CN104878404A - Emulsion-type antirust cleaning agent and preparation method thereof - Google Patents
Emulsion-type antirust cleaning agent and preparation method thereof Download PDFInfo
- Publication number
- CN104878404A CN104878404A CN201510234152.2A CN201510234152A CN104878404A CN 104878404 A CN104878404 A CN 104878404A CN 201510234152 A CN201510234152 A CN 201510234152A CN 104878404 A CN104878404 A CN 104878404A
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- CN
- China
- Prior art keywords
- emulsion
- cleaning agent
- rust
- preparation
- type antirust
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000012459 cleaning agent Substances 0.000 title claims abstract description 10
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000002480 mineral oil Substances 0.000 claims abstract description 9
- 235000010446 mineral oil Nutrition 0.000 claims abstract description 9
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 7
- 239000003208 petroleum Substances 0.000 claims abstract description 7
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 7
- 239000011734 sodium Substances 0.000 claims abstract description 7
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 7
- 229910052788 barium Inorganic materials 0.000 claims abstract description 6
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000003899 bactericide agent Substances 0.000 claims abstract description 5
- 229920000570 polyether Polymers 0.000 claims abstract description 4
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 claims abstract description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 3
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000003921 oil Substances 0.000 claims description 9
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- RAADJDWNEAXLBL-UHFFFAOYSA-N 1,2-di(nonyl)naphthalene Chemical compound C1=CC=CC2=C(CCCCCCCCC)C(CCCCCCCCC)=CC=C21 RAADJDWNEAXLBL-UHFFFAOYSA-N 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 4
- 229960004418 trolamine Drugs 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 abstract description 17
- 229910052751 metal Inorganic materials 0.000 abstract description 12
- 239000002184 metal Substances 0.000 abstract description 12
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 8
- 238000000034 method Methods 0.000 abstract description 7
- 230000004224 protection Effects 0.000 abstract description 5
- 239000004721 Polyphenylene oxide Substances 0.000 abstract 1
- 230000003749 cleanliness Effects 0.000 abstract 1
- 208000002741 leukoplakia Diseases 0.000 abstract 1
- 239000010721 machine oil Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 description 12
- 230000002265 prevention Effects 0.000 description 7
- 239000006260 foam Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 229910000831 Steel Inorganic materials 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000010408 film Substances 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000004945 emulsification Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004663 powder metallurgy Methods 0.000 description 2
- DAJSVUQLFFJUSX-UHFFFAOYSA-M sodium;dodecane-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCS([O-])(=O)=O DAJSVUQLFFJUSX-UHFFFAOYSA-M 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- VUWCWMOCWKCZTA-UHFFFAOYSA-N 1,2-thiazol-4-one Chemical class O=C1CSN=C1 VUWCWMOCWKCZTA-UHFFFAOYSA-N 0.000 description 1
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 1
- 206010044565 Tremor Diseases 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 230000032798 delamination Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 150000003016 phosphoric acids Chemical class 0.000 description 1
- 229920000151 polyglycol Polymers 0.000 description 1
- 239000010695 polyglycol Substances 0.000 description 1
- 239000011253 protective coating Substances 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000010729 system oil Substances 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
Abstract
The invention provides an emulsion-type antirust cleaning agent and a preparation method thereof. The emulsion-type antirust cleaning agent comprises the following components in percentage by mass: 50%-60% of machine oil, 9%-12% of petroleum sodium sulfonate, 5%-8% of dinonyl-naphthalenesulfonic aci barium, 1.8%-3% of polyether, 3%-5% of alcohol alkoxylate, 0.4%-0.6% of butyl cellosolve, 0.7%-1.2% of triethanolamine, 1.5%-3% of an anticorrosion and bactericidal agent and the balance of mineral oil. The emulsion-type antirust cleaning agent can be applied to greasy dirt cleaning of black metal and non-ferrous metal, and rust protection between procedures and short-term rust protection, is good in dispersing and stripping effects on greasy dirt, and simultaneously has an anti-rust effect between the procedures; the anti-rust workpiece is bright and clean in surface, free of a decorative design, leukoplakia or spots, can well meet the requirements on the cleanliness and the brightness of the workpiece surface, and is simple in preparation process, low in cost, and free of an odor; and the discharge is free of pollution to the environment.
Description
technical field:
The present invention relates to a kind of anti-rust cleaning agent and preparation method, particularly relate to a kind of emulsion-type antirust clean-out system and preparation method thereof.
background technology:
In the manufacturing process to ferrous metal and non-ferrous metal, as in the steel product or steel products of Iron and Steel Production, oil removing or decontamination cleaning to be carried out to ferrous metal component or non-ferrous metal products, simultaneously also will to its antirust treatment, then lower road technique is entered, occurred that the aqueous component such as decorative pattern, hickie, spot remain by clean metal surface after adopting conventional clean agent cleaning, so seriously have impact on processing to ferrous and nonferrous metals and production, particularly all have larger impact to the surface smoothness etc. of processed product.
On the other hand, at present, during manufacturing process to ferrous metal and non-ferrous metal on market, its clean-out system function singleness used, as otherwise only there is cleaning function and do not have antirust effect, and in use usually can not spray use because clean-out system existing in cleaning process can produce a large amount of foams.The clean-out system raw material simultaneously used in existing rinse product generally contains strong acid salt, as chromic salt, and borons acid salt, nitrite, phosphoric acid salt etc.; The waste water waste materials of discharging etc. are to environment.And after adopting pure clean-out system to clean described product, also to carry out antirust treatment, add workman's work production intensity, add one production process, this also just adds the production cost of product.
summary of the invention:
The invention provides a kind of emulsion-type antirust clean-out system and preparation method thereof, it can be used for greasy dirt cleaning and rust prevention during manufacture, the short-term rust prevention of ferrous metal and non-ferrous metal, it is good to greasy dirt dispersion, peeling effect, there is rust prevention during manufacture effect simultaneously, and it is bright and clean through antirust workpiece surface, without decorative pattern, hickie, spot, workpiece surface degree of cleaning, luminance brightness requirement can be met well, and it is long according to the different antirust time of working concentration during cleaning, product is not containing strong acid salt, and manufacture craft is simple, and cost is low, odorlessness, ejecta environmentally safe.
A kind of emulsion-type antirust clean-out system of the present invention, comprises following quality and forms than component:
Machinery oil 50-60%,
Petroleum sodium sulfonate 9-12%,
Dinonyl naphthalene sulfonate barium 5-8%,
Polyethers 1.8-3%,
Isomeric alcohol polyethenoxy ether 3-5%,
Butyl glycol ether 0.4-0.6%,
Trolamine 0.7-1.2%,
Anticorrosion and bactericidal agent 1.5-3%,
Mineral oil subsidy to 100%.
Another object of the present invention is the preparation method of described emulsion-type antirust clean-out system, and it is prepared as follows: under normal temperature condition, is first dissolved in machinery oil by petroleum sodium sulfonate, dinonyl naphthalene sulfonate barium; Then add other raw materials except mineral oil successively and be stirred to transparent, finally add mineral oil and be constantly stirred to transparent; Obtain product of the present invention.
Anti-rust cleaning agent of the present invention, except above-mentioned substance component, can also allow to add other materials, as other sodium salt, as sodium laurylsulfonate etc.
Stability: anti-rust cleaning agent composition prepared by the present invention is placed after 4-6 hour and observed solution delamination, and stabilize to not stratified, not muddy, shakiness is decided to be layering or muddiness.
Cleaning rate: cleaning rate=wash mixed dirt weight/mixed dirt original weight.
The present invention adopts said components to have following features: one is, it is good to greasy dirt dispersion, peeling effect, simultaneously
There is rust prevention during manufacture effect, and different according to working concentration during cleaning, its rust prevention during manufacture effect can be up to half a year more than;
Two is that anti-rust cleaning agent of the present invention combines the performance advantage of oil product and the advantage of aqueous product environmental protection, has multi-usage attribute and still to low bubble performance, can flexible Application in methods such as various spray, immersion, showerings;
Three is short-term rust prevention protections that this product of the present invention is also applicable to various special type application, as powder metallurgy cleaning rust-proof, can directly use; Also be applicable to the short-term rust prevention protection of various special type application, as powder metallurgy cleaning rust-proof, can directly use, water, solvent or oil dilution can be used to use;
Four are antirust film protective layers that anti-rust cleaning agent of the present invention is formed is films inconspicuous, and does not have film wrinkle, makes to detect, process, and packaging is all more prone to; And compatible with most terminal rust-preventive agent, can running cost be reduced, when part short-term indoor storage, not need the thinfilm protective coating removing this product.
Clean-out system foam control of the present invention designs and uses in Sprayer Circulation cleaning, produces the shortcoming of a large amount of foam when overcoming the cleaning of conventional emulsification type clean-out system; Even if in hard water, product water latex emulsion of solubleness also can keep satisfactory stability.Product of the present invention overcomes the shortcoming that conventional emulsification type clean-out system foam easy to foaming is not suitable for cleaning showers on the other hand simultaneously, and the low bubble of product, to still, can meet the requirement of cleaning showers completely.
Product of the present invention detects through Institute of Analysis of Jiangxi Province, and all technical all reaches requirement, and concrete all technical sees the following form 1
Test atmosphere condition, temperature: 20 DEG C, humidity: 55%,
Test basis, GB, T44721984 etc.,
Testing instruments, automatical potentiometric titrimeter etc.,
Sample situation, sampling, liquid;
The all technical of product of the present invention is as follows.
Table 1
Illustrate: product of the present invention after testing indices all reaches requirement.
embodiment:below in conjunction with embodiment, the present invention is described in further detail.
embodiment:as follows
Illustrate: petroleum sodium sulfonate of the present invention can be sodium laurylsulfonate, and polyethers has another name called polyglycol ether, machinery oil is total loss system oil described on market.Anticorrosion and bactericidal agent be can be used for clean-out system anticorrosion and bactericidal agent as isothiazolinone compounds, above-mentioned each component of the present invention is all commercially available.
The various embodiments described above of the present invention are all prepared by following method: under normal temperature condition, are first dissolved in machinery oil by petroleum sodium sulfonate, dinonyl naphthalene sulfonate barium; Then add other raw materials except mineral oil successively and be stirred to transparent, finally add mineral oil and be constantly stirred to transparent, obtaining product transparent liquid of the present invention.
Claims (2)
1. an emulsion-type antirust clean-out system, comprises following quality and forms than component:
Machinery oil 50-60%,
Petroleum sodium sulfonate 9-12%,
Dinonyl naphthalene sulfonate barium 5-8%,
Polyethers 1.8-3%,
Isomeric alcohol polyethenoxy ether 3-5%,
Butyl glycol ether 0.4-0.6%,
Trolamine 0.7-1.2%,
Anticorrosion and bactericidal agent 1.5-3%,
Mineral oil subsidy to 100%.
2. according to a preparation method for newborn type anti-rust cleaning agent according to claim 1, it is characterized in that preparing as follows: under normal temperature condition, first petroleum sodium sulfonate, dinonyl naphthalene sulfonate barium are dissolved in machinery oil; Then add other raw materials except mineral oil successively and be stirred to transparent, finally add mineral oil and be constantly stirred to transparent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510234152.2A CN104878404B (en) | 2015-05-11 | 2015-05-11 | Emulsion-type antirust cleaning agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510234152.2A CN104878404B (en) | 2015-05-11 | 2015-05-11 | Emulsion-type antirust cleaning agent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104878404A true CN104878404A (en) | 2015-09-02 |
| CN104878404B CN104878404B (en) | 2017-06-20 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510234152.2A Active CN104878404B (en) | 2015-05-11 | 2015-05-11 | Emulsion-type antirust cleaning agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104878404B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106148987A (en) * | 2016-06-25 | 2016-11-23 | 佛山市三水金大田门业有限公司 | A kind of steel casement door rustless steel cleaning agent |
| CN106637271A (en) * | 2017-02-13 | 2017-05-10 | 江苏广通管业制造有限公司 | Technology for removing rust on surface of brass corrugated pipe |
| CN108004053A (en) * | 2017-12-19 | 2018-05-08 | 山东联星能源集团有限公司 | A kind of detergent and preparation method of efficient communications equipment of rationing the power supply for military nothing |
| CN108149253A (en) * | 2017-11-29 | 2018-06-12 | 中国海洋石油集团有限公司 | Antiseptic treating agent and its preparation, construction method in a kind of coiled tubing |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1353173A (en) * | 2001-11-21 | 2002-06-12 | 蔡毓英 | Dewatering antirust oil |
| JP2009084390A (en) * | 2007-09-28 | 2009-04-23 | Dai Ichi Kogyo Seiyaku Co Ltd | Metal cleaning agent composition and metal cleaning agent |
| CN102787006A (en) * | 2012-07-20 | 2012-11-21 | 诺泰生物科技(合肥)有限公司 | Extreme-pressure metalworking liquid and its preparation method |
-
2015
- 2015-05-11 CN CN201510234152.2A patent/CN104878404B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1353173A (en) * | 2001-11-21 | 2002-06-12 | 蔡毓英 | Dewatering antirust oil |
| JP2009084390A (en) * | 2007-09-28 | 2009-04-23 | Dai Ichi Kogyo Seiyaku Co Ltd | Metal cleaning agent composition and metal cleaning agent |
| CN102787006A (en) * | 2012-07-20 | 2012-11-21 | 诺泰生物科技(合肥)有限公司 | Extreme-pressure metalworking liquid and its preparation method |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106148987A (en) * | 2016-06-25 | 2016-11-23 | 佛山市三水金大田门业有限公司 | A kind of steel casement door rustless steel cleaning agent |
| CN106637271A (en) * | 2017-02-13 | 2017-05-10 | 江苏广通管业制造有限公司 | Technology for removing rust on surface of brass corrugated pipe |
| CN108149253A (en) * | 2017-11-29 | 2018-06-12 | 中国海洋石油集团有限公司 | Antiseptic treating agent and its preparation, construction method in a kind of coiled tubing |
| CN108149253B (en) * | 2017-11-29 | 2020-03-31 | 中国海洋石油集团有限公司 | Anti-corrosion treatment agent for interior of continuous oil pipe and preparation and construction methods thereof |
| CN108004053A (en) * | 2017-12-19 | 2018-05-08 | 山东联星能源集团有限公司 | A kind of detergent and preparation method of efficient communications equipment of rationing the power supply for military nothing |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104878404B (en) | 2017-06-20 |
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| CP03 | Change of name, title or address |
Address after: 336000 No. 39, Chunfeng Road, Yichun Economic and Technological Development Zone, Jiangxi Province Patentee after: Jiangxi Ruisibo New Material Co.,Ltd. Address before: No. 585, Huancheng South Road, Yuanzhou District, Yichun City, Jiangxi Province Patentee before: JIANGXI RUISIBO CHEMICAL ENGINEERING Co.,Ltd. |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Emulsified antirust cleaner and its preparation method Effective date of registration: 20230130 Granted publication date: 20170620 Pledgee: Yichun Branch of China Everbright Bank Co.,Ltd. Pledgor: Jiangxi Ruisibo New Material Co.,Ltd. Registration number: Y2023980031789 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20170620 Pledgee: Yichun Branch of China Everbright Bank Co.,Ltd. Pledgor: Jiangxi Ruisibo New Material Co.,Ltd. Registration number: Y2023980031789 |