CN104984819B - A kind of oil shale end ore deposit ore-dressing technique - Google Patents

A kind of oil shale end ore deposit ore-dressing technique Download PDF

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Publication number
CN104984819B
CN104984819B CN201510465338.9A CN201510465338A CN104984819B CN 104984819 B CN104984819 B CN 104984819B CN 201510465338 A CN201510465338 A CN 201510465338A CN 104984819 B CN104984819 B CN 104984819B
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product
oil shale
ore
water
ore deposit
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CN104984819A (en
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常建勇
石增鑫
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JINYITONG TECHNOLOGY (BEIJING) CO LTD
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JINYITONG TECHNOLOGY (BEIJING) CO LTD
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03BSEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
    • B03B7/00Combinations of wet processes or apparatus with other processes or apparatus, e.g. for dressing ores or garbage
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03BSEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
    • B03B9/00General arrangement of separating plant, e.g. flow sheets
    • B03B9/02General arrangement of separating plant, e.g. flow sheets specially adapted for oil-sand, oil-chalk, oil-shales, ozokerite, bitumen, or the like
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B07SEPARATING SOLIDS FROM SOLIDS; SORTING
    • B07BSEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
    • B07B1/00Sieving, screening, sifting, or sorting solid materials using networks, gratings, grids, or the like
    • B07B1/28Moving screens not otherwise provided for, e.g. swinging, reciprocating, rocking, tilting or wobbling screens

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Geology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

A kind of oil shale end ore deposit ore-dressing technique, belongs to oil shale industry field, and be particularly suitable for use in oil shale end ore deposit processing and utilization industry.Water is added to carry out (10 13) mm screenings in oil shale raw ore, product on sieve (>10 13mm) carry out it is broken after and undersized product (<10 13mm) mixing sorted using hydrocyclone, underflow product is dehydrated into spoil product by high-frequency screen, overflow product is granulated after high-frequency screen is dehydrated, as block concentrate product, it is all that concentrating clarifying is carried out by black water caused by high-frequency screen, sediment obtains product from failing through press filtration, and primary water and filtrate are used as recirculated water.The present invention is after the ore deposit sieving approach of oil shale end, directly sorted using hydrocyclone, it is simple, efficient, economical, solve the problems, such as that conventional technological process is complicated, investment of production is high, the efficiency of separation is low, the concentrate yield of oil shale is effectively increased, there is higher economic value.

Description

A kind of oil shale end ore deposit ore-dressing technique
Technical field
The invention belongs to oil shale industry field, and be particularly suitable for use in oil shale end ore deposit processing and utilization industry, for removing oil Inorganic mineral in the ore deposit of shale end, higher concentrate yield is obtained, produce bigger economic benefit.
Background technology
Oil shale belongs to unconventional petroleum resources, and it is non-to be listed in 21 century with aboundresources and the feasibility of utilization Often important takes over the energy, and it is all non-renewable fossil energy as oil, natural gas, coal.Oil shale is done through low temperature Shale oil can be obtained by evaporating, and like crude oil gasoline, diesel oil can be made or as fuel oil in shale oils.In Waste Era of Oil, have It is active to close utilization of the country to oil shale.Oil Shale Resources in China rich reserves, are also produced in progress of coal mining A large amount of oil shales are given birth to, utilization oil shale can not only alleviate contradiction between oil supply and demand, can also solve because discarding oil shale Caused by environmental problem, improve resource utilization.
At present, the oil shale Chemical Manufacture process in China, simple crushing and screening is only passed through to oil shale raw ore To certain grade (common is 10-80mm), product is directly subjected to chemical industry conversion.This method causes a large amount of spoils to reside in oil It is unfavorable to subsequent transformation in shale raw ore.Publication No. disclosed in China State Intellectual Property Office September in 2014 19 days A kind of oil shale pre-selection discharge refuse -- distillation process contained CN104194814A, disclose a kind of simple two products jigging sorting Method, but pass through substantial amounts of industrial experiment in putting into practice, it was demonstrated that this method can not effectively be sorted to oil shale, in practice more There is no separating effect in the case of more, due to the very close Rock Specific Gravity of oil shale proportion, and the specific gravity of separation is all in 2.5 gram per centimeters3 More than, conventional coal jigging technology can not be used.The technique for coarse grain (>10mm) oil shale carries out pre- discharge refuse, and for oil The pre- discharge refuse technique of shale end ore deposit, still belongs to blank field, therefore how to sort oil shale end ore deposit and obtain good separating effect, into For industry problems, a kind of oil shale end mineral water is proposed by many experiments present invention and is situated between the new technology of sorting.
The content of the invention
The purpose of the present invention is the processing and utilization for oil shale end ore deposit, there is provided it is a kind of it is simple, efficiently, can significantly improve The oil shale end ore deposit ore-dressing technique of oil shale concentrate yield.
The object of the present invention is achieved like this, and the oil shale beneficiation method step is as follows:
A. oil shale raw ore is subjected to (10-13) mm screenings, produces undersized product and granularity of the granularity for-(10-13) mm For product on+(10-13) mm sieve;
B. sieve upper product turns into broken material with crusher in crushing to (10-13) mm is less than, and is mixed with undersized product;
C. mixed material is classified using hydraulic classification swirler, and two kinds of materials, underflow product are produced after classification And overflow product;
D. underflow product produces spoil product and black water by high-frequency screen dehydration;
E. overflow product produces light product and black water by high-frequency screen dehydration;
F. light product, which be granulated, turns into block concentrate product;
G. the black water obtained by dehydration d. and dehydration e. collects carry out concentrating clarifying, produces primary water And enriched product;
H. enriched product turns into product from failing by press filtration, and filtrate is continuing with primary water collectively as recirculated water.
The dehydration equipment is high-frequency screen or its equivalent screening installation.
Above-mentioned ore-dressing technique is employed, the present invention can largely improve the oil content of oil shale concentrate, can effectively improve spoil Ash content, simplification of flowsheet, sorting cost is reduced, is a kind of brand-new oil shale end ore deposit method for separating.This method also improves The resource utilization of oil shale, the economic benefit of enterprise is added, meet the requirement of sustainable development and energy-conserving and environment-protective, had wide General practicality.
Brief description of the drawings
Fig. 1 is a kind of oil shale end ore deposit mineral processing circuit figure of the present invention.
In figure:1. undersized product;2. the upper product of sieve;3. broken material;4. underflow product;5. overflow product;6. spoil produces Product;7. black water;8. black water;9. light product;10. piece concentrate product;11. primary water;12. enriched product;13. filtrate;14. Product from failing;
Embodiment
One embodiment of the present of invention is further described below in conjunction with accompanying drawing:
As shown in figure 1, a kind of oil shale end ore deposit ore-dressing technique step of the present invention is as follows:
A. oil shale raw ore is subjected to (10-13) mm screenings, produces undersized product 1 and granularity of the granularity for-(10-13) mm For product 2 on+(10-13) mm sieve;
B. sieve upper product 2 turns into broken material 3 with crusher in crushing to (10-13) mm is less than, and mixed with undersized product 1 Close;
C. mixed material is classified using hydraulic classification swirler, and two kinds of materials, underflow product 4 are produced after classification And overflow product 5;
D. underflow product 4 produces spoil product 6 and black water 7 by high-frequency screen dehydration;
E. overflow product 5 produces light product 9 and black water 8 by high-frequency screen dehydration;
F. light product 9, which be granulated, turns into block concentrate product 10;
G. the black water 7,8 obtained by dehydration d. and dehydration e. collects carry out concentrating clarifying, produces clear Clear water 11 and enriched product 12;
H. enriched product 12 turns into product from failing 14 by press filtration, and filtrate 13 is continued with primary water 11 collectively as recirculated water Use.
The dehydration equipment is high-frequency screen or its equivalent screening installation.
Though the present invention lists less embodiment, what the person skilled of this area was done to the present invention some changes Type, improvement, replacement etc., or the embodiment above make any combinations change, within protection scope of the present invention.

Claims (2)

1. a kind of oil shale end ore deposit ore-dressing technique, it is characterised in that the processing step is as follows:
A. oil shale raw ore is subjected to (10-13) mm screenings, produce granularity is for-(10-13) mm undersized product (1) and granularity Product (2) on+(10-13) mm sieve;
B. sieve upper product (2) turns into broken material (3) with crusher in crushing to (10-13) mm is less than, and mixed with undersized product (1) Close;
C. mixed material is classified using hydraulic classification swirler, after classification produce two kinds of materials, underflow product (4) and Overflow product (5);
D. underflow product (4) produces spoil product (6) and black water (7) by high-frequency screen dehydration;
E. overflow product (5) produces light product (9) and black water (8) by high-frequency screen dehydration;
F. light product (9), which be granulated, turns into block concentrate product (10);
G. carry out concentrating clarifying is collected in the black water (7) obtained by dehydration d. and dehydration e., (8), produces clear Clear water (11) and enriched product (12);
H. enriched product (12) turns into product from failing (14) by press filtration, and filtrate (13) is with primary water (11) collectively as recirculated water It is continuing with.
2. a kind of oil shale end ore deposit ore-dressing technique according to claim 1, it is characterised in that the dehydration equipment is high frequency Sieve.
CN201510465338.9A 2015-07-31 2015-07-31 A kind of oil shale end ore deposit ore-dressing technique Active CN104984819B (en)

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Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105536980B (en) * 2016-01-28 2017-12-08 北京国华科技集团有限公司 A kind of oil shale high accuracy method for separating
CN105665125A (en) * 2016-03-23 2016-06-15 北京科技大学 Device and method for concentrating kerogen from easily-slimed oil shale
CN106607183B (en) * 2017-02-09 2019-11-08 中国矿业大学 A kind of modular high-density coal measures oil shale process for upgrading and upgrading system
CN108855579B (en) * 2017-05-12 2020-09-01 山西世纪新龙腾科技有限公司 Coal dressing method by using aqueous medium cyclone
CN111298954A (en) * 2020-03-04 2020-06-19 中国矿业大学 Process for heavy-medium separation of oil shale from two pressurized products
CN115338105A (en) * 2022-07-28 2022-11-15 秦皇岛优格玛工业技术有限公司 Method and system for grading, removing powder, selecting and upgrading oil shale

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4506835A (en) * 1982-05-06 1985-03-26 Occidental Research Corp. Oil shale beneficiation
US4528090A (en) * 1983-10-17 1985-07-09 Mobil Oil Corporation Oil shale beneficiation by size reduction combined with heavy media separation
CN101602029A (en) * 2009-06-27 2009-12-16 勃利县森清能源开发有限公司 From raw coal and select the technology of cleaned coal in the locked middlings of coal
CN103831164A (en) * 2014-02-24 2014-06-04 太原理工大学 Gravity-flotation joint separation technology for coking middlings
CN104194814A (en) * 2014-09-19 2014-12-10 中国矿业大学(北京) Oil shale primary gangue discharging and distillation process
CN104226465A (en) * 2014-09-17 2014-12-24 中国矿业大学(北京) Gravity separation and kerogen enrichment technology of oil shale

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4506835A (en) * 1982-05-06 1985-03-26 Occidental Research Corp. Oil shale beneficiation
US4528090A (en) * 1983-10-17 1985-07-09 Mobil Oil Corporation Oil shale beneficiation by size reduction combined with heavy media separation
CN101602029A (en) * 2009-06-27 2009-12-16 勃利县森清能源开发有限公司 From raw coal and select the technology of cleaned coal in the locked middlings of coal
CN103831164A (en) * 2014-02-24 2014-06-04 太原理工大学 Gravity-flotation joint separation technology for coking middlings
CN104226465A (en) * 2014-09-17 2014-12-24 中国矿业大学(北京) Gravity separation and kerogen enrichment technology of oil shale
CN104194814A (en) * 2014-09-19 2014-12-10 中国矿业大学(北京) Oil shale primary gangue discharging and distillation process

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