CN104975307A - Monolithic vinyl-furan resin concrete electrolytic cell and manufacturing method thereof - Google Patents
Monolithic vinyl-furan resin concrete electrolytic cell and manufacturing method thereof Download PDFInfo
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- CN104975307A CN104975307A CN201510414386.5A CN201510414386A CN104975307A CN 104975307 A CN104975307 A CN 104975307A CN 201510414386 A CN201510414386 A CN 201510414386A CN 104975307 A CN104975307 A CN 104975307A
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Abstract
The invention discloses a monolithic vinyl-furan resin concrete electrolytic cell and a manufacturing method thereof, and particularly relates to a monolithic resin concrete-covered anticorrosion fiber reinforced plastic electrolytic cell and a manufacturing method thereof. The electrolytic cell is composed of anticorrosion fiber reinforced plastic protection layers and a furan resin concrete structure layer. The anticorrosion fiber reinforced plastic protection layers cover the inner surface and the outer surface of the furan resin concrete structure layer. The anticorrosion fiber reinforced plastic protection layers and the furan resin concrete structure layer are closely bound. The electrolytic cell has the advantages of low cost of furan resin concrete and good durability of a vinyl electrolytic cell.
Description
Technical field
The present invention relates to industrial equipments manufacture technology field, particularly non-ferrous metal industry electrolysis, electrodeposition process equipment manufacturing technical field, specifically refer to that a kind of overall resin concrete covers Anti-corrosion glass steel electrolyzer and preparation method thereof.
Background technology
Electrolyzer experienced by conventional composite electrolyzer and two stages of traditional integral electrolyzer.Conventional composite electrolyzer is made up of preservative coat package structure layer, and the preservative coat on surface mostly is the materials such as glass reinforced plastic, soft plastics, PE, and structural sheet is inside cement concrete.This type of cell construction layer is not corrosion-resistant, once preservative coat is destroyed, cause structural sheet to be easily corroded, work-ing life is short.Traditional integral electrolyzer mostly is overall grouan electrolyzer, overall water glass electrolyzer, whole glass steel electrolyzer, overall polypropylene electrolyzer, overall polyethylene electrolyzer, and wherein whole glass steel electrolyzer use range is the widest.This kind of overall electrolytic cell body poor rigidity, glass reinforced plastic is easily aging, yielding in use procedure, cracking, seepage, and after cell body seepage, the electrolytic solution conduction of crystallization, easily punctures adjacent cell body, uses more serious more for a long time.
Integral resin concrete electrolytic tank is the development trend of hydrometallurgy equipment.This kind of integral resin concrete electrolytic tank is generally overall vinyl ester resin concret electrolytic bath and overall furan resin concrete electrolyzer in the market.Integral resin concrete electrolytic tank adopts corrosion resistant resin concrete to be that material makes cell body, makes cell body entirety all corrosion-resistant, substantially increases the corrosion resistance nature of electrolyzer.The overall vinyl ester resin concret electrolytic bath had also increases one deck vinyl ester glass reinforced plastic protective layer on cell body surface, with the impermeability of the erosion resistibility and whole cell body that strengthen cell body surface.This kind of overall Vinylite concret electrolytic bath life-span covering vinyl glass reinforced plastic protective layer is longer, but cost is high, and equipment investment is large, is unfavorable for popularizing.
Increasingly mature along with coloured wet process smelting technique, domestic electrolysis industry starts to high benefit low cost future development, therefore inexpensive furan resin concrete is utilized, development meets manufacturing technique requirent, product performance are close, and working life, the long and integral resin concrete electrolytic tank of relative inexpensiveness became the active demand of industry.
Summary of the invention
The object of the invention is to overcome above-mentioned prior art and economic shortcoming, a kind of overall vinyl-furan resin concrete electrolyzer and preparation method thereof is provided.
To achieve these goals, the technical scheme that the present invention takes is:
A kind of overall vinyl-furan resin concrete electrolyzer; it is characterized in that: be made up of Anti-corrosion glass steel protective layer and furan resin concrete structural sheet; Anti-corrosion glass steel protective layer is wrapped in the inside and outside surface of furan resin concrete structural sheet, mutual tight bond between Anti-corrosion glass steel protective layer and furan resin concrete structural sheet.
A kind of overall vinyl-furan resin concrete electrolyzer, be further characterized in that: described furan resin concrete structural sheet, be jointly built by the furan resin concrete material prepared and glass-fiber reinforcement rack to form, glass-fiber reinforcement rack is positioned at the middle part of furan resin concrete structural sheet; Described furan resin concrete, be made up of the material of following weight parts: Vinylite 5 ~ 12 parts, 0.1 ~ 0.24 part, solidifying agent, promotor 0.5 ~ 1.2 part, defoamer 0.05 ~ 0.24 part, furane resin liquid 4 ~ 8 parts, 40 ~ 60 order silica powders 9 ~ 17 parts, 10 ~ 40 order quartz sands 6 ~ 12 parts, 5 ~ 15 millimeters of quartzites 17 ~ 33 parts.
A kind of overall vinyl-furan resin concrete electrolyzer, is further characterized in that: described solidifying agent is methylethyl ketone peroxide or benzoyl peroxide acetyl, and described promotor is cobalt naphthenate or cobalt iso-octoate, and described defoamer is aerosil.
A kind of overall vinyl-furan resin concrete electrolyzer, be further characterized in that: described glass-fiber reinforcement rack, formed by the glass-fiber reinforcement colligation of diameter 6 ~ 12 millimeters, the sizing grid of colligation is 100 millimeters × 100 millimeters to 500 millimeters × 500 millimeters.
A kind of overall vinyl-furan resin concrete electrolyzer, be further characterized in that: described Anti-corrosion glass steel protective layer, successively flood glass-fiber-fabric and glass chopped strand mats curing molding by Vinylite, its thickness is 1.5 ~ 2.5 millimeters.
Above-mentioned overall vinyl-furan resin concrete electrolyzer making method provided by the invention, comprises following processing step:
A. polished finish is carried out to exterior mold surface in steel, until form smooth surface; B. one deck paraffin release agent is smeared at polished die surface; C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed; D. the surperficial felt flooded through Vinylite in above-mentioned surperficial stickers lining, shortly cut felt and glass-fiber-fabric, treat its completion of cure, form Anti-corrosion glass steel protective layer; E. according to cell body size and design requirements nylon cable tie colligation glass-fiber reinforcement, glass-fiber reinforcement rack is formed; F. assembled fastening mould, be inverted, and in mould placing glass bar frame; G. furan resin concrete material is prepared, uniform mixing; H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate; I. maintenance 24 ~ 48 hours at ambient temperature; J. remove mould, continue maintenance 7 ~ 14 days; K. check and repair the local defect of cell surface.
embodiment.
embodiment 1
Overall vinyl-furan resin concrete electrolyzer is obtained through following steps
A. polished finish is carried out to exterior mold surface in steel, until form smooth surface;
B. one deck paraffin release agent is smeared at polished die surface;
C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed;
D. the layer of surface felt flooded through Vinylite in above-mentioned surperficial stickers lining, one deck is short cuts felt and two-layer 0.2 mm thick glass-fiber-fabric, treats its completion of cure, forms the Anti-corrosion glass steel protective layer of 1.5 mm thick;
E. use the glass-fiber reinforcement of nylon cable tie colligation diameter 6mm, form glass-fiber reinforcement rack, the sizing grid of colligation is 100 millimeters × 100 millimeters;
F. assembled fastening mould, be inverted, and in mould placing glass bar frame;
G. according to following part by weight preparation furan resin concrete material, uniform mixing: Vinylite 5 parts, methylethyl ketone peroxide 0.1 part, cobalt naphthenate 0.5 part, aerosil 0.05 part, furane resin liquid 4 parts, 40-60 order silica powder 17 parts, 10-40 order quartz sand 6 parts, 5-15 millimeter quartzite 33 parts;
H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate;
I. maintenance 24 hours at ambient temperature;
J. remove mould, continue maintenance 7 days;
K. check and repair the local defect of cell surface.
embodiment 2
Overall vinyl-furan resin concrete electrolyzer is obtained through following steps
A. polished finish is carried out to exterior mold surface in steel, until form smooth surface;
B. one deck paraffin release agent is smeared at polished die surface;
C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed;
D. the layer of surface felt flooded through Vinylite in above-mentioned surperficial stickers lining, one deck is short cuts felt and two-layer 0.2 mm thick glass-fiber-fabric, treats its completion of cure, forms the Anti-corrosion glass steel protective layer of 1.5 mm thick;
E. use the glass-fiber reinforcement of nylon cable tie colligation diameter 6mm, form glass-fiber reinforcement rack, the sizing grid of colligation is 100 millimeters × 100 millimeters;
F. assembled fastening mould, be inverted, and in mould placing glass bar frame;
G. according to following part by weight preparation furan resin concrete material, uniform mixing: Vinylite 6 parts, methylethyl ketone peroxide 0.14 part, cobalt iso-octoate 0.5 part, aerosil 0.05 part, furane resin liquid 5 parts, 40-60 order silica powder 15 parts, 10-40 order quartz sand 7 parts, 5-15 millimeter quartzite 30 parts;
H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate;
I. maintenance 24 hours at ambient temperature;
J. remove mould, continue maintenance 7 days;
K. check and repair the local defect of cell surface.
embodiment 3
Overall vinyl-furan resin concrete electrolyzer is obtained through following steps
A. polished finish is carried out to exterior mold surface in steel, until form smooth surface;
B. one deck paraffin release agent is smeared at polished die surface;
C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed;
D. the layer of surface felt flooded through Vinylite in above-mentioned surperficial stickers lining, one deck is short cuts felt and two-layer 0.2 mm thick glass-fiber-fabric, treats its completion of cure, forms the Anti-corrosion glass steel protective layer of 1.5 mm thick;
E. use the glass-fiber reinforcement of nylon cable tie colligation diameter 9mm, form glass-fiber reinforcement rack, the sizing grid of colligation is 100 millimeters × 100 millimeters;
F. assembled fastening mould, be inverted, and in mould placing glass bar frame;
G. according to following part by weight preparation furan resin concrete material, uniform mixing: Vinylite 7 parts, methylethyl ketone peroxide 0.17 part, cobalt naphthenate 0.8 part, aerosil 0.05 part, furane resin liquid 6 parts, 40-60 order silica powder 13 parts, 10-40 order quartz sand 8 parts, 5-15 millimeter quartzite 27 parts;
H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate;
I. maintenance 24 hours at ambient temperature;
J. remove mould, continue maintenance 7 days;
K. check and repair the local defect of cell surface.
embodiment 4
Overall vinyl-furan resin concrete electrolyzer is obtained through following steps
A. polished finish is carried out to exterior mold surface in steel, until form smooth surface;
B. one deck paraffin release agent is smeared at polished die surface;
C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed;
D. the layer of surface felt flooded through Vinylite in above-mentioned surperficial stickers lining, two-layerly shortly cut felt and two-layer 0.2 mm thick glass-fiber-fabric, treat its completion of cure, form the Anti-corrosion glass steel protective layer of 2.0 mm thick;
E. use the glass-fiber reinforcement of nylon cable tie colligation diameter 9mm, form glass-fiber reinforcement rack, the sizing grid of colligation is 300 millimeters × 300 millimeters;
F. assembled fastening mould, be inverted, and in mould placing glass bar frame;
G. according to following part by weight preparation furan resin concrete material, uniform mixing: Vinylite 8 parts, methylethyl ketone peroxide 0.20 part, cobalt iso-octoate 0.8 part, aerosil 0.1 part, furane resin liquid 7 parts, 40-60 order silica powder 11 parts, 10-40 order quartz sand 9 parts, 5-15 millimeter quartzite 24 parts;
H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate;
I. maintenance 24 hours at ambient temperature;
J. remove mould, continue maintenance 10 days;
K. check and repair the local defect of cell surface.
embodiment 5
Overall vinyl-furan resin concrete electrolyzer is obtained through following steps
A. polished finish is carried out to exterior mold surface in steel, until form smooth surface;
B. one deck paraffin release agent is smeared at polished die surface;
C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed;
D. the layer of surface felt flooded through Vinylite in above-mentioned surperficial stickers lining, two-layerly shortly cut felt and two-layer 0.2 mm thick glass-fiber-fabric, treat its completion of cure, form the Anti-corrosion glass steel protective layer of 2.0 mm thick;
E. use the glass-fiber reinforcement of nylon cable tie colligation diameter 12mm, form glass-fiber reinforcement rack, the sizing grid of colligation is 300 millimeters × 300 millimeters;
F. assembled fastening mould, be inverted, and in mould placing glass bar frame;
G. according to following part by weight preparation furan resin concrete material, uniform mixing: Vinylite 9 parts, methylethyl ketone peroxide 0.24 part, cobalt naphthenate 1.0 parts, aerosil 0.1 part, furane resin liquid 8 parts, 40-60 order silica powder 9 parts, 10-40 order quartz sand 10 parts, 5-15 millimeter quartzite 21 parts;
H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate;
I. maintenance 24 hours at ambient temperature;
J. remove mould, continue maintenance 10 days;
K. check and repair the local defect of cell surface.
embodiment 6
Overall vinyl-furan resin concrete electrolyzer is obtained through following steps
A. polished finish is carried out to exterior mold surface in steel, until form smooth surface;
B. one deck paraffin release agent is smeared at polished die surface;
C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed;
D. the layer of surface felt flooded through Vinylite in above-mentioned surperficial stickers lining, two-layerly shortly cut felt and two-layer 0.2 mm thick glass-fiber-fabric, treat its completion of cure, form the Anti-corrosion glass steel protective layer of 2.0 mm thick;
E. use the glass-fiber reinforcement of nylon cable tie colligation diameter 12mm, form glass-fiber reinforcement rack, the sizing grid of colligation is 300 millimeters × 300 millimeters;
F. assembled fastening mould, be inverted, and in mould placing glass bar frame;
G. according to following part by weight preparation furan resin concrete material, uniform mixing: Vinylite 10 parts, 0.1 part, benzoyl peroxide acetyl, cobalt iso-octoate 1.0 parts, aerosil 0.1 part, furane resin liquid 4 parts, 40-60 order silica powder 17 parts, 10-40 order quartz sand 11 parts, 5-15 millimeter quartzite 18 parts;
H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate;
I. maintenance 48 hours at ambient temperature;
J. remove mould, continue maintenance 10 days;
K. check and repair the local defect of cell surface.
embodiment 7
Overall vinyl-furan resin concrete electrolyzer is obtained through following steps
A. polished finish is carried out to exterior mold surface in steel, until form smooth surface;
B. one deck paraffin release agent is smeared at polished die surface;
C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed;
D. the two layers of surface felt flooded through Vinylite in above-mentioned surperficial stickers lining, two-layerly shortly cut felt and two-layer 0.2 mm thick glass-fiber-fabric, treat its completion of cure, form the Anti-corrosion glass steel protective layer of 2.5 mm thick;
E. use the glass-fiber reinforcement of nylon cable tie colligation diameter 6mm, form glass-fiber reinforcement rack, the sizing grid of colligation is 500 millimeters × 500 millimeters;
F. assembled fastening mould, be inverted, and in mould placing glass bar frame;
G. according to following part by weight preparation furan resin concrete material, uniform mixing: Vinylite 11 parts, 0.15 part, benzoyl peroxide acetyl, cobalt naphthenate 1.2 parts, aerosil 0.2 part, furane resin liquid 5 parts, 40-60 order silica powder 15 parts, 10-40 order quartz sand 12 parts, 5-15 millimeter quartzite 17 parts;
H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate;
I. maintenance 48 hours at ambient temperature;
J. remove mould, continue maintenance 14 days;
K. check and repair the local defect of cell surface.
embodiment 8
Overall vinyl-furan resin concrete electrolyzer is obtained through following steps
A. polished finish is carried out to exterior mold surface in steel, until form smooth surface;
B. one deck paraffin release agent is smeared at polished die surface;
C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed;
D. the two layers of surface felt flooded through Vinylite in above-mentioned surperficial stickers lining, two-layerly shortly cut felt and two-layer 0.2 mm thick glass-fiber-fabric, treat its completion of cure, form the Anti-corrosion glass steel protective layer of 2.5 mm thick;
E. use the glass-fiber reinforcement of nylon cable tie colligation diameter 9mm, form glass-fiber reinforcement rack, the sizing grid of colligation is 500 millimeters × 500 millimeters;
F. assembled fastening mould, be inverted, and in mould placing glass bar frame;
G. according to following part by weight preparation furan resin concrete material, uniform mixing: Vinylite 12 parts, 0.20 part, benzoyl peroxide acetyl, cobalt iso-octoate 1.2 parts, aerosil 0.2 part, furane resin liquid 6 parts, 40-60 order silica powder 13 parts, 10-40 order quartz sand 6 parts, 5-15 millimeter quartzite 20 parts;
H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate;
I. maintenance 48 hours at ambient temperature;
J. remove mould, continue maintenance 14 days;
K. check and repair the local defect of cell surface.
embodiment 9
Overall vinyl-furan resin concrete electrolyzer is obtained through following steps
A. polished finish is carried out to exterior mold surface in steel, until form smooth surface;
B. one deck paraffin release agent is smeared at polished die surface;
C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed;
D. the two layers of surface felt flooded through Vinylite in above-mentioned surperficial stickers lining, two-layerly shortly cut felt and two-layer 0.2 mm thick glass-fiber-fabric, treat its completion of cure, form the Anti-corrosion glass steel protective layer of 2.5 mm thick;
E. use the glass-fiber reinforcement of nylon cable tie colligation diameter 12mm, form glass-fiber reinforcement rack, the sizing grid of colligation is 500 millimeters × 500 millimeters;
F. assembled fastening mould, be inverted, and in mould placing glass bar frame;
G. according to following part by weight preparation furan resin concrete material, uniform mixing: Vinylite 5 parts, 0.24 part, benzoyl peroxide acetyl, cobalt naphthenate 1.2 parts, aerosil 0.24 part, furane resin liquid 7 parts, 40-60 order silica powder 11 parts, 10-40 order quartz sand 7 parts, 5-15 millimeter quartzite 25 parts;
H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate;
I. maintenance 48 hours at ambient temperature;
J. remove mould, continue maintenance 14 days;
K. check and repair the local defect of cell surface.
Claims (7)
1. overall vinyl-furan resin concrete electrolyzer; it is characterized in that: be made up of Anti-corrosion glass steel protective layer and furan resin concrete structural sheet; Anti-corrosion glass steel protective layer is wrapped in the inside and outside surface of furan resin concrete structural sheet, mutual tight bond between Anti-corrosion glass steel protective layer and furan resin concrete structural sheet.
2. a kind of overall vinyl-furan resin concrete electrolyzer as claimed in claim 1, be further characterized in that: described furan resin concrete structural sheet, be jointly built by the furan resin concrete material prepared and glass-fiber reinforcement rack to form, glass-fiber reinforcement rack is positioned at the middle part of furan resin concrete structural sheet.
3. furan resin concrete material as claimed in claim 2, be made up of the material of following weight parts: Vinylite 5 ~ 12 parts, 0.1 ~ 0.24 part, solidifying agent, promotor 0.5 ~ 1.2 part, defoamer 0.05 ~ 0.24 part, furane resin liquid 4 ~ 8 parts, 40 ~ 60 order silica powders 9 ~ 17 parts, 10 ~ 40 order quartz sands 6 ~ 12 parts, 5 ~ 15 millimeters of quartzites 17 ~ 33 parts.
4. furan resin concrete material as claimed in claim 3, is further characterized in that: described solidifying agent is methylethyl ketone peroxide or benzoyl peroxide acetyl, and described promotor is cobalt naphthenate or cobalt iso-octoate, and described defoamer is aerosil.
5. a kind of overall vinyl-furan resin concrete electrolyzer as claimed in claim 2, be further characterized in that: described glass-fiber reinforcement rack, formed by the glass-fiber reinforcement colligation of diameter 6 ~ 12 millimeters, the sizing grid of colligation is 100 millimeters × 100 millimeters to 500 millimeters × 500 millimeters.
6. a kind of overall vinyl-furan resin concrete electrolyzer as claimed in claim 1; be further characterized in that: described Anti-corrosion glass steel protective layer; successively flood glass-fiber-fabric and glass chopped strand mats curing molding by Vinylite, its thickness is 1.5 ~ 2.5 millimeters.
7. a making method for overall vinyl-furan resin concrete electrolyzer, is characterized in that, the method comprises following processing step: a. carries out polished finish to exterior mold surface in steel, until form smooth surface; B. one deck paraffin release agent is smeared at polished die surface; C. at interior exterior mold surface brushing one deck Vinylite equably, gel coat is formed; D. the surperficial felt flooded through Vinylite in above-mentioned surperficial stickers lining, shortly cut felt and glass-fiber-fabric, treat its completion of cure, form Anti-corrosion glass steel protective layer; E. according to cell body size and design requirements nylon cable tie colligation glass-fiber reinforcement, glass-fiber reinforcement rack is formed; F. assembled fastening mould, be inverted, and in mould placing glass bar frame; G. furan resin concrete material is prepared, uniform mixing; H. in inverted mould, build the furan resin concrete material prepared, and fully vibrate; I. maintenance 24 ~ 48 hours at ambient temperature; J. remove mould, continue maintenance 7 ~ 14 days; K. check and repair the local defect of cell surface.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510414386.5A CN104975307A (en) | 2015-07-15 | 2015-07-15 | Monolithic vinyl-furan resin concrete electrolytic cell and manufacturing method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510414386.5A CN104975307A (en) | 2015-07-15 | 2015-07-15 | Monolithic vinyl-furan resin concrete electrolytic cell and manufacturing method thereof |
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| CN201510414386.5A Pending CN104975307A (en) | 2015-07-15 | 2015-07-15 | Monolithic vinyl-furan resin concrete electrolytic cell and manufacturing method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109504986A (en) * | 2018-12-11 | 2019-03-22 | 河南菲迪泰环境科技有限公司 | A kind of integrated poured vinylite electrolytic cell and preparation method thereof |
| CN110436821A (en) * | 2019-06-27 | 2019-11-12 | 杭州三耐环保科技股份有限公司 | A kind of novel defecator and preparation method thereof |
-
2015
- 2015-07-15 CN CN201510414386.5A patent/CN104975307A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109504986A (en) * | 2018-12-11 | 2019-03-22 | 河南菲迪泰环境科技有限公司 | A kind of integrated poured vinylite electrolytic cell and preparation method thereof |
| CN110436821A (en) * | 2019-06-27 | 2019-11-12 | 杭州三耐环保科技股份有限公司 | A kind of novel defecator and preparation method thereof |
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