CN104984706B - Reaction still - Google Patents
Reaction still Download PDFInfo
- Publication number
- CN104984706B CN104984706B CN201510325781.6A CN201510325781A CN104984706B CN 104984706 B CN104984706 B CN 104984706B CN 201510325781 A CN201510325781 A CN 201510325781A CN 104984706 B CN104984706 B CN 104984706B
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- CN
- China
- Prior art keywords
- sealing film
- sealing
- support
- electric heating
- cover
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000007789 sealing Methods 0.000 claims abstract description 28
- 238000010438 heat treatment Methods 0.000 claims abstract description 25
- 238000005485 electric heating Methods 0.000 claims abstract description 17
- 238000003756 stirring Methods 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000005273 aeration Methods 0.000 claims description 10
- 238000002347 injection Methods 0.000 claims description 7
- 239000007924 injection Substances 0.000 claims description 7
- 238000003780 insertion Methods 0.000 claims description 5
- 230000037431 insertion Effects 0.000 claims description 5
- 229910052756 noble gas Inorganic materials 0.000 claims description 5
- 238000007599 discharging Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 239000000463 material Substances 0.000 abstract description 19
- 238000005276 aerator Methods 0.000 abstract 2
- 239000007789 gas Substances 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 238000004043 dyeing Methods 0.000 description 2
- 150000002835 noble gases Chemical class 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000007639 printing Methods 0.000 description 2
- 230000004044 response Effects 0.000 description 2
- 238000013019 agitation Methods 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 210000004907 gland Anatomy 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Abstract
The invention relates to a reaction still. A support is fixed above a round hole in the center of a tank cover of the reaction still, a sealing spherical bearing is arranged in the support, a sphere of the sealing spherical bearing is connected with a stirring shaft, a sealing film is fixed between the round hole and the sphere, a sealing cavity is formed between the sealing film and the support, and water is injected in the sealing cavity. The reaction still further comprises a gas heating device and a gas inlet pipe inserted from the bottom, the end, inserted into a tank body, of the gas inlet pipe is connected with a spiral aerator pipe in the tank body, and the spiral aerator pipe is located below an electric heating pipe. Due to the fact that the water is injected in the sealing cavity above the sealing film, when pressure in a tank changes, the sealing cavity can achieve the good supporting function on the sealing film, the sealing film cannot bulge or collapse so that the sealing film cannot bear extra tension, damage is not prone to happening, and the service life is longer. Gas input by the gas inlet pipe has the characteristic of quickly moving upwards, and therefore materials can generate convection, and heat of the electric heating pipe can be transmitted to the materials faster and more evenly.
Description
This case is Chinese invention patent application cn 201410139088.5, applying date 2014-04-09, and title is " a kind of
The divisional application of reactor "
Technical field
The present invention relates to a kind of reactor.
Background technology
Now great majority are not provided with agitating device for the reactors preparing printing and dyeing assistant so that the thing of reaction on the market
Material stirring is insufficient and uneven, and this just directly results in response speed slowly, and reacts not exclusively, wastes resource, improves life
Some reaction mediums under residual in tank after producing cost, and reaction easily corrode, and have impact on consersion unit it is impossible to improve economic effect
Benefit.
In order to solve the above problems, Chinese utility model patent cn 203123964 u, disclose one kind for preparation print
The reaction unit of dye auxiliary agent, it is provided with the shaft being inserted in can body on cover, and shaft bottom is provided with anchor oar
Leaf, realizes the stirring to material, accelerates response speed.
But some printing and dyeing assistants has harmful substance to volatilize it is therefore desirable to carry out in closed environment in preparation process
Stirring.Traditional stirred autoclave adopts packing seal or mechanical seal mostly, gland sealed poor sealing performance and resistance be big,
Easily it is lost；And mechanical seal then price height, declined using sealing property after a period of time, safeguard that replacement cost is high.
Additionally, reaction sometimes needs certain heating environment, tradition can only be realized to material by heating to tank body
Heating, firing rate is slow and tank in temperature of charge uneven, be unfavorable for that reacts is smoothed out.
Content of the invention
It is an object of the invention to: overcome the defect of above-mentioned prior art, propose a kind of reactor.
In order to achieve the above object, reactor proposed by the present invention, composition includes can body, cover, stirring motor, stirring
Axle, stirring paddle, described can body be provided with dog-house, discharging opening it is characterised in that: described cover central authorities open up circular hole, on circular hole
Side is fixed with support, is provided with sealed spherical bearing, the spheroid of described sealed spherical bearing connects shaft, close in described support
The bearing housing of blocking spherical bearing and support are fixed, and are fixed with soft sealing film between described circular hole and spheroid, described flexible sealing
Form annular seal space, this sealing intracavity fills pure water between film and support；Described can body bottom is provided with electric heating tube, and described electricity adds
Can body inwall above heat pipe is fixed with the nozzle towards obliquely downward to injection, and the can body bottom below described electric heating tube is fixed with
Pump mouth, is provided with, outside described can body, the pipeline being connected pump mouth with nozzle, and pipeline is provided with water pump；Reactor also includes
Gas-heating apparatus and an air inlet pipe inserting can body from bottom, the outlet side phase of described air inlet pipe and gas-heating apparatus
Even, the inlet end of described gas-heating apparatus connects noble gas source by pipeline, and the air inlet tube end of insertion can body connects
It is installed on the spiral type aeration tube in can body, described spiral type aeration tube is located at below electric heating tube, and described cover is provided with
Exhaustor, equipped with relief valve on described exhaustor.
Reactor of the present invention, is further improved by:
1st, on described cover, observation panel is installed.
The 2nd, thermometer in insertion can body is provided with described cover.
3rd, ringwise, interior outside is tightly connected with spheroid, cover circular hole described soft sealing film respectively by flange.
4th, the seam of described cover and can body is bonded.
5th, the injection direction of described nozzle is contrary with stirring rotational axis direction.
Reactor of the present invention realizes the omnibearing agitation of stirring paddle using ball bearing, does not stay dead angle；From soft sealing film
Sealing so that in inner pot gas do not reveal, effective protection operator and will not be to environment；Due on diaphragm seal
The sealing intracavity of side is marked with water, therefore when pressure inside the tank changes, when particularly pressure is significantly increased or when pressure drastically reduces,
Annular seal space can play good supporting role to diaphragm seal, this is because the volume of liquid is with almost when ambient pressure changes
Do not change, therefore diaphragm seal will not be heaved or subside, also would not be subject to extra tension force, therefore not cracky, use
Life-span is longer.
Therefore, the sealing structure used by the present invention is with low cost, and can bear different pressure changes in tank, has higher
Adaptability.
It is provided with electric heating tube in can body, material can be heated, and improved by the way of water circulation injection
The uniformity of heating, can transfer heat to rapidly the material in can body, realize the purpose to material heating, compare tradition not
Equipment with heating or to can body heating, reactor of the present invention can make material evenly heated, improves the anti-of material
Answer speed and stationarity, further improve production efficiency.
Additionally, the can body bottom of reactor of the present invention has been passed through air inlet pipe, using this air inlet pipe to can body delivered inside warp
Cross the noble gases of heating, and by spiral type aeration tube, hot gas is scatter, can transfer heat to rapidly in can body
Material, realize to material heating purpose；Further, since the characteristic of the gas fast upward motion of air inlet pipe input, help
In material is produced convection current, make the heat of electric heating tube faster evenly pass to material.Two aspects act on simultaneously, promote mutually
Enter, be capable of the raising temperature of charge of even.
Brief description
The present invention is further illustrated below in conjunction with the accompanying drawings.
Fig. 1 is reactor structural representation of the present invention.
Fig. 2 is the spiral type aeration tube schematic diagram of reactor of the present invention.
Fig. 3 is the nozzle jet water course schematic diagram of reactor of the present invention.
In figure label is schematically as follows:
1- can body, 1 ＇-cover, 2- motor, 3- shaft, 4- stirring paddle, 5- dog-house, 6- discharging opening, 7- observation panel, 8-
Support, 9- bearing housing, 10- spheroid, 11- soft sealing film, 12- annular seal space, 13- nozzle, 14- electric heating tube, 15- thermometer,
16- water pump, 17- pipeline, 18- exhaustor, 19- relief valve, 20- pump mouth, 21- air inlet pipe, 22- spiral type aeration tube, 23- manages
Road, 24- gas-heating apparatus.
Specific embodiment
The present invention will be further described with specific embodiment below in conjunction with the accompanying drawings.
As shown in figure 1, being reactor of the present invention, cover 1 ＇ that composition includes can body 1 and is arranged at can body 1 top, cover
1 ＇ is bonded with the seam of can body 1, cover 1 ＇ is provided with exhaustor 18, equipped with relief valve 19, cover on exhaustor 18
Observation panel 7, the thermometer 15 inserting in can body 1 are also equipped with 1 ＇, can body 1 is provided with dog-house 5, discharging opening 6, described cover
1 ＇ is provided with and is inserted into the shaft 3 driven by motor 2 in can body 1, and shaft 3 bottom is fixed with stirring paddle 4, cover 1 ＇ central authorities
Open up circular hole, circular hole is fixedly arranged above support 8, be provided with sealed spherical bearing in support 8 (by bearing housing 9 and 10 groups of spheroid
Become), the spheroid 10 of sealed spherical bearing connects shaft 3, the bearing housing 9 of sealed spherical bearing and support 8 fixation, circular hole and ball
It is fixed with ring-shaped flexible seal film 11, in ring-shaped flexible seal film 11, outside passes through flange and spheroid 10, tank respectively between body 10
Lid circular hole is tightly connected；Form annular seal space 12 between soft sealing film 11 and support 8, in this annular seal space 12, fill pure water；Can body 1
Bottom is provided with spiral type electric heating tube 14, and can body 1 inwall of electric heating tube 14 top is fixed with the spray towards obliquely downward to injection
Mouth 13, the can body bottom of electric heating tube 14 lower section is fixed with pump mouth 20, is provided with by pump mouth 20 with nozzle 13 even outside can body
The pipeline 17 connecing, pipeline 17 is provided with water pump 16.Material is extracted out by available water pump from can body bottom, and sprays from nozzle,
On the one hand improve mixing effect, another convenience can improve heating uniformity.
As shown in figure 1, the air inlet that the reactor of this example also has gas-heating apparatus 24 and inserts can body from bottom
Pipe 21, air inlet pipe 21 is connected with the outlet side of gas-heating apparatus 24, and the inlet end of gas-heating apparatus 24 passes through pipeline 23 even
Connect noble gas source, the spiral type aeration tube 22(that air inlet pipe 21 end of insertion can body 1 is connected and installed in can body is shown in figure
2), spiral type aeration tube 22 is located at below electric heating tube 14.
This reactor one side utilizes air inlet pipe to can body delivered inside through the noble gases heating, can be rapidly by heat
Amount passes to the material in can body, realizes the purpose to material heating, and the gas that aeration tube sprays simultaneously moves upwards, contributes to
Material is produced convection current, improves the efficiency of heating surface of electric heating tube；On the other hand, this equipment can utilize water pump by material from can body bottom
Portion extracts out, and sprays from nozzle, can improve heating uniformity while improving mixing effect.
As shown in figure 3, in this example, the injection direction c of nozzle 13 is contrary with stirring rotational axis direction a.In this example, stirring paddle
In addition to being revolved round the sun, also carry out autobiography, in figure, b is stirring paddle rotation rotation direction.In figure, 1 is can body.
In addition to the implementation, the present invention can also have other embodiment.All employing equivalents or equivalent transformation shape
The technical scheme becoming, all falls within the protection domain of application claims.
Claims (1)
1. a kind of reactor, composition includes can body, cover, stirring motor, shaft, stirring paddle, and described can body is provided with and feeds intake
Mouthful, discharging opening it is characterised in that: described cover central authorities open up circular hole, and circular hole is fixedly arranged above support, are provided with described support
Sealed spherical bearing, the spheroid of described sealed spherical bearing connects shaft, and the bearing housing of sealed spherical bearing and support are fixed,
It is fixed with soft sealing film between described circular hole and spheroid, between described soft sealing film and support, form annular seal space, this sealing
Intracavity fills pure water；Described can body bottom is provided with electric heating tube, and the can body inwall above described electric heating tube is fixed with towards oblique
The nozzle of lower direction injection, the can body bottom below described electric heating tube is fixed with pump mouth, is provided with and will take out outside described can body
The pipeline that the mouth of a river is connected with nozzle, pipeline is provided with water pump；Reactor also includes gas-heating apparatus and inserts tank from bottom
A piece air inlet pipe of body, described air inlet pipe is connected with the outlet side of gas-heating apparatus, the inlet end of described gas-heating apparatus
Noble gas source is connected by pipeline, the air inlet tube end of insertion can body is connected and installed in the spiral type aeration tube in can body,
Described spiral type aeration tube is located at below electric heating tube, described cover is provided with exhaustor, equipped with pressure release on described exhaustor
Valve；Thermometer in insertion can body is provided with described cover；Ringwise, flange is passed through in interior outside to described soft sealing film respectively
It is tightly connected with spheroid, cover circular hole；Described cover is bonded with the seam of can body；The injection direction of described nozzle with stir
Mix rotational axis direction contrary.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510325781.6A CN104984706B (en) | 2014-04-09 | 2014-04-09 | Reaction still |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510325781.6A CN104984706B (en) | 2014-04-09 | 2014-04-09 | Reaction still |
| CN201410139088.5A CN103933918B (en) | 2014-04-09 | 2014-04-09 | A kind of reactor |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410139088.5A Division CN103933918B (en) | 2014-04-09 | 2014-04-09 | A kind of reactor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104984706A CN104984706A (en) | 2015-10-21 |
| CN104984706B true CN104984706B (en) | 2017-01-18 |
Family
ID=51181950
Family Applications (4)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510325648.0A Expired - Fee Related CN104984705B (en) | 2014-04-09 | 2014-04-09 | A kind of sealed stirrer |
| CN201510325781.6A Active CN104984706B (en) | 2014-04-09 | 2014-04-09 | Reaction still |
| CN201410139088.5A Active CN103933918B (en) | 2014-04-09 | 2014-04-09 | A kind of reactor |
| CN201510325965.2A Active CN104888683B (en) | 2014-04-09 | 2014-04-09 | A kind of reactor with mechanical agitation structure |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510325648.0A Expired - Fee Related CN104984705B (en) | 2014-04-09 | 2014-04-09 | A kind of sealed stirrer |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410139088.5A Active CN103933918B (en) | 2014-04-09 | 2014-04-09 | A kind of reactor |
| CN201510325965.2A Active CN104888683B (en) | 2014-04-09 | 2014-04-09 | A kind of reactor with mechanical agitation structure |
Country Status (1)
| Country | Link |
|---|---|
| CN (4) | CN104984705B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113573805A (en) * | 2019-03-20 | 2021-10-29 | 株式会社钟化 | Reaction device |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104607121A (en) * | 2015-01-22 | 2015-05-13 | 宜兴市阳洋塑料助剂有限公司 | Esterification reaction device for preparing plasticizers |
| CN104923094A (en) * | 2015-05-29 | 2015-09-23 | 安徽育安实验室装备有限公司 | Solution blending device |
| CN105381775A (en) * | 2015-12-16 | 2016-03-09 | 吴伟峰 | Chemical reactor |
| CN105833757A (en) * | 2016-04-29 | 2016-08-10 | 芜湖杨燕制药有限公司 | Medicine liquid dosing tank |
| CN106955620A (en) * | 2017-04-21 | 2017-07-18 | 四川纳诺科技有限公司 | The agitating device of nano material quality can be improved |
| CN108579596A (en) * | 2018-05-18 | 2018-09-28 | 苏州市金翔钛设备有限公司 | A kind of liquid material mixing apparatus |
| CN116716168B (en) * | 2023-06-14 | 2024-02-09 | 西安工程大学 | Stable microbial inoculum apparatus for producing |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19643165A1 (en) * | 1995-07-10 | 1998-04-23 | Vincent Simon Ellis | Process for performing equilibrium reactions |
| CN2274525Y (en) * | 1996-10-28 | 1998-02-18 | 李彩琴 | Hot air distributor |
| CN101362070A (en) * | 2007-08-09 | 2009-02-11 | 宏大化纤技术装备有限公司 | Reaction device with outer circulation device and method for controlling the reaction process |
| CN201308832Y (en) * | 2008-10-22 | 2009-09-16 | 宁夏建筑材料研究院 | Gas-liquid direct heat exchanging type gypsum normal pressure reaction vessel |
| CN101844048B (en) * | 2010-03-08 | 2013-06-12 | 曾沂水 | Static seal stirrer |
| CN202570171U (en) * | 2012-06-10 | 2012-12-05 | 刘方旭 | Double-layer warming air-adding stirring reaction kettle |
| CN203123964U (en) * | 2012-12-28 | 2013-08-14 | 珠海华大浩宏化工有限公司 | Reaction device for preparing printing and dyeing auxiliary |
| CN103111251B (en) * | 2013-02-20 | 2015-05-27 | 安徽天意环保科技有限公司 | Waste acid utilization device of acidification kettle |
| CN203790941U (en) * | 2014-04-09 | 2014-08-27 | 陆曹生 | Reaction kettle |
-
2014
- 2014-04-09 CN CN201510325648.0A patent/CN104984705B/en not_active Expired - Fee Related
- 2014-04-09 CN CN201510325781.6A patent/CN104984706B/en active Active
- 2014-04-09 CN CN201410139088.5A patent/CN103933918B/en active Active
- 2014-04-09 CN CN201510325965.2A patent/CN104888683B/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113573805A (en) * | 2019-03-20 | 2021-10-29 | 株式会社钟化 | Reaction device |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104984705B (en) | 2016-09-14 |
| CN103933918A (en) | 2014-07-23 |
| CN104984705A (en) | 2015-10-21 |
| CN104888683A (en) | 2015-09-09 |
| CN104888683B (en) | 2016-08-31 |
| CN103933918B (en) | 2015-08-05 |
| CN104984706A (en) | 2015-10-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Lin Guihua Inventor before: Lu Caosheng |
|
| COR | Change of bibliographic data | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20161018 Address after: 362100 Fujian city of Quanzhou Province Taiwan investment zone Dong Yuan Zhen Dong Yuan Cun East Road Applicant after: Quanzhou Taiwanese Investment Zone Shang Liang Building Decoration Co., Ltd. Address before: 226004 Jiangsu Province, Nantong City Chongchuan District Yuelong Road No. 179 3 floor East Applicant before: Lu Caosheng |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Qiu Xianhu Inventor before: Lin Guihua |
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| TR01 | Transfer of patent right |
Effective date of registration: 20170721 Address after: 519000 workshop No. 4, road three, village 2, Toyama Industrial Zone, Guangdong, Zhuhai Patentee after: Zhuhai new materials Co. Ltd. Address before: 362100 Fujian city of Quanzhou Province Taiwan investment zone Dong Yuan Zhen Dong Yuan Cun East Road Patentee before: Quanzhou Taiwanese Investment Zone Shang Liang Building Decoration Co., Ltd. |
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| TR01 | Transfer of patent right |