CN104959094A - Continuous chlorination tower-type reaction kettle - Google Patents
Continuous chlorination tower-type reaction kettle Download PDFInfo
- Publication number
- CN104959094A CN104959094A CN201510396495.9A CN201510396495A CN104959094A CN 104959094 A CN104959094 A CN 104959094A CN 201510396495 A CN201510396495 A CN 201510396495A CN 104959094 A CN104959094 A CN 104959094A
- Authority
- CN
- China
- Prior art keywords
- tower
- joint
- tower joint
- reactor
- tower section
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention relates to a continuous chlorination tower-type reaction kettle. The continuous chlorination tower-type reaction kettle is characterized by comprising a tower kettle, wherein the tower kettle is provided with a first tower section, the first tower section is provided with a second tower section, the second tower section is provided with a third tower section, the third tower section is provided with a fourth tower section, the fourth tower section is provided with a tower top, the tower kettle, the first tower section, the second tower section, the third tower section, the fourth tower section and the tower top are manufactured and formed by adopting a steel-lined glass-lining material, the outer wall is provided with a jacket, the inner wall is provided with a white glaze layer, a chlorine inlet and a liquid material outlet are formed in the bottom of the tower kettle, a chlorine distributor is arranged in the tower kettle, the chlorine distributor is connected with the chlorine inlet, the tower kettle, the first tower section, the second tower section, the third tower section and the fourth tower section are respectively provided with a jacket inlet-outlet and a temperature measuring opening, the first tower section, the second tower section, the third tower section and the fourth tower section are respectively provided with a lighting opening, an LED (light emitting diode) lamp is arranged in each lighting opening, a liquid material inlet and a chlorine outlet are formed in the tower top, the liquid material inlet is connected with a circulating pump, and the other end of the circulating pump is connected with the liquid material outlet.
Description
Technical field
The present invention relates to chlorination reactor, particularly relate to a kind of tower reactor of continuous chlorination.
Background technology
Chlorination reaction is a kind of very common chemical engineering unit operation, is widely used in agricultural chemicals, medicine and dyestuff and intermediate processing.In recent years, along with chlorination technique constantly develops, there is multiple chlorination reactor application technology, as China Patent No. ZL201420577333.6, patent name is " a kind of novel photochlorination apparatus ", comprises condenser, agitating device, light transmission piece, thermometer, power-equipment, on-line period device etc.; Thermometer is separately positioned on the top and bottom of reactor side, the both sides mid portion of reactor is light transmission piece and is tightly connected with reactor, one end of discharge pipe is connected with the bottom of reactor, the other end is connected with one end of the first Matter Transfer pipeline, the other end of the first Matter Transfer pipeline is connected with power-equipment, on-line period device is connected with the second Matter Transfer pipeline, and one end of the second Matter Transfer pipeline is connected with the upper end of reactor, and the other end is connected with power-equipment; Part corresponding with light transmission piece in second Matter Transfer pipeline is also be made up of material identical with light transmission piece.This patent also exists system complex, operation inconvenience, the shortcomings such as leakage point is many, and equipment investment is high.And for example Chinese patent ZL201420545621.3, patent name is " the liquid phase Light chlorimation tank reactor of built-in light source ", comprise reactor top and be respectively arranged with manhole, electric light source sleeve opening, the thermometer wrap mouth of pipe, charging aperture, rise gas port, refluxing opening, pressure tap, technique mouth, mouth for subsequent use, described reactor lower part is respectively arranged with chlorine inlet, discharging opening, the outer wall that described reactor lower part divides is provided with chuck, described thermometer wrap mouth of pipe interpolation enters thermometer boss, electric light source sleeve pipe is inserted in described electric light source sleeve opening, chlorine gas distributor is connect in described discharging opening.This patent structure is simple to operation, but cannot realize continuous prodution operation.
Summary of the invention
The object of the invention is the shortcoming existed to overcome prior art, provide a kind of structure simple, easy to operate, equipment investment is low, and Ta Neitong light is even, energy continuous seepage, the tower reactor of the continuous chlorination of enhancing productivity.
The technical scheme of the tower reactor of continuous chlorination of the present invention is: it is characterized in that comprising tower reactor, tower reactor is arranged the first tower joint, first tower joint is arranged the second tower joint, second tower joint is arranged the 3rd tower joint, 3rd tower joint is arranged the 4th tower joint, 4th tower joint arranges tower top, described tower reactor, first tower joint, second tower joint, 3rd tower joint, 4th tower joint and tower top are that the manufacture of steel lining enamel material is shaping, at its outer wall, chuck is set, its inwall has white glaze layer, chlorine inlet and liquid material outlet are set under described tower reactor, in tower reactor, chlorine gas distributor is set, chlorine gas distributor is connected with chlorine inlet, described tower reactor, first tower joint, second tower joint, 3rd tower joint and the 4th tower joint arrange chuck import and export and temperature-measuring port respectively, the first described tower joint, second tower joint, 3rd tower joint and the 4th tower joint arrange logical light mouth respectively, in logical light mouth, LED is set, described tower top is arranged liquid material import and chlorine gas outlet, liquid material import connects circulating pump, the other end of circulating pump connects liquid material outlet.
The invention discloses a kind of tower reactor of continuous chlorination, main feature is the tower joint of design 4 series connection jacketed, each tower joint is all provided with Tong Guangkou, tower saves, tower reactor, tower top adopts steel lining enamel material to manufacture shaping, its inwall has white glaze layer, during work, by circulating pump, the liquid material import of liquid material from tower top is inputted, chlorine then inputs from the chlorine inlet of tower reactor, the chlorine risen and the liquid material of decline form adverse current, liquid material is fully contacted with chlorine, circulating pump is adopted to make reactor energy continuous prodution, enhance productivity, and on each tower joint, logical light mouth is set, in logical light mouth, LED is set, inner wall of tower scribbles white glaze layer, white glaze layer can be effectively reflective, make Ta Neitong light even, improve reaction efficiency, and whole tower reactor is easy to operate, structure is simple, reduce equipment investment cost.
The tower reactor of continuous chlorination of the present invention, what the first described tower joint, the second tower joint, the 3rd tower joint and the 4th tower saved is evenly equipped with four logical light mouths all around.The position of the logical light mouth of reasonable layout four, can regulate light intensity as required, improves reaction efficiency, makes Light chlorimation more even.The height H of described each tower joint is 1500mm.
Accompanying drawing explanation
Fig. 1 is the structural representation of the tower reactor of continuous chlorination of the present invention;
Fig. 2 is the structural representation of tower reactor;
Fig. 3 is the structural representation of the first tower joint;
Fig. 4 is the structural representation of tower top.
Detailed description of the invention
The present invention relates to a kind of tower reactor of continuous chlorination, as shown in Fig. 1-4, it is characterized in that: comprise tower reactor 1, tower reactor is arranged the first tower joint 2, first tower joint is arranged the second tower joint 3, second tower joint is arranged the 3rd tower joint 4, 3rd tower joint is arranged the 4th tower joint 5, 4th tower joint arranges tower top 6, described tower reactor 1, first tower joint 2, second tower joint 3, 3rd tower joint 4, 4th tower joint 5 and tower top 6 are that the manufacture of steel lining enamel material is shaping, at its outer wall, chuck 11 is set, its inwall has white glaze layer 12, described tower reactor arranges chlorine inlet 13 and liquid material outlet 14 for 1 time, chlorine gas distributor 15 is set in tower reactor, chlorine gas distributor is connected with chlorine inlet, described tower reactor 1, first tower joint 2, second tower joint 3, 3rd tower joint 4 and the 4th tower joint 5 arrange chuck import and export 7 and temperature-measuring port 8 respectively, the first described tower joint 2, second tower joint 3, 3rd tower joint 4 and the 4th tower joint 5 arrange logical light mouth 9 respectively, in logical light mouth, LED is set, described tower top 6 is arranged liquid material import 61 and chlorine gas outlet 62, liquid material import 61 connects circulating pump 63, the other end of circulating pump connects liquid material outlet 14.Main feature is the tower joint of design 4 series connection jacketed 11, each tower joint is all provided with logical light mouth 9, tower saves, tower reactor 1, it is shaping that tower top 6 adopts steel lining enamel material to manufacture, its inwall has white glaze layer 12, during work, by circulating pump 63, the liquid material import 61 of liquid material from tower top 6 is inputted, chlorine then inputs from the chlorine inlet 13 of tower reactor 1, the chlorine risen and the liquid material of decline form adverse current, liquid material is fully contacted with chlorine, circulating pump 63 is adopted to make reactor energy continuous prodution, enhance productivity, and on each tower joint, logical light mouth 9 is set, in logical light mouth, LED is set, inner wall of tower scribbles white glaze layer 12, white glaze layer can be effectively reflective, make Ta Neitong light even, improve reaction efficiency, and whole tower reactor is easy to operate, structure is simple, reduce equipment investment cost.Described first tower joint 2, second tower joint the 3, the 3rd tower joint 4 and the 4th tower joint 5 be evenly equipped with four logical light mouths 9 all around.The position of the logical light mouth 9 of reasonable layout four, can regulate light intensity as required, improves reaction efficiency, makes Light chlorimation more even.The height H of described each tower joint is 1500mm.
Claims (3)
1. the tower reactor of continuous chlorination, it is characterized in that: comprise tower reactor (1), tower reactor is arranged the first tower joint (2), first tower joint arranges the second tower joint (3), second tower joint arranges the 3rd tower joint (4), 3rd tower joint arranges the 4th tower joint (5), 4th tower joint arranges tower top (6), described tower reactor (1), first tower joint (2), second tower joint (3), 3rd tower joint (4), 4th tower joint (5) and tower top (6) for steel lining enamel material manufacture shaping, at its outer wall, chuck (11) is set, its inwall has white glaze layer (12), chlorine inlet (13) and liquid material outlet (14) are set under described tower reactor (1), chlorine gas distributor (15) is set in tower reactor, chlorine gas distributor is connected with chlorine inlet, described tower reactor (1), first tower joint (2), second tower joint (3), 3rd tower joint (4) and the 4th tower joint (5) arrange chuck import and export (7) and temperature-measuring port (8) respectively, the first described tower joint (2), second tower joint (3), 3rd tower joint (4) and the 4th tower joint (5) arrange logical light mouth (9) respectively, in logical light mouth, LED is set, described tower top (6) is arranged liquid material import (61) and chlorine gas outlet (62), liquid material import (61) connects circulating pump (63), the other end of circulating pump connects liquid material outlet (14).
2. the tower reactor of continuous chlorination as claimed in claim 1, is characterized in that: what the first described tower joint (2), the second tower joint (3), the 3rd tower joint (4) and the 4th tower saved (5) is evenly equipped with four logical light mouths (9) all around.
3. the tower reactor of continuous chlorination as claimed in claim 1, is characterized in that: the height H of described each tower joint is 1500mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510396495.9A CN104959094A (en) | 2015-07-08 | 2015-07-08 | Continuous chlorination tower-type reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510396495.9A CN104959094A (en) | 2015-07-08 | 2015-07-08 | Continuous chlorination tower-type reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104959094A true CN104959094A (en) | 2015-10-07 |
Family
ID=54213278
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510396495.9A Pending CN104959094A (en) | 2015-07-08 | 2015-07-08 | Continuous chlorination tower-type reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104959094A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110511110A (en) * | 2019-08-09 | 2019-11-29 | 浙江衢州巨塑化工有限公司 | A kind of 1,1,2- trichloroethanes reactor and its method |
| CN113861028A (en) * | 2021-10-29 | 2021-12-31 | 山西碧洲生物科技股份有限公司 | Process method and device for continuously producing di (trichloromethyl) carbonate |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2151599Y (en) * | 1992-12-18 | 1993-12-29 | 张天安 | Multiple purpose active antenna for household appliances |
| CN204933447U (en) * | 2015-07-08 | 2016-01-06 | 江苏联化科技有限公司 | The tower reactor of continuous chlorination |
-
2015
- 2015-07-08 CN CN201510396495.9A patent/CN104959094A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2151599Y (en) * | 1992-12-18 | 1993-12-29 | 张天安 | Multiple purpose active antenna for household appliances |
| CN204933447U (en) * | 2015-07-08 | 2016-01-06 | 江苏联化科技有限公司 | The tower reactor of continuous chlorination |
Non-Patent Citations (2)
| Title |
|---|
| 曾繁芯: "《化学工艺学概论》", 30 June 2005 * |
| 马振华: "《烷基苯磺酸钠洗衣粉的生产》", 31 July 1980 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110511110A (en) * | 2019-08-09 | 2019-11-29 | 浙江衢州巨塑化工有限公司 | A kind of 1,1,2- trichloroethanes reactor and its method |
| CN110511110B (en) * | 2019-08-09 | 2023-10-20 | 浙江衢州巨塑化工有限公司 | 1, 2-trichloroethane reactor and method thereof |
| CN113861028A (en) * | 2021-10-29 | 2021-12-31 | 山西碧洲生物科技股份有限公司 | Process method and device for continuously producing di (trichloromethyl) carbonate |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104959094A (en) | Continuous chlorination tower-type reaction kettle | |
| CN204933447U (en) | The tower reactor of continuous chlorination | |
| CN204093431U (en) | A kind of tower continuous light chlorination reaction device | |
| CN102847506A (en) | Novel reaction still structure | |
| CN205909718U (en) | Lens monomer raw materials reation kettle is with oily condensing equipment of heat | |
| CN205586983U (en) | Produce production line of many color ring oxygen tree fat | |
| CN209128712U (en) | A kind of flax of interlayer heating boils bleaching device | |
| CN204485849U (en) | A kind of adhesive production system | |
| CN203618725U (en) | High-temperature energy-saving beverage instantaneous sterilizing device | |
| CN204582607U (en) | A kind of extraction equipment | |
| CN203577773U (en) | Insulated water heating kettle convenient to maintain | |
| CN202893353U (en) | Reaction kettle | |
| CN203980999U (en) | The automatic separating device of a kind of lonicerae syrup spraying cooling water-cooled | |
| CN207493705U (en) | A kind of efficient reaction kettle | |
| CN204275935U (en) | A kind of reactor group | |
| CN107356138A (en) | The quick heat exchange Quick cleaning device of chemical industry easy to clean | |
| CN201333401Y (en) | Reaction kettle | |
| CN204841631U (en) | Liquid mixing arrangement | |
| CN205136873U (en) | Stainless steel covers moulds nipple | |
| CN202666846U (en) | Chlorination device | |
| CN103637351A (en) | High-temperature energy-saving instantaneous drink sterilization device and method | |
| CN204522357U (en) | A kind of efficient phenylphenol production equipment | |
| CN216296293U (en) | Ultraviolet light chemical reaction device | |
| CN202315372U (en) | Rectification system device | |
| CN203803485U (en) | Tubular microwave reaction kettle |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20170330 Address after: 224631 Jiangsu Province, Yancheng City chemical industry park. Applicant after: Jiangsu Lianhua Technology Co., Ltd. Applicant after: Lianhua Technology (Yancheng) Co., Ltd. Applicant after: Lianhe Chemical Technology Co., Ltd. Address before: 224631 Jiangsu Province, Yancheng City chemical industry park. Applicant before: Jiangsu Lianhua Technology Co., Ltd. |
|
| TA01 | Transfer of patent application right | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20151007 |
|
| RJ01 | Rejection of invention patent application after publication |