensure that data has
Effect property and the degree of accuracy.
Wherein, in the step B, the environment temperature for weighing record is 21-25C °, humidity 8-10%.Under low-moisture conditions
Dried solid is weighed, avoids ambient humidity too high, the moisture in solid sorbent environment, reduces measurement error, improves measurement
The degree of accuracy.
The beneficial effects of the present invention are:The present invention need not measure the flow into slurry, good slurry and slurry, reduce measurement
The amount of data, significantly shortens time of measuring, improves operating efficiency, it is only necessary to measures the concentration into slurry, good slurry and slurry
The ash-retention efficiency of heavy scummer can be drawn by data processing, scheme is simple, and required time of measuring is short, efficiency high, and passes through
The ash-retention efficiency of heavy scummer is directly calculated in concentration, and intuitively, the degree of accuracy is high.
Embodiment 1
A kind of measuring method of the ash-retention efficiency of heavy scummer, comprises the following steps:
Step A, sample:Sampled using sample cock in the stock inlet of scummer, good slurry outlet and slurry exit, with title
Amount equipment weighs M1Gram enter to starch sample, M2Gram good slurry sample and M3Gram slurry sample, save backup;
Step B, the measurement of concetration of sample:Each sample of separation of solid and liquid, isolated solid is placed in baking oven and is dried to
Constant weight, and the quality recorded into after isolated solid drying to the constant weight of slurry sample, good slurry sample, slurry sample is weighed respectively
m1、m2、m3, then calculated and measured into slurry sample solution concentration C respectively by concentration formula C=m/MEnter, good slurry sample solution concentration CIt is good, slurry examination
Sample concentration CSlag;
Step C, ash-retention efficiency calculates:Pass through formula CT=CSlag/CEnterTry to achieve enrichment factor CT, finally by formula S=(CSlag-CIt is good×
CT)/(CSlag-CIt is good) × 100% measures the ash-retention efficiency S of heavy scummer.
The weighing equipment is the electronic balance that precision is 0.01g.
It is described to enter to starch sample, good slurry sample, the mass M of slurry sample1、M2、M3It is 25g.
Equipment is bottle,suction used by separation of solid and liquid.
The suction filtration time that the bottle,suction carries out separation of solid and liquid is 11min.
The drying temperature of the baking oven is 125C °, drying time 30min.
The group number of each sample is 5 groups, and the ash-retention efficiency is that remaining each group sample is surveyed after 5 groups of samples remove invalid group
Measure the average value of result.
In the step B, the environment temperature for weighing record is 21C °, humidity 8%.
The measurement data of the present embodiment, see the table below: