CN104922976B - A kind of technique for Catalyst Production emulsion continuous purification - Google Patents
A kind of technique for Catalyst Production emulsion continuous purification Download PDFInfo
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- CN104922976B CN104922976B CN201510250030.2A CN201510250030A CN104922976B CN 104922976 B CN104922976 B CN 104922976B CN 201510250030 A CN201510250030 A CN 201510250030A CN 104922976 B CN104922976 B CN 104922976B
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Abstract
A kind of new technology for Catalyst Production emulsion continuous purification, combined by tunnel type magnetic quantum demulsification technology, the big system of slurry bed reactor catalyst filtration technique two, this technique achieves filtration, breakdown of emulsion, Liquid liquid Separation, concentration, filtration, Liquid liquid Separation integration realize in same equipment, need not evaporate and just improve breakdown of emulsion efficiency；The assemblies such as filter element uses pottery, metal filter cloth, element kit or metal filter cloth form flat membrane stack, and when filter cake is formed, breakdown of emulsion need not add flocculant, does not change chemical constituent and the character of emulsion, reduces process costs under computer program control；Decreasing equipment operation cost, Fei Chao company uses the filtering type method for demulsifying and purifying of original creation simultaneously；Complete to filter and breakdown of emulsion in an equipment simultaneously, accomplish that, without filter aid dry residue emission, emulsion can recycle simultaneously, solve the problems such as existing technique breakdown of emulsion is thorough, process costs is high.
Description
Technical field
The present invention is used for Catalyst Production emulsion, a kind of new work for Catalyst Production emulsion continuous purification
Skill, relates to bioengineering extraction and separation technology field.
Background technology
Catalyst Production emulsion is with silicone oil etc. as raw material, is refined into stable breast through scientific formula and unique emulsifying process
Liquid, nontoxic, tasteless, soluble in water, chemical stability is good, when emulsion is the milky Miniemulsion of micro-blueing light, weather resisteant
Good, emulsion diluted without layering or floating oil phenomenon, available water arbitrary proportion, obtained variable concentrations more than 1 year stabilization time
Emulsion, keeps stable, and not stratified, not floating oil, emulsifier is few, thus embodies the effect of containing hydrogen silicone oil to greatest extent, can shape
Become stable water proof anti-soil film, with hydroxy-silicone-oil emulsion immixture, water proofing property and the flexibility of fabric can be improved, it may also be used for
Leather, paper, glass, pottery, metal, cement, marble etc. are carried out antifouling, moistureproof, water-proofing treatment etc., and range of application compares
Extensively, and the quality difficulty of Catalyst Production emulsion is stable, and especially demulsification technology is complicated.
The continuous flow upstream ultrasonic dehydration equipment used at present, is the most more advanced emulsion breaking device, low-temperature demulsification with
Liquid liquid Separation, although product quality has promoted but production efficiency and improved little, this equipment exist defective workmanship breakdown of emulsion not thoroughly,
Process time length, floor space are big, power consumption waste, operate the shortcomings such as more complicated, and the present invention reduces, alleviates labour intensity,
Avoid environmental pollution, be the new technology of a set of efficient, energy-conservation, safe and environment-friendly emulsion continuous purification production.
Summary of the invention
The invention aims to overcome above-mentioned weak point, and devise a kind of low energy consumption, demulsification efficiency height, used time
A kind of new technology for Catalyst Production emulsion continuous purification of short, technique, in order to realize foregoing invention purpose, this
Bright innovation point has:
1. use filtering type breakdown of emulsion, filter and realize in same set of process system with Liquid liquid Separation；
2. filter element is assembly, element kit or the flat membrane stacks such as pottery, metal and filter cloth, is formed at filter cake
Front breakdown of emulsion；
3. it is not added with flocculant, does not change chemical constituent and the character of emulsion；
4. or filter aid can be used less；
5. tunnel type magnetic quantum breakdown of emulsion, need not evaporate or burn.
This innovative technology is by tunnel type magnetic quantum demulsification technology, slurry bed reactor catalyst filtration technique two big system knot
Close, it is achieved that filtrations, breakdown of emulsion, Liquid liquid Separation, concentrate, filter, Liquid liquid Separation integration realization in same equipment, need not evaporate
Just improve breakdown of emulsion efficiency；The assemblies such as filter element uses pottery, metal filter cloth, element kit or metal filter cloth composition are flat
Membrane stack, when filter cake is formed, breakdown of emulsion need not add flocculant, does not change chemical constituent and the character of emulsion, in computer program control
Under reduce process costs；Decreasing equipment operation cost, Fei Chao company uses the filtering type method for demulsifying and purifying of original creation simultaneously；
It is to complete to filter and breakdown of emulsion in an equipment simultaneously, accomplishes that, without filter aid dry residue emission, emulsion can recycle simultaneously, solve
The problems such as existing technique breakdown of emulsion of having determined is thorough, process costs is high.
Technical scheme is as follows
A kind of new technology for Catalyst Production emulsion continuous purification, is by tunnel type magnetic quantum breaking device technique system
System and slurry bed reactor catalyst filtration process system composition, it is characterised in that: tunnel type magnetic quantum demulsification system device A
With the perfect adaptation of slurry bed reactor catalyst filtration process unit B, its bag is scraped in tunnel type magnetic quantum demulsification system device A
Cathode quantum generator 6, tunnel type quantum clash into magnetic field 7, the big core of anode quantum generator 8 three；The tunnel type quantity of magnetism
Sub-demulsification system device A carries out breakdown of emulsion process to material；Slurry bed reactor catalyst filtration process unit B is to materials abstraction liquid
Carry out point slipping process and shunting storage extraction concentrate；The extractant of tunnel type magnetic quantum demulsification system device A, was extracting
Journey clashes into magnetic field 7 to tunnel type quantum and provides extraction solution, at the work of cathode quantum generator 6 with anode quantum generator 8
Under with, extraction solution breakdown of emulsion in tunnel type quantum clashes into magnetic field 7, enable in particular to realize breakdown of emulsion time before filter cake is formed.
Described tunnel type magnetic quantum demulsification system device A need not with flocculant, material solution entrance tunnel type quantum
After clashing into magnetic field 7, just sent instruction by data processor 14；Cathode quantum generator 6, anode quantum generator 8 just start,
Tunnel type quantum clashes into produce in magnetic field 7 and rotates in magnetic wave, accompanying drawing 7, and negative and positive the two poles of the earth are clashed into quantum and launched and realize filtration cycle and break
Breast.
Described material remains static, in suction and conveying inside the molten batch can 1 of tunnel type magnetic quantum demulsification system device A
Under the sending of pump 5, suction effect, material is under pottery separating filter 2, the circulation of partial pressure type container 4 multi-reflow, data processor 14
Control two-way valve 2-2, the open and close of two-way shut-off valve 3-2 according to point breast instrument 3-1 information, make active ingredient in material reach
The purpose of filter breakdown of emulsion, breakdown of emulsion processes can take to circulate continuously the mode of breakdown of emulsion, improves technology utilization rate, decreases and operate into
This, suction and conveying pump 5 has suction, the dual-use function that send emulsion is convertible.
In described slurry bed reactor catalyst filtration process unit B, B-1, B-2 have the effect that can shunt, and use and become silted up
In slurry bed reactor catalyst filtration process unit B, B-1 is connected with tunnel type magnetic quantum demulsification system device A, simplifies system
Equipment, has saved production installing space.(with reference to accompanying drawing 1)
Core " the collection that in described slurry bed reactor catalyst filtration process unit B, B-1 Main Function is in system
Bundle formula filter ", in accompanying drawing 2, B is under this Fei Chao group company: the patent of Feature-Tec's design
Product, is the necessary requirement forming continuous purification new technology of the present invention, the patent No.: 2015200378138.
It is this group's skill that tunnel type quantum in described tunnel type magnetic quantum demulsification system device A technique clashes into magnetic field 7
Art personnel's is well-designed, will be applied for a patent by Feature-Tec (Wuxi) Filtering Technology Co., Ltd.: " a kind of tunnel type magnetic quantum breakdown of emulsion
Process system apparatus ", cathode quantum generator 6 is supplied for cooperation unit's customization with anode quantum generator 8, two-way valve 2-2, double
Showing controller 15 buy for market to stop valve 3-2, control valve 13, data processor 14, journey, other annex is enterprise of Fei Chao group
Industry oneself manufactures.
The invention has the beneficial effects as follows
This innovative technology is by tunnel type magnetic quantum demulsification technology, slurry bed reactor catalyst filtration technique two big system knot
Close, it is achieved that filtrations, breakdown of emulsion, Liquid liquid Separation, concentrate, filter, Liquid liquid Separation integration realization in same equipment, need not evaporate
Just improve breakdown of emulsion efficiency；The assemblies such as filter element uses pottery, metal filter cloth, element kit or metal filter cloth composition are flat
Membrane stack, when filter cake is formed, breakdown of emulsion need not add flocculant, does not change chemical constituent and the character of emulsion, in computer program control
Process costs is reduced under system；Decreasing equipment operation cost, Fei Chao company uses the filtering type breakdown of emulsion purification side of original creation simultaneously
Method；It is to complete to filter and breakdown of emulsion in an equipment simultaneously, accomplishes that, without filter aid dry residue emission, emulsion can circulate profit simultaneously
With, solve the problems such as existing technique breakdown of emulsion is thorough, process costs is high.
Accompanying drawing explanation
Fig. 1 is present system schematic diagram；
Fig. 2 is present invention process exploded view；
In Fig. 2, A figure portion markings is understood: it is two-way that 1 molten batch can, 2 pottery separating filters, 2-1 melt breast instrument, 2-2 two-way valve, 3-2
Stop valve, 3-1 divide breast instrument, 3 breakdown of emulsion analyzers, 4 partial pressure type containers, 5 suction and conveying pumps, 6 cathode quantum generators, 7 tunnel type quantum
Clash at magnetic field, 8 anode quantum generators, 9 magnetic filters, 10 batch hoppers, 11 feed hoppers, 12 conveying pipe, 13 control valves, 14 data
Reason device, 15 journeys show controller；B is cluster type filter.
Detailed description of the invention
As shown in Figure 2: whole technique is mainly by tunnel type magnetic quantum breaking device process system, slurry bed reactor
Catalyst filtration process system forms, tunnel type magnetic quantum demulsification system device A and slurry bed reactor catalyst filtration technique
The perfect adaptation of device B, cathode quantum generator 6, tunnel type quantum in tunnel type magnetic quantum demulsification system device A clash into magnetic
Field 7, anode quantum generator 8 are three big cores；Material is carried out at breakdown of emulsion by tunnel type magnetic quantum demulsification system device A
Reason；Materials abstraction liquid is carried out point slipping process and shunting storage extraction concentrating by slurry bed reactor catalyst filtration process unit B
Liquid；Tunnel type magnetic quantum demulsification system device A extractant also clashes into magnetic field 7 offer extraction to tunnel type quantum in extraction process
Taking solution, cathode quantum generator 6 is with under the effect of anode quantum generator 8, and extraction solution clashes into magnetic field 7 at tunnel type quantum
Middle breakdown of emulsion, it is achieved breakdown of emulsion before filter cake is formed, tunnel type magnetic quantum demulsification system device A need not with flocculant, material solution
Enter after tunnel type quantum clashes into magnetic field 7 and just sent instruction by data processor 14；Cathode quantum generator 6, anode quantum are sent out
Raw device 8 just starts, and produces and rotate magnetic wave in tunnel type quantum shock magnetic field 7, and negative and positive the two poles of the earth shock quantum is launched realization and filtered
Circulation breakdown of emulsion.
Material remains static, at suction and conveying pump 5 inside the molten batch can 1 of tunnel type magnetic quantum demulsification system device A
The lower material of effect is under pottery separating filter 2, more than 4 circulation of partial pressure type container, and data processor 14 is according to a point breast instrument 3-1 information
Controlling two-way valve 2-2, two-way shut-off valve 3-2, make active ingredient in material reach to filter the purpose of breakdown of emulsion, breakdown of emulsion processes and can take
Circulate the mode of breakdown of emulsion continuously, improve technology utilization rate, decrease operating cost, slurry bed reactor catalyst filtration technique
In device B B-1, B-2 have can shunting action, use B-1 and tunnel type in slurry bed reactor catalyst filtration process unit B
Magnon demulsification system device A connects, and simplifies system equipment, has saved production installing space.
Embodiment 1:
By slurry bed reactor catalyst filtration process unit B: the material in cluster type filter is entered by carrying pipe 12
Molten batch can 1, suction and conveying pump 5, to send pressure mode by liquid material force feed to pottery separating filter 2, forms liquid material under the control melting breast instrument 2-1
Primary emulsifying, now closing control valve 13；Open two-way valve 2-2, two-way shut-off valve 3-2, by point breast instrument 3-1 by colostrum journey
Degree, allows breakdown of emulsion analyzer 3 measure breakdown of emulsion data and is transferred to data processor 14, and the emulsion measured through breakdown of emulsion analyzer 3 is passed through defeated
Send pipe 12, feed hopper 11, enter tunnel type quantum and clash into magnetic field 7；At cathode quantum generator 6, the work of anode quantum generator 8
Using lower breakdown of emulsion, now suction and conveying pump 5 is converted to inhale breast function, through conveying pipe 12 by breakdown of emulsion liquid circulating reflux to partial pressure type container 4
Last layer, loops back flow point slag in magnetic filter 9.
Embodiment 2:
Being set in journey shows controller 15 according to technological process by programmer, data processor 14 is according to the work set
Skill requirement processes breakdown of emulsion, filtration, sends instruction and opens, closes, breakdown of emulsion liquid circulating reflux to partial pressure type is held through conveying pipe 12
The emulsion of device 4 last layer, after magnetic filter 9 loops back flow point slag, emulsion in magnetic filter 9 circulating reflux at partial pressure type container
Upper strata in 4, lower floor's continuous purification, when data processor 14 sends catalyst production process deficiency, opening controlling valve 13 enters
The backflow of row midway, can add a small amount of filter aid from batch hopper 10 simultaneously, helps to discharge dry slag.
A kind of technique for Catalyst Production emulsion continuous purification of present invention design greatly enhances breakdown of emulsion
Efficiency and effect, reduce production technology cost, compensate for the deficiency of existing similar technique, and concrete system and device will be by flying Chao Ji
Under League flag, company " Feature-Tec (Wuxi) Filtering Technology Co., Ltd. " manufactures and designs, and by patent application separately, and permits to use and this
Case has relevant description to state, novelty of conflicting the most therewith.
Listed above is only the several specific embodiments realizing the present invention, it is clear that the invention is not restricted to above example,
Can also there be many deformation.The institute that those of ordinary skill in the art can directly derive from present disclosure or associate
There is deformation, be all considered as protection scope of the present invention.
Claims (1)
1. for a technique for Catalyst Production emulsion continuous purification, including in tunnel type magnetic quantum demulsification system device (A)
Cathode quantum generator (6), tunnel type quantum clash into magnetic field (7), the big core of anode quantum generator (8) three；Tunnel
Formula magnon demulsification system device (A) carries out breakdown of emulsion process to material；Slurry bed reactor catalyst filtration process unit (B) is right
Materials abstraction liquid carries out fractionation process and shunts storage extraction concentrate；Tunnel type magnetic quantum demulsification system device (A) extracts molten
Agent also clashes into magnetic field (7) offer extraction solution to tunnel type quantum in extraction process, it is characterized in that: at cathode quantum generator
(6) with under the effect of anode quantum generator (8), solution breakdown of emulsion in tunnel type quantum clashes into magnetic field (7) is extracted, it is achieved in filter
Cheese becomes front breakdown of emulsion, and tunnel type magnetic quantum demulsification system device (A) need not with flocculant, material solution entrance tunnel type quantum
Just instruction is sent by data processor (14) after clashing into magnetic field (7)；Cathode quantum generator (6), anode quantum generator (8) are
Startup, produces in tunnel type quantum shock magnetic field (7) and rotates magnetic wave, and the shock quantum transmitting of negative and positive the two poles of the earth realizes filtration cycle and breaks
Breast；Material remains static, at suction and conveying pump (5) in molten batch can (1) inside of tunnel type magnetic quantum demulsification system device (A)
The lower material of effect is under pottery separating filter (2), partial pressure type container (4) repeatedly circulate, and data processor (14) is according to a point breast instrument
(3-1) information controls two-way valve (2-2), two-way shut-off valve (3-2) makes active ingredient in material reach to filter the purpose of breakdown of emulsion, broken
Breast processes can take to circulate continuously the mode of breakdown of emulsion.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510250030.2A CN104922976B (en) | 2015-05-18 | 2015-05-18 | A kind of technique for Catalyst Production emulsion continuous purification |
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| CN201510250030.2A CN104922976B (en) | 2015-05-18 | 2015-05-18 | A kind of technique for Catalyst Production emulsion continuous purification |
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| CN104922976B true CN104922976B (en) | 2016-09-07 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4116829A (en) * | 1974-01-18 | 1978-09-26 | English Clays Lovering Pochin & Company Limited | Magnetic separation, method and apparatus |
| CN101208144A (en) * | 2005-06-06 | 2008-06-25 | 英国石油有限公司 | Method for separating emulsions |
| CN101733045A (en) * | 2008-11-14 | 2010-06-16 | 中国石油化工股份有限公司 | Solid-liquid separation device and solid-liquid separation method for slurry bed reactor |
| CN202173815U (en) * | 2010-12-27 | 2012-03-28 | 重庆工商大学 | Water hammer harmonic emulsion breaker for emulsified oil |
| CN102626568A (en) * | 2012-04-13 | 2012-08-08 | 上海蓝科石化工程技术有限公司 | Product filtering system for three-phase slurry bed reactor |
-
2015
- 2015-05-18 CN CN201510250030.2A patent/CN104922976B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4116829A (en) * | 1974-01-18 | 1978-09-26 | English Clays Lovering Pochin & Company Limited | Magnetic separation, method and apparatus |
| CN101208144A (en) * | 2005-06-06 | 2008-06-25 | 英国石油有限公司 | Method for separating emulsions |
| CN101733045A (en) * | 2008-11-14 | 2010-06-16 | 中国石油化工股份有限公司 | Solid-liquid separation device and solid-liquid separation method for slurry bed reactor |
| CN202173815U (en) * | 2010-12-27 | 2012-03-28 | 重庆工商大学 | Water hammer harmonic emulsion breaker for emulsified oil |
| CN102626568A (en) * | 2012-04-13 | 2012-08-08 | 上海蓝科石化工程技术有限公司 | Product filtering system for three-phase slurry bed reactor |
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| CN104922976A (en) | 2015-09-23 |
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Effective date of registration: 20171018 Address after: 214000 Xishan Economic Development Zone, Jiangsu, Rong Rong Road No. 71, No. Patentee after: Feature-Tec (Wuxi) Filtration Technology Co., Ltd. Address before: 100083 Beijing City, Haidian District Xueyuan Road No. 30, large industrial building 5 storey block B room 05 Patentee before: BEIJING FEATURE ENVIRONMENT ENGINEERING TECHNOLOGY CO., LTD. |