CN104891570A - Liquid phase synthetic Zr<4+> doped bismuth fluoride lithium-ion battery positive electrode material and preparation method thereof - Google Patents
Liquid phase synthetic Zr<4+> doped bismuth fluoride lithium-ion battery positive electrode material and preparation method thereof Download PDFInfo
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- CN104891570A CN104891570A CN201510195223.2A CN201510195223A CN104891570A CN 104891570 A CN104891570 A CN 104891570A CN 201510195223 A CN201510195223 A CN 201510195223A CN 104891570 A CN104891570 A CN 104891570A
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- solution
- bismuth
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- water
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- 229910001416 lithium ion Inorganic materials 0.000 title claims abstract description 25
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 239000007791 liquid phase Substances 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000007774 positive electrode material Substances 0.000 title abstract description 15
- BRCWHGIUHLWZBK-UHFFFAOYSA-K bismuth;trifluoride Chemical compound F[Bi](F)F BRCWHGIUHLWZBK-UHFFFAOYSA-K 0.000 title abstract 6
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 22
- 150000001621 bismuth Chemical class 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 56
- 239000000126 substance Substances 0.000 claims description 32
- 229910052797 bismuth Inorganic materials 0.000 claims description 26
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims description 26
- LDDQLRUQCUTJBB-UHFFFAOYSA-N ammonium fluoride Chemical compound [NH4+].[F-] LDDQLRUQCUTJBB-UHFFFAOYSA-N 0.000 claims description 23
- JHXKRIRFYBPWGE-UHFFFAOYSA-K bismuth chloride Chemical compound Cl[Bi](Cl)Cl JHXKRIRFYBPWGE-UHFFFAOYSA-K 0.000 claims description 17
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 claims description 14
- 238000010907 mechanical stirring Methods 0.000 claims description 14
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 14
- 230000015572 biosynthetic process Effects 0.000 claims description 13
- 238000003786 synthesis reaction Methods 0.000 claims description 13
- 239000010405 anode material Substances 0.000 claims description 9
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 7
- DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical compound [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 claims description 7
- -1 dodecyl dimethyl hydroxypropyl Chemical group 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 7
- 229910017604 nitric acid Inorganic materials 0.000 claims description 7
- 238000005406 washing Methods 0.000 claims description 7
- 238000003860 storage Methods 0.000 claims description 6
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 claims description 5
- CCUWGJDGLACFQT-UHFFFAOYSA-N 2,2,3,3,4,4-hexafluoropentanedioic acid Chemical compound OC(=O)C(F)(F)C(F)(F)C(F)(F)C(O)=O CCUWGJDGLACFQT-UHFFFAOYSA-N 0.000 claims description 4
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims description 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 4
- PIYVNGWKHNMMAU-UHFFFAOYSA-N [O].O Chemical compound [O].O PIYVNGWKHNMMAU-UHFFFAOYSA-N 0.000 claims description 4
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 claims description 4
- ZWBAMYVPMDSJGQ-UHFFFAOYSA-N perfluoroheptanoic acid Chemical compound OC(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F ZWBAMYVPMDSJGQ-UHFFFAOYSA-N 0.000 claims description 4
- 229940079781 sodium cocoyl glutamate Drugs 0.000 claims description 4
- 229940045944 sodium lauroyl glutamate Drugs 0.000 claims description 4
- IWIUXJGIDSGWDN-UQKRIMTDSA-M sodium;(2s)-2-(dodecanoylamino)pentanedioate;hydron Chemical compound [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC(O)=O IWIUXJGIDSGWDN-UQKRIMTDSA-M 0.000 claims description 4
- NLOQZPHAWQDLQW-UHFFFAOYSA-J zirconium(4+);disulfate;tetrahydrate Chemical compound O.O.O.O.[Zr+4].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O NLOQZPHAWQDLQW-UHFFFAOYSA-J 0.000 claims description 4
- JRURZFNGMMYBAO-UHFFFAOYSA-N 2-(dodecylamino)propanoic acid;sodium Chemical compound [Na].CCCCCCCCCCCCNC(C)C(O)=O JRURZFNGMMYBAO-UHFFFAOYSA-N 0.000 claims description 3
- KMLMOVWSQPHQME-UHFFFAOYSA-N 2,2-difluorocyclopropane-1-carboxylic acid Chemical class OC(=O)C1CC1(F)F KMLMOVWSQPHQME-UHFFFAOYSA-N 0.000 claims description 2
- 239000000243 solution Substances 0.000 abstract description 90
- 239000000463 material Substances 0.000 abstract description 20
- 238000000034 method Methods 0.000 abstract description 11
- 238000006243 chemical reaction Methods 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 7
- 150000003839 salts Chemical class 0.000 abstract description 6
- 239000007787 solid Substances 0.000 abstract description 5
- DDFHBQSCUXNBSA-UHFFFAOYSA-N 5-(5-carboxythiophen-2-yl)thiophene-2-carboxylic acid Chemical compound S1C(C(=O)O)=CC=C1C1=CC=C(C(O)=O)S1 DDFHBQSCUXNBSA-UHFFFAOYSA-N 0.000 abstract description 4
- 239000000047 product Substances 0.000 abstract description 4
- 239000007795 chemical reaction product Substances 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 238000007086 side reaction Methods 0.000 abstract description 3
- 239000007788 liquid Substances 0.000 abstract description 2
- 239000002245 particle Substances 0.000 abstract 2
- 239000012266 salt solution Substances 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- BDJYZEWQEALFKK-UHFFFAOYSA-N bismuth;hydrate Chemical compound O.[Bi] BDJYZEWQEALFKK-UHFFFAOYSA-N 0.000 description 8
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 5
- 229910052744 lithium Inorganic materials 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 230000008901 benefit Effects 0.000 description 3
- 230000004087 circulation Effects 0.000 description 3
- 239000011572 manganese Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 239000002671 adjuvant Substances 0.000 description 2
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 description 2
- 239000010941 cobalt Substances 0.000 description 2
- 229910017052 cobalt Inorganic materials 0.000 description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 2
- 238000009831 deintercalation Methods 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000012827 research and development Methods 0.000 description 2
- 230000001988 toxicity Effects 0.000 description 2
- 231100000419 toxicity Toxicity 0.000 description 2
- 230000009466 transformation Effects 0.000 description 2
- 239000002028 Biomass Substances 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 229910012851 LiCoO 2 Inorganic materials 0.000 description 1
- 229910010707 LiFePO 4 Inorganic materials 0.000 description 1
- 229910015645 LiMn Inorganic materials 0.000 description 1
- 229910014689 LiMnO Inorganic materials 0.000 description 1
- 229910013292 LiNiO Inorganic materials 0.000 description 1
- KFDQGLPGKXUTMZ-UHFFFAOYSA-N [Mn].[Co].[Ni] Chemical compound [Mn].[Co].[Ni] KFDQGLPGKXUTMZ-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000010406 cathode material Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- QHGJSLXSVXVKHZ-UHFFFAOYSA-N dilithium;dioxido(dioxo)manganese Chemical compound [Li+].[Li+].[O-][Mn]([O-])(=O)=O QHGJSLXSVXVKHZ-UHFFFAOYSA-N 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 229920000831 ionic polymer Polymers 0.000 description 1
- GELKBWJHTRAYNV-UHFFFAOYSA-K lithium iron phosphate Chemical compound [Li+].[Fe+2].[O-]P([O-])([O-])=O GELKBWJHTRAYNV-UHFFFAOYSA-K 0.000 description 1
- ZAUUZASCMSWKGX-UHFFFAOYSA-N manganese nickel Chemical compound [Mn].[Ni] ZAUUZASCMSWKGX-UHFFFAOYSA-N 0.000 description 1
- 230000010534 mechanism of action Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 229910021518 metal oxyhydroxide Inorganic materials 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 229910052596 spinel Inorganic materials 0.000 description 1
- 239000011029 spinel Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- LSGOVYNHVSXFFJ-UHFFFAOYSA-N vanadate(3-) Chemical compound [O-][V]([O-])([O-])=O LSGOVYNHVSXFFJ-UHFFFAOYSA-N 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
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- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
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CN201510195223.2A CN104891570B (en) | 2015-04-19 | 2015-04-19 | A kind of liquid phase synthesis Zr4+Doping fluorination bismuth anode material for lithium-ion batteries and preparation method thereof |
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CN201510195223.2A CN104891570B (en) | 2015-04-19 | 2015-04-19 | A kind of liquid phase synthesis Zr4+Doping fluorination bismuth anode material for lithium-ion batteries and preparation method thereof |
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CN104891570A true CN104891570A (en) | 2015-09-09 |
CN104891570B CN104891570B (en) | 2017-07-25 |
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CN201510195223.2A Expired - Fee Related CN104891570B (en) | 2015-04-19 | 2015-04-19 | A kind of liquid phase synthesis Zr4+Doping fluorination bismuth anode material for lithium-ion batteries and preparation method thereof |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106190109A (en) * | 2016-07-01 | 2016-12-07 | 深圳市亚辉龙生物科技股份有限公司 | Chemiluminescence intensifier and chemiluminescence immune detection reagent kit |
CN106876681A (en) * | 2017-03-25 | 2017-06-20 | 宁波吉电鑫新材料科技有限公司 | A kind of continuous conduction liquid phase synthesis C/Bi/BiF3Compound fluorination bismuth anode material for lithium-ion batteries and preparation method thereof |
CN106876706A (en) * | 2017-03-25 | 2017-06-20 | 宁波吉电鑫新材料科技有限公司 | A kind of monolithic conductive original position C/Bi/BiF3Compound fluorination bismuth anode material for lithium-ion batteries and preparation method thereof |
CN106953083A (en) * | 2017-03-25 | 2017-07-14 | 宁波吉电鑫新材料科技有限公司 | A kind of continuous conduction original position C/ metal solid solutions/Ni2+,Ca2+Adulterate BiF3Positive pole and preparation method |
CN106953082A (en) * | 2017-03-25 | 2017-07-14 | 宁波吉电鑫新材料科技有限公司 | A kind of non-acid system liquid phase synthesis C/ metal solid solutions/Ba2+,Ce4+Adulterate BiF3Positive pole and preparation method |
US10745425B2 (en) | 2016-07-01 | 2020-08-18 | Shenzhen Yhlo Biotech Co., Ltd. | Chemiluminescence enhancer and chemiluminescence immunodetection kit |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20070243466A1 (en) * | 2004-10-01 | 2007-10-18 | Rutgers, The State University | Bismuth Fluoride Based Nanocomposites as Electrode Materials |
CN101212050A (en) * | 2007-12-21 | 2008-07-02 | 湘潭大学 | Method for producing bismuth trifluoride anode material of Li secondary battery |
CN102299328A (en) * | 2011-08-31 | 2011-12-28 | 北京理工大学 | Metal fluoride cathode material of lithium secondary battery and preparation method of cathode material |
CN104157836A (en) * | 2014-07-14 | 2014-11-19 | 宁波大学 | Cu<2+>, Co<2+>, Zr<4+> and Ag+ doped ferric fluoride composite anode material and preparation method |
-
2015
- 2015-04-19 CN CN201510195223.2A patent/CN104891570B/en not_active Expired - Fee Related
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20070243466A1 (en) * | 2004-10-01 | 2007-10-18 | Rutgers, The State University | Bismuth Fluoride Based Nanocomposites as Electrode Materials |
CN101212050A (en) * | 2007-12-21 | 2008-07-02 | 湘潭大学 | Method for producing bismuth trifluoride anode material of Li secondary battery |
CN102299328A (en) * | 2011-08-31 | 2011-12-28 | 北京理工大学 | Metal fluoride cathode material of lithium secondary battery and preparation method of cathode material |
CN104157836A (en) * | 2014-07-14 | 2014-11-19 | 宁波大学 | Cu<2+>, Co<2+>, Zr<4+> and Ag+ doped ferric fluoride composite anode material and preparation method |
Non-Patent Citations (2)
Title |
---|
孟根其其格: "《化工机器》", 31 January 2013, 北京理工大学出版社 * |
胡本安: "锂离子电池铋基正极材料的制备、改性及性能研究", 《中国优秀硕士学位论文全文数据库 工程科技I辑》 * |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106190109A (en) * | 2016-07-01 | 2016-12-07 | 深圳市亚辉龙生物科技股份有限公司 | Chemiluminescence intensifier and chemiluminescence immune detection reagent kit |
US10745425B2 (en) | 2016-07-01 | 2020-08-18 | Shenzhen Yhlo Biotech Co., Ltd. | Chemiluminescence enhancer and chemiluminescence immunodetection kit |
CN106876681A (en) * | 2017-03-25 | 2017-06-20 | 宁波吉电鑫新材料科技有限公司 | A kind of continuous conduction liquid phase synthesis C/Bi/BiF3Compound fluorination bismuth anode material for lithium-ion batteries and preparation method thereof |
CN106876706A (en) * | 2017-03-25 | 2017-06-20 | 宁波吉电鑫新材料科技有限公司 | A kind of monolithic conductive original position C/Bi/BiF3Compound fluorination bismuth anode material for lithium-ion batteries and preparation method thereof |
CN106953083A (en) * | 2017-03-25 | 2017-07-14 | 宁波吉电鑫新材料科技有限公司 | A kind of continuous conduction original position C/ metal solid solutions/Ni2+,Ca2+Adulterate BiF3Positive pole and preparation method |
CN106953082A (en) * | 2017-03-25 | 2017-07-14 | 宁波吉电鑫新材料科技有限公司 | A kind of non-acid system liquid phase synthesis C/ metal solid solutions/Ba2+,Ce4+Adulterate BiF3Positive pole and preparation method |
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Publication number | Publication date |
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CN104891570B (en) | 2017-07-25 |
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